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Powder Formulation For Waterproofing Membrane And A Process Of Preparing Thereof

Abstract: The present disclosure relates to a powder formulation for waterproofing membrane and a process of preparing thereof. The waterproofing membrane is a high performance, single component PMMA & acetate hybrid waterproofing system. It is spray applied in a sandwich structure between two layers of sprayed concrete/cast concrete layers creating a double bonded composite shell lining. It is an effective alternative to conventional waterproofing sheet membranes. As a double bonded system, this provides excellent water tightness, preventing the development of water migration on both sides of the membrane.

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Notices, Deadlines & Correspondence

Patent Information

Application #
Filing Date
05 June 2023
Publication Number
08/2024
Publication Type
INA
Invention Field
CIVIL
Status
Email
Parent Application

Applicants

Fibrex Construction Chemicals Pvt. Ltd.
Vill. Sarai Khatela, Gudrana Road, The. – Hodal, Palwal, Haryana – 121106

Inventors

1. Puneet Kakroo
Vill. Sarai Khatela, Gudrana Road, The. – Hodal, Palwal, Haryana – 121106
2. Sonika Kakroo
Vill. Sarai Khatela, Gudrana Road, The. – Hodal, Palwal, Haryana – 121106

Specification

DESC:FIELD OF THE INVENTION

The present disclosure relates to a powder formulation for waterproofing membrane and a process of preparing thereof.

BACKGROUND OF THE INVENTION

In the dynamic landscape of the construction industry, where structural integrity is paramount, the role of waterproofing cannot be overstated. It serves as a crucial element in prolonging the life of structures and shielding them from the deleterious effects of water-induced concrete and reinforced steel degradation. Recognizing the significance of this, Fibrex has undertaken an extensive research initiative to develop an innovative powder material that not only addresses the pervasive need for waterproofing but also boasts compatibility with a myriad of construction surfaces, both new and old.

The culmination of years of dedicated research efforts has resulted in Fibrex's groundbreaking powder material. This proprietary substance exhibits unparalleled waterproofing properties, presenting a versatile solution for a multitude of application areas within the construction industry. Whether it be sunken structures, basements, roofs, or water-retaining elements in buildings and concrete structures, Fibrex's powder material stands as a testament to advancements in construction waterproofing technology.

Within the realm of waterproofing methodologies, the invention draws attention to sheet-like waterproofing membrane laminates, a well-established approach for applications on concrete and various substrates. Typically comprising a carrier sheet and a pressure-sensitive adhesive layer, these laminates have found widespread use. In one application method, the waterproofing sheet material is applied to an already cured concrete surface, such as a building foundation, with the adhesive layer bonding to the concrete. Another technique involves affixing the waterproofing membrane to the concrete form or lagging, where the carrier sheet faces the lagging, and the adhesive portion is oriented towards the cavity where concrete will be poured. Referred to as "blind side" or pre-applied waterproofing, this process results in the adhesive portion adhering to the freshly poured concrete, creating a fully adhered waterproofing membrane on the cured concrete surface post-lagging removal.

Moreover, the versatility of Fibrex's powder material is evident in its application on horizontal surfaces. Whether applied to compacted soil, gravel, or a concrete slab, with the adhesive portion facing upward, this material offers a unique solution. Concrete can then be cast against the membrane, creating a comprehensive waterproofing system.

In one solution, a waterproofing membrane includes laminated layers: layer A comprising a waterproofing adhesive; layer B comprising a carrier sheet; layer C comprising a releasable bonding material; and layer D comprising a protective coating; wherein (i) the laminated layers are arranged in the sequential order A-B-C-D; or (ii) the laminated layers are arranged in the sequential order B-C-D-A; or (iii) the laminated layers are arranged in the sequential order C-D-A-B. The membrane does not include a removable release sheet that is typically used to prevent the adhesive from adhering to the carrier sheet or other portion of the membrane when the membrane is rolled up. Also disclosed is a method of making the aforementioned membrane. Preferably, layer C will comprise a water-soluble polymer, an alkali-soluble polymer, or a homopolymer or copolymer of polyvinyl acetate.

In another solution, a membrane comprising a barrier layer comprising a thermoplastic polymer component and a contact layer bonded to at least a portion of the barrier layer, the contact layer comprising a mixture of a solid filler component and a thermoplastic polymer component. The disclosure is also directed to a method for producing the membrane, a method for waterproofing a substrate, a waterproofed construction, a method for sealing a substrate against water penetration, and a sealed construction for sealing a substrate against water penetration.

In the view of the forgoing discussion, it is portrayed that in the prior arts, membranes become soft and easily mesh with a hand at low temperatures. Therefore, there is a need to develop a waterproofing membrane formulation with High crack bridging, High adhesion, and High water pressure resistance.

SUMMARY OF THE INVENTION

The present disclosure relates to a powder formulation for waterproofing membrane and a process of preparing thereof. The waterproofing membrane is a high-performance, single-component PMMA & acetate hybrid waterproofing system. It is spray applied in a sandwich structure between two layers of sprayed concrete/cast concrete layers creating a double bonded composite shell lining. It is an effective alternative to conventional waterproofing sheet membranes. As a double-bonded system, this provides excellent water tightness, preventing the development of water migration on both sides of the membrane. The invention further relates to a waterproofing material obtainable by adding water to such dry powder composition and a substrate coated with a FIBELASTIC PLT layer deposited from such waterproofing material.

In an embodiment, a dry powder composition for waterproofing membrane comprises 0.1% to 5% by weight of cement, 2% to 4% by weight of aluminous cement, 2% to 4% by weight of sulfate aluminate cement, 40% to 80% by weight of dispersible binder polymer particles, 0.01 to 0.5% by weight of cellulose ether, 0.5 to 1% by weight of chile saltpeter, 0.2 to 4% by weight of inorganic defoamer, 1.3 to 10% by weight of calcium carbonate, 1 to 5% by weight of oxide pigment, and 20% to 30% by weight of silica sand.

In another embodiment, a process of preparing powder formulation for waterproofing membrane includes collecting raw materials thereby stacking them in bags, the raw material comprises 0.1% to 5% by weight of cement.
The process further includes feeding of raw material to a pneumatic conveying system achieved by bag slitting machines, an electric hoist, and a bag massager system.
The process further includes weighing and adding ingredients including 40% to 80% by weight of dispersible binder polymer particles, 0.01 to 0.5% by weight of a cellulose ether, 0.5 to 1% by weight of a chile saltpeter, 0.2 to 4% by weight of an inorganic defoamer, 1.3 to 10% by weight of calcium carbonate, 1 to 5% by weight of an oxide pigment, and 20% to 30% by weight of silica sand.
The process further includes blending and mixing the raw material and ingredients using a blender/mixer received from the charge hoppers through a screw conveyor for formulating powder formulation for the waterproofing membrane.

The objective of the present invention is to provide waterproofing material that is cheap, reliable, easy to use, and suitable for almost all substrates like concrete, metals, boards, etc., and areas like sunken, roofs, basements, retaining structures, etc.

The present invention provides a waterproofing layer-like barrier to water penetration. One of the advantages of this product, it can withstand a negative temperature without losing its mechanical properties. This product is designed for high adhesion, which is generally missing in cost-effective waterproofing products. The same product can be used in negative and also positive sides.

To further clarify the advantages and features of the present disclosure, a more particular description of the invention will be rendered by reference to specific embodiments thereof, which are illustrated in the appended drawings. It is appreciated that these drawings depict only typical embodiments of the invention and are therefore not to be considered limiting of its scope. The invention will be described and explained with additional specificity and detail in the accompanying drawings.

BRIEF DESCRIPTION OF FIGURES

These and other features, aspects, and advantages of the present disclosure will become better understood when the following detailed description is read concerning the accompanying drawings in which like characters represent like parts throughout the drawings, wherein:

Figure 1 illustrates a flow chart of a process of preparing powder formulation for the waterproofing membrane of the present invention with respect to the existing invention;
Figure 2 illustrates Table 1 depicts a comparison data of the present invention with respect to the existing invention; and
Figure 3 illustrates Table 2 depicts a technical specifications of the present invention with respect to the existing invention.

Further, skilled artisans will appreciate that elements in the drawings are illustrated for simplicity and may not have necessarily been drawn to scale. For example, the flow charts illustrate the method in terms of the most prominent steps involved to help improve understanding of aspects of the present disclosure. Furthermore, in terms of the construction of the device, one or more components of the device may have been represented in the drawings by conventional symbols, and the drawings may show only those specific details that are pertinent to understanding the embodiments of the present disclosure so as not to obscure the drawings with details that will be readily apparent to those of ordinary skill in the art having the benefit of the description herein.

DETAILED DESCRIPTION:

To promote an understanding of the principles of the invention, reference will now be made to the embodiment illustrated in the drawings and specific language will be used to describe the same. It will nevertheless be understood that no limitation of the scope of the invention is thereby intended, such alterations and further modifications in the illustrated system, and such further applications of the principles of the invention as illustrated therein being contemplated as would normally occur to one skilled in the art to which the invention relates.

It will be understood by those skilled in the art that the foregoing general description and the following detailed description are exemplary and explanatory of the invention and are not intended to be restrictive thereof.

Reference throughout this specification to “an aspect”, “another aspect” or similar language means that a particular feature, structure, or characteristic described in connection with the embodiment is included in at least one embodiment of the present disclosure. Thus, appearances of the phrase “in an embodiment”, “in another embodiment” and similar language throughout this specification may, but do not necessarily, all refer to the same embodiment.

The terms "comprises", "comprising", or any other variations thereof, are intended to cover a non-exclusive inclusion, such that a process or method that comprises a list of steps does not include only those steps but may include other steps not expressly listed or inherent to such process or method. Similarly, one or more devices or sub-systems or elements or structures or components proceeded by "comprises...a" does not, without more constraints, preclude the existence of other devices or other sub-systems or other elements or other structures or other components or additional devices or additional sub-systems or additional elements or additional structures or additional components.

Unless otherwise defined, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The system, methods, and examples provided herein are illustrative only and not intended to be limiting.

Embodiments of the present disclosure will be described below in detail with reference to the accompanying drawings.

In an embodiment, a dry powder composition for waterproofing membrane comprises 0.1% to 5% by weight of cement, 2% to 4% by weight of aluminous cement, 2% to 4% by weight of sulfate aluminate cement, 40% to 80% by weight of dispersible binder polymer particles, 0.01 to 0.5% by weight of cellulose ether, 0.5 to 1% by weight of chile saltpeter, 0.2 to 4% by weight of inorganic defoamer, 1.3 to 10% by weight of calcium carbonate, 1 to 5% by weight of oxide pigment, and 20% to 30% by weight of silica sand.

Referring to Figure 1, a flow chart of a process of preparing powder formulation for a waterproofing membrane is disclosed in the present invention with respect to the existing invention. At step 102, process 100 includes collecting raw materials and thereby stacking in bags, the raw material comprises 0.1% to 5% by weight of cement.

At step 104, process 100 includes feeding of raw material to a pneumatic conveying system achieved by bag slitting machines, an electric hoist, and a bag massager system.

At step 106, process 100 includes weighing and adding ingredients including 40% to 80% by weight of dispersible binder polymer particles, 0.01 to 0.5% by weight of a cellulose ether, 0.5 to 1% by weight of a chile saltpeter, 0.2 to 4% by weight of an inorganic defoamer, 1.3 to 10% by weight of calcium carbonate, 1 to 5% by weight of an oxide pigment, and 20% to 30% by weight of silica sand.

At step 108, process 100 includes blending and mixing the raw material and ingredients using a blender/mixer received from the charge hoppers through a screw conveyor for formulating powder formulation for the waterproofing membrane.

In another embodiment, the bag slitting machines are employed for small bags of 25 kg, and an electric hoist & bag massager system is utilized for big bags of 50 kg.

In another embodiment, the quantity of raw material is decided, in which, the bulk quantity of raw material is transferred to storage silos, wherein the pneumatic conveying system transfers the material to silos.

In another embodiment, the ingredients weighing includes determining user-defined proportions of each ingredient based on a user-defined formula upon providing storage silos for housing the ingredients, wherein the ingredients are stored separately. Then, measuring ingredient quantities with a hopper with weighing cells below each storage silo. Then, metering the raw material from the storage silos to the respective weigh hoppers, ensuring a controlled and consistent flow upon implementing screw conveyors. Then, determining the quantity of the respective ingredient in accordance with the user-defined proportions by initiating the weighing process in each hopper. Then, conveying the measured material from the weighing hopper to a charge hopper through a conveying line. Thereafter, regulating the flow of material into the charge hopper by employing rotary airlock valves in the conveying line and ensuring that the material in the charge hopper is dosed accurately and consistently, based on the user-defined proportions of the ingredients employing the dosed material from the charge hopper.

In another embodiment, the blender mixing time ranges from 15 to 30 minutes for even mixing of the raw materials and ingredients.

In another embodiment, the cement is selected from a group consisting of Portland cement, aluminous cement, and sulfate aluminate cement.

In another embodiment, the process 100 further comprises verifying and optimizing the prepared formulation based on the physical and chemical properties of the formulation thereby packing and storing the prepared formulation, wherein the physical and chemical properties are selected from -5°c to +40°c of application temperature, >2.5 MPa Adhesion/Bond strength to concrete and >265 % Elongation.

In another embodiment, the prepared formulation is optimized by measuring the user-defined raw materials and ingredients using a controller through a programmable logic circuit (PLC) panel.

Figure 2 illustrates Table 1 depicts a comparison data of the present invention with respect to the existing invention.

The present invention relates to a dry powder composition comprising 0.1% to 5% by weight of cement, wherein the cement is one selected from the group consisting of Portland cement; 2% to 4% by weight of aluminous cement, and sulfate aluminate cement; 40% to 80% by weight of dispersible binder polymer particles; 0.01 to 0.5% by weight of a cellulose ether; 0.5 to 1% by weight of a chile saltpeter, 0.2 to 4% by weight of an inorganic defoamer, 1.3 to 10% by weight of a calcium carbonate, 1 to 5% by weight of an oxide pigment,20% to 30% by weight of a silica sand, wherein all percentages by weight are based on the total weight of the composition. The invention further relates to a waterproofing material obtainable by adding water to such dry powder composition and a substrate coated with a layer deposited from such waterproofing material.

Manufacturing Process:
The major ingredients of the membrane are vinyl acetate base polymer powder & minerals fillers in fixed quantities along with other minor ingredients.
The manufacturing process can be done in 5 steps
1. Taking raw materials from storage
2. Weighing of the ingredients
3. Conveying raw material to charge hoppers
4. Blending & mixing
5. Testing Correction, packing and storage
1. Taking of raw materials from storage: Raw materials stacked in small bags of 25 kg & 50 kg after tested ok. Unloading of these bags and feeding of raw material to the conveying system shall be achieved by bag slitting machines for small bags and with an electric hoist & bag massager system in case of big bags. Depending upon the finished product, the quantity of raw material can be decided. First, the bulk quantity of raw material is transferred to storage silos. For transferring the material to silos, a pneumatic conveying system is preferred as it is economical and robust, both in operation as well as maintenance.
2. Weighing of the ingredients: The ingredients should be added in exact proportions (determined by formula) to ensure producing premium quality. Therefore, a hopper with weighing cells must be located below the storage silos. Metering of the raw material from the silo to weigh hopper should be performed by screw conveyors. After getting the right quantity of material in the weighing hopper, it will be dosed to charge the hopper by conveying line via rotary airlock valves.
3. Conveying of raw material to charge hoppers: The raw material must now be conveyed to charge hoppers as per requirement. The selection of charge hoppers is done with the help of diverters in the conveying line. Conveying capacity is decided by the blender batch cycle time. Based on capacity requirement & distance, conveying air is calculated & a blower is selected.
4. Blending & mixing: After the material is charged in a charge hopper, it gets dosed in a blender/mixer with the help of a screw conveyor. The average blender mixing time is between 15-30 minutes.
5. Testing Correction & Packing: After mixing a small quantity is checked in the lab and if any correction needs the lab in-charge corrects it and then the material is transferred to the packing machine where it is duly packed. The final product is then moved to the finished goods storage area. All the system operations can be controlled through a PLC panel. Using PLC programming, the system measures the accuracy of various raw materials mixed in the ingredients, thus delivering superior quality. Consequently, it also reduces labor intensity in addition to environmental pollution.
The product has a high quantity of very flexible copolymer of vinyl acetate and ethylene that provides the properties of adhesion and flexibility at a wide range of temperatures. Redispersible polymer powders are polymer emulsions that have been converted by a series of processes such as high temperatures and pressures, spray drying, and surface treatment to powdered thermoplastic resin materials. When mixed with water, these powdered organic binders can redisperse in water back into new emulsions with essentially identical properties to the original copolymer emulsions.
Redispersible Polymer powder (ordinary type) is composed of special polymers made of powder adhesive after spray drying. This powder is in contact with water and can be dispersed again soon after forming an emulsion, and with nature the same as the initial emulsion, namely the film can be formed after moisture evaporation, the film has high flexibility, high resistance to weathering, and on various substrate with high caking property. It can improve the performance of the waterproofing membrane, raise the bonding strength of the waterproofing membrane with the different substrate materials, and improve flexibility. Feature: Redispersible Polymer powder is the main raw material in the production of Waterproofing membranes.
Redispersible Polymer powder has obvious functions in the dry-mixed waterproofing membrane. It can improve strength and bonding force, the elastic bending strength. It also improves the freeze-proof property, weathering resistance, durability, and wear resistance of the materials. As well as intensify the hydrophobicity and reduce the water absorption, improve the construction characteristics. The powder can efficiently prevent water penetration.

1. Improvement of the bonding strength and bonding force: It is quite necessary to add Redispersible Polymer powder to the products of waterproof powder material. It can improve the bonding strength and bonding force of materials. Furthermore, due to the fine bonding force of polymer resin, the powder has better effects on improving the bonding force of the waterproofing membrane to the basis materials.
2. Improvement of the tensile property: Redispersible Polymer powder increases the tensile property due to its interbonding properties.
3. Improvement of the hydrophobicity and reduction of the water absorption: The addition of the Redispersible Polymer powder can improve the microscopic structure of the waterproofing membrane. The polymer forms the irreversible network during the curing process.
4. Improvement of the freeze-thawing stability and efficient prevention of the cracking of materials: The plasticity function possessed by the thermoplastic resin of Redispersible Polymer powder can overcome the flatulence damage for waterproofing materials brought by temperature difference changes.
The waterproofing membrane base of a copolymer of vinyl acetate and ethylene provides the properties of adhesion and flexibility at a wide range of temperatures. When mixed with water, these powdered organic binders can redisperse in water back into new emulsions with essentially identical properties to the original copolymer emulsions. After application, it became a waterproofing material, which resists the penetration of water.
AREAS OF APPLICATION:
• Particularly well suited for underground structures with complex profiles and geometry
• Sprayed concrete tunnel and shaft linings
• Underground Basements
• Water Retaining structures
• Negative waterproofing
ADVANTAGE
• Fast and Easy Application
• Non Toxic
• Excellent Adhesion to concrete
• Double bonded system enhances the waterproofing performance
• Tough and flexible for use with steel fibre-sprayed concrete
• No special transportation classifications
• Can be applied to 24-hour cured concrete also
• Non Ignitable
• Excellent crack-bridging ability
MIXING:
Powder: Water
Waterproofing Membrane: 38% to 40% by weight of powder.
Add water first into the bucket & scale while stirring add powder till the mix is smooth & consistent.
PRIMING: Waterproofing Membrane Powder does not normally require primer. However, high absorbent surfaces such as porous Concrete, sand/cement, and cement boards will require sealing to prevent absorption of Primer.
APPLYING AND LAYING: The material should be applied to the prepared surface using a spray, roller, or brush. Ensure material is spread evenly. Do not re-roll later. The work area should be protected during the installation process and during the initial curing time to ensure that no airborne debris can contaminate it.

PACKAGING: Waterproofing Membrane is available in 15 kg Plastic Bags.
PRECAUTIONS: During mixing and application the following precautions should be observed: ensure adequate ventilation and avoid contact of the material with the eyes, nasal passages, mouth, and unprotected skin. Avoid contact with the hands by wearing protective gloves and, if necessary, a suitable barrier cream. In case of contact with the eyes, rinse immediately with plenty of water and seek medical advice and after contact with the skin wash immediately with plenty of soap and water (do not use solvents). Prolonged contact with the skin should be avoided Always wear gloves and eye/face protection as necessary. Observe personal hygiene, particularly washing hands after work has been completed or at any interruption whilst work is in progress. Care should be taken when removing gloves to avoid contaminating the insides. In case of accidents seek medical advice.

Figure 3 illustrates Table 2 depicts a technical specifications of the present invention with respect to the existing invention.

Fibelastic PLT
Fibelastic PLT stands as a high-performance, single-component waterproofing system, blending PMMA (Polymethyl Methacrylate) and acetate in a hybrid formulation. Applied through a spray technique, it forms a sandwich structure between two layers of either sprayed or cast concrete. This unique application creates a double-bonded composite shell lining, serving as a highly effective alternative to traditional waterproofing sheet membranes. The dual-bonded nature of the system ensures outstanding water tightness, preventing water migration on both sides of the membrane.

Areas of Application:

Underground Structures: Particularly well-suited for structures with complex profiles and geometry.
Sprayed Concrete Tunnel and Shaft Linings: Ideal for ensuring waterproofing integrity in tunnel and shaft constructions.
Underground Basements: A reliable solution for waterproofing basements to protect against water ingress.
Water Retaining Structures: Applicable to structures requiring water retention, providing a robust barrier against water infiltration.
Negative Waterproofing: Suitable for scenarios where preventing water ingress from the exterior is crucial.
Advantages:

Fast and Easy Application: Streamlined application process for efficiency.
Non-toxic: Complies with safety standards, posing no harm to health.
Excellent Adhesion to Concrete: Ensures a strong bond with concrete surfaces.
Double Bonded System Enhances Waterproofing Performance: Provides a robust defense against water infiltration.
Tough and Flexible for Use with Steel Fiber Sprayed Concrete: Adaptable to various construction scenarios.
No Special Transportation Classifications: Simplifies logistical considerations.
Can Be Applied to 24 Hours Cured Concrete: Allows for a flexible application timeline.
Non-Ignitable: Poses no risk of ignition during application.
Excellent Crack Bridging Ability: Resilient against structural movement.

Application Methodology:

Surface Preparation:

Ensure the surface is free from any contaminants that could affect adhesion.
The surface should be surface-saturated and dry before coating.
Smoothing layers may be applied to rough surfaces to enhance coating uniformity.
Address any active water ingress before application, using suitable materials.
For active water ingress areas, Fibelastic PLT fleece can be applied to facilitate drainage before coating.
The application can be done in two layers for optimal coating.
Mixing:

A specific ratio of Fibelastic PLT to water should be maintained for proper consistency.
Priming:

Fibelastic PLT typically does not require a primer, but absorbent surfaces may benefit from sealing with Fibfloor Cem Primer or Eversil Primer.
Applying and Laying:

Use spray, roller, or brush for application.
Ensure even spread and avoid re-rolling.
Protect the work area during installation to prevent contamination.
Clean-Up:

Tools should be cleaned immediately with water to prevent material hardening.
Packaging:
Fibelastic PLT is available in 15 kg plastic bags.

Storage:
The product has a shelf life of 12 months when stored properly in original, unopened bags between +5°C to +40°C in dry areas.

Precautions:

Follow safety precautions during mixing and application, including adequate ventilation and protective gear.
Attend to any accidents promptly and seek medical advice if necessary.
Disposal/Spillage:
Spillage should be absorbed onto sand or inert material and transferred to a suitable disposable vessel. Disposal should comply with local waste disposal regulations.

Note: Fibseal PLT is formerly known as Fibelastic PLT. The information provided is based on extensive experience and may be subject to updates. The company assumes no liability for conditions beyond its control.

Health and Safety:
Intended for use by trained professionals with proper equipment, following recommended safety measures such as wearing protective gear and avoiding skin contact.

The drawings and the forgoing description give examples of embodiments. Those skilled in the art will appreciate that one or more of the described elements may well be combined into a single functional element. Alternatively, certain elements may be split into multiple functional elements. Elements from one embodiment may be added to another embodiment. For example, orders of processes described herein may be changed and are not limited to the manner described herein. Moreover, the actions of any flow diagram need not be implemented in the order shown; nor do all of the acts necessarily need to be performed. Also, those acts that are not dependent on other acts may be performed in parallel with the other acts. The scope of embodiments is by no means limited by these specific examples. Numerous variations, whether explicitly given in the specification or not, such as differences in structure, dimension, and use of material, are possible. The scope of embodiments is at least as broad as given by the following claims.

Benefits, other advantages, and solutions to problems have been described above about specific embodiments. However, the benefits, advantages, solutions to problems, and any component(s) that may cause any benefit, advantage, or solution to occur or become more pronounced are not to be construed as a critical, required, or essential feature or component of any or all the claims. ,CLAIMS:1. A dry powder composition for waterproofing membrane comprises:
0.1% to 5% by weight of cement;
2% to 4% by weight of aluminous cement;
2% to 4% by weight of sulfate aluminate cement;
40% to 80% by weight of dispersible binder polymer particles;
0.01 to 0.5% by weight of cellulose ether;
0.5 to 1% by weight of chile saltpeter;
0.2 to 4% by weight of inorganic defoamer;
1.3 to 10% by weight of calcium carbonate;
1 to 5% by weight of oxide pigment; and
20% to 30% by weight of silica sand.

2. A process of preparing powder formulation for waterproofing membrane, the process comprises:
collecting raw materials thereby stacking in bags, the raw material comprises 0.1% to 5% by weight of cement;
feeding of raw material to a pneumatic conveying system achieved by bag slitting machines, an electric hoist and a bag massager system;
weighing and adding ingredients including 40% to 80% by weight of dispersible binder polymer particles, 0.01 to 0.5% by weight of a cellulose ether, 0.5 to 1% by weight of a chile saltpeter, 0.2 to 4% by weight of an inorganic defoamer, 1.3 to 10% by weight of calcium carbonate, 1 to 5% by weight of an oxide pigment, and 20% to 30% by weight of silica sand; and
blending and mixing the raw material and ingredients using a blender/mixer received from the charge hoppers through a screw conveyor for formulating powder formulation for the waterproofing membrane.

3. The process as claimed in claim 2, wherein the bag slitting machines are employed for small bags of 25 kg and an electric hoist & bag massager system is utilized for big bags of 50 kg.

4. The process as claimed in claim 2, wherein the quantity of raw material is decided, in which, the bulk quantity of raw material is transferred to storage silos, wherein the pneumatic conveying system transfers the material to silos.

5. The process as claimed in claim 2, wherein the ingredients weighing comprises:
determining user-defined proportions of each ingredient based on a user-defined formula upon providing storage silos for housing the ingredients, wherein the ingredients are stored separately;
measuring ingredient quantities by a hopper with weighing cells below each storage silo;
metering the raw material from the storage silos to the respective weigh hoppers, ensuring a controlled and consistent flow upon implementing screw conveyors; and
determining the quantity of the respective ingredient in accordance with the user-defined proportions by initiating the weighing process in each hopper.

6. The process as claimed in claim 5, further comprises:
conveying the measured material from the weighing hopper to a charge hopper through a conveying line; and
regulating the flow of material into the charge hopper by employing rotary airlock valves in the conveying line and ensuring that the material in the charge hopper is dosed accurately and consistently, based on the user-defined proportions of the ingredients employing the dosed material from the charge hopper.

7. The process as claimed in claim 2, wherein the blender mixing time ranges from 15 to 30 minutes for even mixing of the raw materials and ingredients.

8. The process as claimed in claim 2, wherein the cement is selected from a group consisting of Portland cement, aluminous cement, and sulfate aluminate cement.

9. The process as claimed in claim 2, further comprises verifying and optimizing the prepared formulation based on physical and chemical properties of the formulation thereby packing and storing the prepared formulation, wherein the physical and chemical properties are selected from -5°c to +40°c of application temperature, >2.5 MPa Adhesion/Bond strength to concrete and >265 % Elongation.

10. The process as claimed in claim 9, wherein the prepared formulation is optimized by measuring the user-defined raw materials and ingredients using a controller through a programmable logic circuit (PLC) panel.

Documents

Application Documents

# Name Date
1 202311038378-STATEMENT OF UNDERTAKING (FORM 3) [05-06-2023(online)].pdf 2023-06-05
2 202311038378-PROVISIONAL SPECIFICATION [05-06-2023(online)].pdf 2023-06-05
3 202311038378-FORM FOR SMALL ENTITY(FORM-28) [05-06-2023(online)].pdf 2023-06-05
4 202311038378-FORM FOR SMALL ENTITY [05-06-2023(online)].pdf 2023-06-05
5 202311038378-FORM 1 [05-06-2023(online)].pdf 2023-06-05
6 202311038378-FIGURE OF ABSTRACT [05-06-2023(online)].pdf 2023-06-05
7 202311038378-EVIDENCE FOR REGISTRATION UNDER SSI(FORM-28) [05-06-2023(online)].pdf 2023-06-05
8 202311038378-EVIDENCE FOR REGISTRATION UNDER SSI [05-06-2023(online)].pdf 2023-06-05
9 202311038378-DRAWINGS [05-06-2023(online)].pdf 2023-06-05
10 202311038378-DECLARATION OF INVENTORSHIP (FORM 5) [05-06-2023(online)].pdf 2023-06-05
11 202311038378-Proof of Right [19-06-2023(online)].pdf 2023-06-19
12 202311038378-FORM-26 [19-06-2023(online)].pdf 2023-06-19
13 202311038378-FORM-9 [24-11-2023(online)].pdf 2023-11-24
14 202311038378-FORM-26 [24-11-2023(online)].pdf 2023-11-24
15 202311038378-DRAWING [24-11-2023(online)].pdf 2023-11-24
16 202311038378-CORRESPONDENCE-OTHERS [24-11-2023(online)].pdf 2023-11-24
17 202311038378-COMPLETE SPECIFICATION [24-11-2023(online)].pdf 2023-11-24
18 202311038378-MSME CERTIFICATE [29-11-2023(online)].pdf 2023-11-29
19 202311038378-FORM28 [29-11-2023(online)].pdf 2023-11-29
20 202311038378-FORM 18A [29-11-2023(online)].pdf 2023-11-29
21 202311038378-FORM-8 [03-02-2025(online)].pdf 2025-02-03
22 202311038378-FER.pdf 2025-08-07

Search Strategy

1 202311038378_SearchStrategyNew_E_SearchreportE_04-08-2025.pdf