The present disclosure relates to a process for synthesizing alkyl thiopyrazole. The process in accordance with the present disclosure comprises reacting an alkyl sulfenyl halide, an aminopyrazole, an amine salt and a solvent in an inert atmosphere in the temperature range of -20 to 50°C. The alkyl sulfenyl halide c...
Novel methodology has been presented towards preparation of carbazates further deployed in preparation of semicarbacones maintaining enantiomeric integrity throughout. These semicarbazones and derivatives thereof are of possess arthropodicida properties.
The present disclosure relates to an improved diazotization process for the preparation of 5-amino-3-cyano-1-(2,6-dichloro-4-trifluoromethylphenyl) pyrazole.
A process for preparation of Fipronil (I) from 5- Amino-1-(2,6-dichloro-4-trifluoromethyl pghenyl)-3-cyano-4-trifluromethyl thio pyrazole (II) by oxidation in trichloro acetic acid enriched medium.
The present disclosure relates to a process for preparing trifluoromethanesulfinyl chloride in high yield and high purity. The process of the present disclosure comprises oxidizing o-chlorobenzyltrifluoromethane sulfide to obtain o-chlorobenzyltrifluoromethane sulfoxide, followed by chlorinating o-chlorobenzyltriflu...
The present disclosure relates to a process for preparing 1-(4-chlorophenyl)-3-hydroxypyrazole. The process involves cyclization of 4-chlorophenylhydrazine hydrochloride and alkyl acrylate by using at least one base and at least one first fluid medium to obtain 1-(4-chlorophenyl)-3-pyrazolidinone (pyrazolidinone). T...
The present disclosure relates to a process for production of Temephos having purity greater than 95 %w/w and having Iso-Temephos content less than 1.2 %w/w. The process in accordance with the present disclosure comprises contacting a solution containing dissolved crude Temephos with modified acidic alumina at a tem...
Undesired regioisomer 2-chloro-5-trifluoromethylaniline is formed along with intermediate 2-chloro-4-trifluoromethylaniline in the ammonolysis of 3, 4-dichlorobenzotrifluoride during synthesis of the agrochemical Fipronil. Since this regioisomer is formed in significant amount, overall yield is low. This problem is ...
The present disclosure relates to a process for the synthesis of 2-bromo-4-methyl phenol. The process comprises brominating 4-methyl phenol in the absence of light in a solvent using a brominating agent at a temperature ranging from 200C to 400C.
5-Amino-3-cyano-1-(2,6-dichloro-4-triflouromethylphenyl)pyrazole is an important intermediate in the synthesis of Fipronil. Process for preparing this substituted amino-pyrazole derivative comprises converting 2,6-dichloro-4-trifluormethylaniline into its diazotization salt followed by reaction with ethyl 2,3-dicyan...
The present disclosure relates to a synergistic insecticidal composition comprising Indoxacarb and fipronil. The composition shows synergistic insecticidal activity. The composition of the present disclosure has high bioefficacy, is cost-effective and environment friendly.
The present disclosure relates to a process for preparing polyetherimide. The process of the present disclosure is simple and economic and takes place in short duration of time. The process of the present disclosure comprises reacting bis(ether anhydride) with at least one diamine in the presence of an accelerator t...
The present disclosure relates to a process for the preparation of 3-(4-isopropyl)phenyl-1,1-dimethylurea.
3-(4-isopropyl)phenyl-1,1-dimethylurea is used as a herbicidal agent.
In the present disclosure, 3-(4-isopropyl)phenyl-1,1-dimethylurea is prepared by reaction of 4-isopropylaniline, methyl haloformate, and d...
The preparation of (E)-N1-[(6-chloro-3-pyridyl)methyl]-N2-cyano-N1-methylacetamidine (Acetamiprid) using equivalent moles of pure 2-chloro-5-(methylaminomethyl)pyridine with N-cyanomethylacetimidate without use of any organic solvent or water at 35 to 60 degree/C to produce high yield and high purity Acetamipride in...
The present invention relates to a block copolymer comprising of at least two types homoblocks, all belonging to the polysulfone family, wherein each of the said homoblock has an identical or different molecular weight of at least 1000 and has at least 5% of the overall weight and wherein the block copolymer has a m...
This invention relates to a process for the preparation of polyaryl ether nitriles (PAEN) by the polymerization of a dihalo benzonitrile with at least one dihydroxy aryl compound in the presence of a base in a polar aprotic solvent, wherein the polymer being formed is maintained in solution in the solvent during the...
Process for preparation of Quinopthalone (I) pigment using a solvent mixture
(I)
10
comprising of an aromatic carboxylic acid or substituted aromatic carboxylic acid having melting point between 110°C to 180°C with the aromatic hydrocarbon or chlorinated aromatic hydrocarbons on heating at predetermined temperatu...
The present invention describes the preparation of novel azo pigments, represented by structure (II) from 2-amino acridone derivatives, prepared by known methods and as described by structure (I). ‘A’ in above structure (II) represents various coupling components described herein.
X = Chloro, Bromo, Fluoro
8-Aminoquinoline derivative (II, R = CH₃) is prepared from 8-Haloquinoline derivative (I, R=CH₃) by reacting aq. ammonia solution with the 8-Haloquinoline derivative in the presence of Copper catalyst.
The present invention relates to the use of a new catalyst for the oxidation of hydroxylated and alkoxylated derivatives of the phenyl glyoxylic acid to obtain hydroxylated and alkoxylated aromatic aldehyde derivatives. The invention particularly describes the preparation of vanillin and ethyl vanillin. The scope of...
Carbamic Acid- (chlorocarbonyl)-[(4-Trifluoromethoxy) phenyl] methyl ester compound (I) is prepared reaction of p-Trifluoromethoxy aniline carbate compound with Triphosgene (CI₃OC₃OOCI₃) or Diphosgene (CIC₂OOCI₃) in the presence of aliphatic tertiary amines with C₁-C4 alkyl like triethyl amine, tributyl amine tri is...
The present invention relates to a process of preparing a block copolymer and the block copolymer prepared therefrom comprising of at least two types homoblocks, all belonging to the polysulfone family, wherein each of the said homoblock has an identical or different molecular weight of at least 1000 and has at leas...
A process for the preparation of an alkali metal salt of 4-chloro-4’-hydroxy benzophenone comprising of the steps of (a) preparing purified 4-chloro-4’ hydroxy benzophenone by a process comprising distilling under reduced pressure a liquid containing 4-chloro-4’-hydroxy benzophenone and a solvent selected from diphe...
The present invention describes the preparation of PY-139, an isoindoline class of pigment, as represented by structure no 1 in aqueous media and in the presence of suitably substituted aromatic carboxylic acid as represented by structure no 2.
4-Chloro, 4’-Hydroxy Benzophenone (I) was prepared in 71-72% total yield and >99.5% purity. A one pot synthesis of I by acylation of phenol with 4-Chloro, 4’-Hydroxy Benzophenone in the presence of AICI3 and workup of the reaction mass to give Crude (I) in >95% purity and Yield of 85%. Crude (I) was further purified...
4-Chloro-4'-hydroxybenzophenone - preferably prepared by reaction of 4-chlorobenzoyl chloride and phenol using AlClз catalyst in orthodichlorobenzene solvent - is purified by distillation under vacuum, more conveniently in combination with a solvent such as diphenyl sulfone, to give a high purity monomer which can b...
Process for preparation of 4-Chloro, 4’-hydrroxy benzophenone (I) by reacting p-Chlorobenzoyl chloride with anisole and Aluminum chloride in a suitable solvent at a particular temperature during charging and thereafter heating for a certain for a certain period in a “one-pot” process for subsequent de-methylation in...
The method disclosed herein comprises of a process to prepare exclusively 4,4"- isomer of a monomeric sulfone of the formula
Where X=Halogen, (For X=CI) the compound 4, 4’-bis (4-chlorobenzenesulfonyl) diphenylsulfone in high yield and in high purity by blending an alkali metal salt of p-chlorobenzenesulfonyl chlor...
2-isopropl phenol, a useful building block for the manufacture of agrochemicals, UV stabilizers, polymerization inhibitors and anti-oxidants, is prepared, starting from o-nitro cumene (ONC) in high yield and purity by hydrogenation, followed by diazotization and hydrolysis. 2-nitro cumene is a by product obtained in...
This invention relates to a process for the preparation of quinacridone pigments of the formula (I) employing (a) heating, at a temperature of about 80deg C to about 145 deg C, a reaction mixture comprising (i) 2,5-dianilinoterephthalic acid or a 2,5-
dianilinoterephthalic acid or its ester or derivative having one...
The present disclosure provides an industrially feasible process for the preparing an imidazolidone compound 2-[4,5-dihydro-4-methyl-4-(l-methylethyl)-5-oxo-lH-imidazol-2-yl]-5-ethyl-3-pyridinecarboxylic acid of formula I,
The process involves condensing 5-ethyl-2,3-diethyl pyridine dicarboxylate and 2,3-dimet...
The present disclosure relates to a process for the preparation of 4,6-dialkoxy-2-(alkylsulfonyl)pyrimidine, said process comprising reacting dialkyl malonate and thiourea in the presence of sodium alkoxide and an alcohol to obtain a sodium salt of thiobarbiruric acid; alkylating said salt of thiobarbituric acid wit...
The present disclosure provides a process for the preparation of Bispyribac-metal salt which involves reacting 2,6-dihydroxy benzoic acid with dialkyl sulphate using a base in a solvent to form 2,6-dihydroxy alkyl benzoate; condensing 2-(methylsulfonyl)-4,6-dimethoxy pyrimidine with 2,6-dihydroxyalkyl benzoate to ob...
The present disclosure relates to a process for the preparation of 2, 6-dihydroxybenzoic acid, said process comprises carboxylating resorcinol in the presence of carbon dioxide and at least one base in at least one solvent at a temperature ranging between 100 and 200 °C to obtain a mixture containing 2, 6-dihydroxyb...
The present disclosure relates to a process for the preparation of Bispyribac sodium; said process comprises condensing 2,6-dihydroxy benzoic acid with 2-(aIkyl sulfonyl)-4,6-dialkoxy pyrimidine at a temperature ranging between 20 and 80 C in the presence of at least one base and at least one solvent.
...
The present invention relates to a process of preparing block copolymers comprising of at lest two types of homoblocks, selected from either PSSD, PSSB, TPES, PSS, TMPSS or PESK or selected from at least one of PSSD, PSSB, TPES, PSS, TMPSS or PESK and at least one of PPSU, PES or PSU, wherein each of the said homobl...
The present disclosure relates to a process for preparing a deltamethric acid. The process in accordance with the present disclosure comprises hydrolyzing cypermethric acid ester in the presence of an aqueous solution of a sulfur containing acid. The deltamethric acid is extracted after the complete hydrolysis of th...
The present disclosure relates to a process for preparing a compound of Formula 1,
Formula 1
from a compound of Formula 2,
Formula 2
wherein, the substituents have the meaning as defined in the description. The process comprises a step of hydrolyzing the compound of Formula 2 in an acidic reaction medium...
The present invention relates to a process of oxidation of a sulfenyl compound to a sulfinyl compound. The process involves the steps of reacting a sulfenyl compound with at least one acid, in the presence of at least one phase transfer catalyst and in a solvent to obtain a solution. The oxidizing agent is added dro...
The present disclosure relates to the process of preparation of 4,4’-biphenol, wherein p-bromophenol is subjected to biaryl coupling reaction using at least one base along with Pd/C as a catalyst and at least one reducing agent selected from hydroxylamine sulfate [(NH2OH)2H2SO4] and hydroxylamine hydrochloride follo...
The present disclosure relates to a process for preparing halogenated aromatic compounds. The process comprising mixing at least one alkali salt of a hydro-halo acid, at least one solvent, at least one phase transfer catalyst, at least one aromatic acid dihalide, component, and at least one nitro-aromatic compound t...
Process for preparation of 5-chloro-1,3-phenylenediamine (I) comprises of the steps starting from isophthalic acid to isophthaloyl chloride followed by 5-chloroisophthaloyl chloride using chlorine and a chlorine carrier such as iron chloride at high temperature of 100°C to 200°C for a time period of 10 to 20 hours i...
The present invention relates to a novel crystalline form of 5-amino-1-(2, 6-dichloro-4-trifluoromethylphenyl)-3-cyano-4-ethyl sulfinyl pyrazole. The crystalline form of 5-amino-1-(2, 6-dichloro-4-trifluoromethylphenyl)-3-cyano-4-ethyl sulfinyl pyrazole is described using X-ray powder diffraction patterns, an infrar...
The present disclosure provides a process for preparing 2,3-dicyanopropionic acid ester of formula (I) by 2-cyano-2-propenoic acid ester of formula (II) and/or polymer of 2-cyano-2-propenoic acid ester of formula (III),
wherein, R is selected from the group consisting of C1-C20 straight or branched chain alkyl...
Copolymers of PEEK and PEEK/PEK and methods of preparation thereof are provided. The melt temperatures of the PEEK copolymer and PEEK/PEK copolymer compositions are in the range of 350 °C to 420 °C. The compositions are based on PEEK monomers biphenol and 4,4’-difluorobenzophenone with other PEEK co-monomers such as...
The present invention relates to a process for the preparation of N-alkyl carbazole; said process comprising a)chlorinating cyclohexanone to form 2-chlorocyclohexanone; b)reacting 2-chlorocylohexanone with N-ethyl aniline to form 2-(N-ethyl anilino) cyclohexanone; c) cyclizing 2-(N-ethyl anilino) cyclohexanone by re...
The present disclosure relates to a polymeric blend composite. The polymeric blend composite comprises 60 wt% to 99 wt% Poly Ether Ketone Ketone (PEKK), 1 wt% to 6 wt% Multi walled carbon nanotubes (MWCNTs), and 0 wt% to 40 wt% Poly-(2,5-Benzimidazole) (ABPBI). The present disclosure further provides a process for p...
The present disclosure relates to a polymeric blend composite comprising Poly Ether Ketone/Poly-(2,5-Benzimidazole) containing Multi walled carbon nanotubes (MWCNTs) between 0.5 to 5 wt% were melt processed on a twin-screw extruder and granules so obtained were injection molded to determine heat deflection temperatu...
ABSTRACT
PROCESS FOR THE PREPARATION OF 3-CHLORO-2-HYDRAZINOPYRIDINE
The present disclosure relates to a process for preparing 3-chloro-2-hydrazinopyridine. The process of the present disclosure obtains 3-chloro-2-hydrazinopyridine having a purity greater than 95% and a yield = 85%. The process of the present disc...
The present disclosure relates to a process for the preparation of trifluoromethanesulfinyl chloride. Trifluoromethanesulfinyl chloride is used as an intermediate for preparing pesticides and insecticides. Trifluoromethanesulfinyl chloride is represented by Formula I:
The present disclosure provides a simple, ec...
ABSTRACT
A PROCESS FOR PREPARING CRYSTALLINE PINOXADEN
The present disclosure relates to a process for preparing crystalline pinoxaden. The process of the present disclosure provides the pinoxaden form G. The crystalline pinoxaden form G has purity in the range of 95% to 99.8%. The process is simple, environmental...
ABSTRACT
A PROCESS FOR PREPARING CRYSTALLINE SULFENTRAZONE
The present disclosure relates to a process for preparing crystalline sulfentrazone. The process comprises treating sulfentrazone with an aqueous solution of an alkali salt, to obtain a mixture comprising sulfentrazone. The mixture is dissolved in an aqueo...
ABSTRACT
A PROCESS FOR PREPARATION OF PYRACLOSTROBIN
The present disclosure relates a process for preparing pyraclostrobin (I). The process involves partial reduction of PNBE (II) to obtain PHABE (III), followed by methoxycarbonylation to obtain PHABEC (IV). The PHABEC (IV) is methylated to obtain the pyraclostrob...
ABSTRACT
SYNTHESIS OF MESOTRIONE
The present disclosure relates to a method for the synthesis of mesotrione.
The method comprises reacting p-toluene sulfonyl chloride with alkali metal sulphite and alkali metal bicarbonate to obtain p-toluene alkali metal sulfinate. The p-toluene alkali metal sulfinate is reacte...
The present disclosure relates to a process for preparation of 3-(3,4-dichlorophenyl)-1,1-dimethylurea.
3-(3,4-dichlorophenyl)-1,1-dimethylurea is used as a herbicidal agent.
In the present disclosure, 3-(3,4-dichlorophenyl)-1,1-dimethylurea is prepared by reaction of 3,4-dichloroaniline, methyl haloformate, and d...
The present disclosure relates to a process for synthesizing triclopyr butotyl (I). 3,5,6-Trichloropyridine-2-ol sodium (V), a first fluid medium and a phase transfer catalyst are mixed, and butoxyethyl-haloacetate (III), having purity in the range of 99 % to 99.9 %, is slowly added at 40 ?C to 80 ?C to obtain a fir...
The present disclosure relates to a process for preparing cartap hydrochloride. The process comprises amination of allyl chloride with dimethylamine in the presence of at least one base to obtain N,N-dimethylallylamine. Forming N,N-dimethylallylamine hydrochloride, followed by chlorination of N,N-dimethylallylamine ...
ABSTRACT
A PROCESS FOR THE PREPARATION OF TRICLOPYR-BUTOTYL
The present disclosure relates to a process for the preparation of triclopyr-butotyl. The fluid medium and the acid solution used in the process of the present disclosure can be recovered and recycled making the process environment friendly as well a...
ABSTRACT
A PROCESS FOR THE PREPARATION OF 2-BUTOXYETHYL CHLOROACETATE
The present disclosure relates to a process for the preparation of 2-butoxyethyl chloroacetate. The fluid medium and the catalyst used in the process of the present disclosure can be recovered and recycled thereby making the process environment...
ABSTRACT
A PROCESS FOR THE PREPARATION OF 2-BUTOXYETHYL CHLOROACETATE
The present disclosure relates to a process for the preparation of 2-butoxyethyl chloroacetate. The fluid medium used in the process of the present disclosure is recovered and recycled thereby making the process environment friendly as well as e...
5-acetoacetylamino-2-benzimidazolone is prepared by suspending the 5-amino-benzimidazolone in an organic solvent such as monochlorobenzene, xylene, toluene, dimethylsulfoxide, dichlorobenzene etc. and reacting it with aceto acetic ester viz. methyl, ethyl, butyl, isopropyl at reflux temperature of solvent ra...
This inceniton relates to an improved methodology for N-Carbomethoxylation using sodium hydride particularly of 1.3.4 oxadiazine of compound (II)having varios ratios of S:R. to achieve large scale manufacturing process for Oxadiazine of compund (I) with preservation of enantiomeric integrity through ou...
INSECTICIDAL SUSPENSION CONCENTRATE
The present disclosure relates to an insecticidal suspension concentrate. The insecticidal suspension concentrate comprises Indoxacarb and Fipronil as the active ingredients. The insecticidal suspension concentrate further comprises at least one rainfastness agent that assists in...
The present disclosure relates to a polymeric blend composite comprising Poly Ether Ketone/Poly-(2,5-Benzimidazole) containing Multi walled carbon nanotubes (MWCNTs) between 0.5 to 5 wt% are melt processed on a twin-screw extruder and granules so obtained were injection molded to determine electrical conductivities ...
ABSTRACT
A PROCESS FOR PREPARING 1,4,5-HEXAHYDRO OXADIAZEPINE HYDROCHLORIDE
The present disclosure relates to a process for preparing 1,4,5-hexahydro oxadiazepine hydrochloride. The process of the present disclosure provides 1,4,5–hexahydro oxadiazepine hydrochloride in comparatively high yield and high purity.
...
The present disclosure relates to spun ABPBI fibers and a process for the preparing spun ABPBI fibers using high molecular weight ABPBI dope solution suitable for spinning. The present disclosure further relates to the process for preparing high molecular weight ABPBI dope solution suitable for spinning. The spun AB...
The process of the present disclosure provides fipronil with a yield in the range of
75% to 90% and purity in the range of 95% to 97%. By the process of the present
disclosure, the amount of sulfone impurity i.e., 5-amino-1-(2,6-dichloro-4-
trifluoromethylphenyl)-3-cyano-4-trifluoro methylsulfonyl pyrazole in fip...
ABSTRACT
A PROCESS FOR PREPARATION OF CYPERMETHRIN INTERMEDIATE
The present disclosure relates to a process for the preparation of cypermethrin intermediate, having a general formula represented by:
Formula I
wherein, X is selected from CN, COOH, COCl, COOR, wherein R is selected from C1 to C10 alkyl.
The pr...
The present disclosure relates to a process for obtaining a mixture of Indoxacarb crystals having purity in the range of 95% to 99.5%. The S-isomer crystals are present in an amount in the range of 75% to 90% of the mixture. The raw material is crude Indoxacarb comprising impurities in an amount in the range of 10 w...
ABSTRACT
PROCESS FOR SYNTHESIS OF PYRAZOLIDINONE COMPOUNDS
The present disclosure relates to a process for the synthesis of pyrazolidinone, particularly alkyl 2-(3-chloropyridin-2-yl)-5-oxo-pyrazolidine-3-carboxylate (pyrazolidinone) compound. The process of the present disclosure is simple, economical, and produc...
ABSTRACT
PROCESS FOR SYNTHESIS OF PYRAZOLIDINONE COMPOUNDS
The present disclosure relates to a process for the synthesis of pyrazolidinone, particularly alkyl 2-(3-chloropyridin-2-yl)-5-oxo-pyrazolidine-3-carboxylate (pyrazolidinone) compound. The process of the present disclosure is simple, economical, and produc...
The present disclosure relates to a process for obtaining S-isomer crystals of Indoxacarb having purity in the range of 98% to 99%. The raw material is crude Indoxacarb comprising impurities in an amount in the range of 3 wt.% to 15 wt.%. The process of the present disclosure is simple, economical, and gives S-isome...
The present disclosure relates to a poly ether ketone ketone (PEKK) having terephthaloyl:isophthaloyl (T:I) ratio of 100:0, and a process for preparing the same. The process comprises of polymerizing 1, 4-bis (4-phenoxybenzoyl) benzene (EKKE) with terephthaloyl chloride (TPC), and an end capping agent in a fluid med...
ABSTRACT
PROCESS FOR THE PREPARATION OF CHLORANTRANILIPROLE
The present disclosure relates to a process for the preparation of Chlorantraniliprole. The process of the present disclosure is carried out at an ambient temperature by using an inorganic base which can be readily separated from Chlorantraniliprole. The ...
The present disclosure relates to a process for the synthesis of quaternary ammonium compounds. The quaternary ammonium compounds are known for antimicrobial properties.
The present disclosure relates to a process for the synthesis of quaternary ammonium compounds. The quaternary ammonium compounds are known for antimicrobial properties.
ABSTRACT
A PROCESS FOR THE SYNTHESIS OF 4-METHYL SULFONYL TOLUENE
The present disclosure relates to a process for the synthesis of 4-methyl sulfonyl toluene. The process comprises reacting 4-toluene sulfonyl chloride with sodium sulfite and a base in a fluid medium to obtain a sodium salt of 4-toluene sulfinic aci...
ABSTRACT
A PROCESS FOR THE PREPARATION OF CHLORANTRANILIPROLE
The present disclosure relates to a process for the preparation of Chlorantraniliprole. The process of the present disclosure is carried out at an ambient temperature by using an inorganic base which can be easily separated. The process is simple, effic...
ABSTRACT
A PROCESS FOR THE PREPARATION OF 2-NITRO-4-METHYLSULFONYL BENZOIC ACID
The present disclosure relates to a process for the preparation of 2-nitro-4-methylsulfonyl benzoic acid (NMSBA). The process of the present disclosure is simple, economical and environment-friendly.
ABSTRACT
A PROCESS FOR THE PREPARATION OF 2-(2,6-DIETHYL-4-METHYL-PHENYL)–MALONONITRILE
The present disclosure relates to a process for the preparation of 2-(2,6-diethyl-4-methyl-phenyl)–malononitrile. The process of the present disclosure is carried out devoid of palladium. The process is simple, efficient, envir...
ABSTRACT
A PROCESS FOR THE PREPARATION OF CARTAP HYDROCHLORIDE
The present disclosure relates to a process for the preparation of cartap hydrochloride. The process of the present disclosure is carried out in the presence of a fluid medium that can be readily separated, recovered, and recycled. The process is simpl...
ABSTRACT
A PROCESS FOR THE PREPARATION OF NITRILE HERBICIDES, THEIR ESTERS AND SALTS
The present disclosure relates to a process for the preparation of nitrile herbicides, their esters and salts. The process of the present disclosure provides nitrile herbicides, their esters and salts with high purity and in g...
ABSTRACT
PROCESS FOR PREPARATION OF AZOXYSTROBIN
The present disclosure relates to a process for preparing azoxystrobin. The process involves alkylating 2-hydroxybenzonitrile (II) with 4,6-dichloropyrimidine (III) using first base to obtain 2-[(6-chloropyrimidin-4-yl)oxy]benzonitrile (IV). (2-hydroxyphenyl)acetic ...
ABSTRACT
ISATIN DERIVATIVES AND A PROCESS FOR PREPARATION THEREOF
The present disclosure related to isatin derivatives and a process for preparation thereof. The process of the present disclosure is simple, efficient, environment friendly and economic.
ABSTRACT
A PROCESS FOR CHLORINATION OF 7-METHYLISATIN
The present disclosure relates to a process for chlorination of 7-methylisatin. The process of the present disclosure provides 5-chloro-7-methylisatin with a yield in the range of 80% to 95% and having a purity in the range of 90% to 98%. The process of the pre...
ABSTRACT
A PROCESS FOR THE PREPARATION OF PINOXADEN
The present disclosure relates to a process for the preparation of Pinoxaden. The process of the present disclosure is simple and environmental friendly. The process of the present disclosure provides Pinoxaden having a comparatively high purity and in high yield...
ABSTRACT
A PROCESS FOR THE PREPARATION OF 2-AMINO-5-CHLORO-N,3-
DIMETHYLBENZAMIDE
The present disclosure relates to the process for the preparation of 2-amino-5-
chloro-N,3-dimethylbenzamide. The process of the present disclosure is carried
out in the presence of a fluid medium that can be readily separated, re...
ABSTRACT
A PROCESS FOR THE PREPARATION OF OXYFLUORFEN
The present disclosure relates to a process for the preparation of Oxyfluorfen. The process of the present disclosure provides Oxyfluorfen with comparatively high yield and high purity. The process of the present disclosure is economic and efficient.
...
ABSTRACT
A PROCESS FOR THE SYNTHESIS OF PYRAZOLE-OXADIAZEPINE
The present disclosure relates to a process for the preparation of pyrazole-oxadiazepine. The process of the present disclosure reduces solvent use, uses inexpensive and easily available reagents. The process is simple, efficient, environment friendly, ...
ABSTRACT
A PROCESS FOR THE PREPARATION OF 2-NITRO-4-(METHYLSULFONYL)BENZOIC ACID
The present disclosure relates to a process for the preparation of 2-nitro-4-methylsulfonyl benzoic acid (NMSBA). The process comprises reacting 1-chloro-2-nitro-4-methyl sulfonyl benzene (chloro NMSB) with a compound of Formula II by...
The present disclosure relates to a polymer composite. The polymer composite of the present disclosure is lightweight, has good mechanical and thermal insulation properties. The present disclosure further relates to a simple and economical process for preparing the polymer composite.
ABSTRACT
A PROCESS FOR THE PREPARATION OF CHLORANTRANILIPROLE
The present disclosure relates to a process for the preparation of Chlorantraniliprole. The process of the present disclosure is carried by using a base that is non-toxic, inexpensive that can be readily separated, recovered, and recycled. The process i...
The present disclosure relates to a process for preparing Chlorantraniliprole. The process is simple, efficient and economical. The process of the present disclosure provides a comparatively higher yield of Chlorantraniliprole with greater purity.
ABSTRACT
A PROCESS FOR THE PREPARATION OF 2,3-DICHLORO-6-NITROANILINE
The present disclosure relates to a process for the preparation of 2,3-dichloro-6-nitroaniline. The process of the present disclosure includes nitrating, aminating the reactants to obtain a pure 2,3-dichloro-6-nitroaniline. The process condi...
ABSTRACT
A PROCESS FOR THE PREPARATION OF XANTHONE COMPOUNDS
The present disclosure relates to a process for the preparation of xanthone compounds. The process of the present disclosure is environment friendly, economic and efficient.
The present disclosure relates to a friction material composition comprising reactive poly aryl ether ketone (R-PAEK) as a binder. The present disclosure further relates to a process for the preparation of a friction material composition. Furthermore, the present disclosure relates to a process for the fabrication o...
ABSTRACT
A PROCESS FOR THE PREPARATION OF ETHIPROLE
The present disclosure relates to a process for the preparation of ethiprole. The process of the present disclosure avoids the use of ethyl mercaptan for the preparation of ethiprole. The reagents used in the present disclosure are safe, can be recovered, and rec...
ABSTRACT
PROCESS FOR THE PREPARATION OF DISULFIDE COMPOUNDS
The present disclosure relates to a process for the preparation of disulfide compounds. The process of the present disclosure provides disulfide compounds with comparatively better purity and better yield. The process of the present disclosure is simple a...
ABSTRACT
PROCESS FOR THE PURIFICATION OF CHLORANTRANILIPROLE
The present disclosure relates to a process for the purification of Chlorantraniliprole. The process comprises purifying the crude Chlorantraniliprole by using suitable fluid media to obtain a pure Chlorantraniliprole. The process of the present disclo...
ABSTRACT
A PROCESS FOR THE PREPARATION OF 2-AMINO-5-CHLORO-3-METHYLBENZOIC ACID
The present disclosure relates to the process for the preparation of 2-amino-5-chloro-3-methylbenzoic acid. The process of the present disclosure uses mild reaction conditions to provide 2-amino-5-chloro-3-methylbenzoic acid. The proce...
ABSTRACT
A PROCESS FOR THE PREPARATION OF PHENYLPYRAZOLE DERIVATIVES
The present disclosure relates to a process for the preparation of phenylpyrazole derivatives. The process of the present disclosure provides phenylpyrazole derivatives with a comparatively high purity and high yield. The process of the prese...
ABSTRACT
PROCESS AND APPARATUS FOR THE PURIFICATION OF POLYETHERKETONEKETONE
The present disclosure relates to a process and an apparatus for the purification of polyetherketoneketone (PEKK). The process comprises purifying the PEKK by using a solvent with continuous reflux to obtain the purified PEKK with enh...
ABSTRACT
A PROCESS FOR THE PREPARATION OF PYROXASULFONE
The present disclosure relates to a process for the preparation of pyroxasulfone. The process steps for the preparation of pyroxasulfone proceeds under mild reaction conditions. The reagents used in the present disclosure are safe, can be recovered, and r...
ABSTRACT
A PROCESS FOR THE PREPARATION OF 2-(2,2-DIFLUOROETHOXY)-6-(TRIFLUOROMETHYL)BENZENE SULFONYL CHLORIDE
The present disclosure relates to a process for the preparation of 2-(2,2-difluoroethoxy)-6-(trifluoromethyl)benzene sulfonyl chloride. The process of the present disclosure is simple, environment friend...
ABSTRACT
A PROCESS FOR THE PREPARATION OF HERBICIDE INTERMEDIATES
The present disclosure relates to a process for the preparation of herbicide intermediates. Particularly, the present disclosure relates to a process for the preparation of 1,2,3-trichlorobenzene. The process comprises chlorinating ortho nitro chlor...
ABSTRACT
A PROCESS FOR THE PREPARATION OF 4-(HALOMETHYL)-5 (DIFLUOROMETHOXY)-1-METHYL-3-(TRIFLUOROMETHYL)-1H-PYRAZOLE
The present disclosure relates to a process for the preparation of 4-(halomethyl)-5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazole compounds. The process of the present disclosure proce...
ABSTRACT
A PROCESS FOR THE PREPARATION OF CHLORANTRANILIPROLE
The present disclosure relates to a process for the preparation Chlorantraniliprole. The process of the present disclosure provides Chlorantraniliprole with high purity and in greater yields. Further, the process of the present disclosure is simple, eff...
ABSTRACT
A PROCESS FOR THE PREPARATION OF CHLORANTRANILIPROLE
The present disclosure relates to a process for the preparation Chlorantraniliprole. The process of the present disclosure provides a polymorph B of Chlorantraniliprole with high purity and in greater yields. Further, the process of the present disclosu...