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Method For Enhancing Bond Strength Of Engineered Cementitious Composites Under Freeze Thaw Cycles Using Ggbs And Nano Silica As Partial Cement Replacement

Abstract: ABSTRACT METHOD FOR ENHANCING BOND STRENGTH OF ENGINEERED CEMENTITIOUS COMPOSITES UNDER FREEZE-THAW CYCLES USING GGBS AND NANO SILICA AS PARTIAL CEMENT REPLACEMENT This study investigates the effects of freeze-thaw cycles on the bond strength and durability of Engineered Cementitious Composites (ECC) incorporating Ground Granulated Blast Furnace Slag (GGBS) and Nano-Silica as partial cement replacements. Aimed at enhancing structural performance in cold climates, the research explores optimized ECC mix designs using various GGBS/cement ratios and hybrid fiber reinforcements (Steel and Polyvinyl Alcohol fibers) to improve ductility and crack resistance. Mechanical behavior is assessed through tests on 150 × 150 mm cubes and 100 × 200 mm cylinders for compressive, split tensile, and shear bond strength. Additionally, 750 × 150 × 150 mm beam specimens are evaluated for flexural performance under freeze-thaw exposure. Three beam configurations are tested: fully ECC, fully Self-Compacting Concrete (SCC), and hybrid ECC-SCC layers. Freeze-thaw cycling is applied to analyze durability, crack propagation, and interfacial bond integrity. Results reveal how GGBS and Nano-Silica enhance the microstructure, improve freeze-thaw resistance, and strengthen ECC and ECC-SCC hybrid systems. An ANSYS-based finite element model (FEM) validates the experimental findings, confirming the reliability of the proposed mix designs for durable concrete infrastructure. This research contributes to the development of sustainable, high-performance cementitious materials with superior environmental resistance.

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Notices, Deadlines & Correspondence

Patent Information

Application #
Filing Date
24 May 2025
Publication Number
22/2025
Publication Type
INA
Invention Field
CHEMICAL
Status
Email
Parent Application

Applicants

SR UNIVERSITY
ANANTHSAGAR, HASANPARTHY (M), WARANGAL URBAN, TELANGANA - 506371, INDIA

Inventors

1. DR. DURGAM RAJABABU
SR UNIVERSITY, ANANTHSAGAR, HASANPARTHY (M), WARANGAL URBAN, TELANGANA - 506371, INDIA
2. N. HARSHITHA
SR UNIVERSITY, ANANTHSAGAR, HASANPARTHY (M), WARANGAL URBAN, TELANGANA - 506371, INDIA
3. M. SUSMITHA
SR UNIVERSITY, ANANTHSAGAR, HASANPARTHY (M), WARANGAL URBAN, TELANGANA - 506371, INDIA
4. M. HARSHIKA
SR UNIVERSITY, ANANTHSAGAR, HASANPARTHY (M), WARANGAL URBAN, TELANGANA - 506371, INDIA

Specification

Description:FIELD OF THE INVENTION
This invention relates to Method for Enhancing Bond Strength of Engineered Cementitious Composites Under Freeze-Thaw Cycles Using GGBS and Nano silica as Partial Cement Replacement
BACKGROUND OF THE INVENTION
The durability of concrete structures in cold climates is significantly impacted by freeze-thaw cycles, which cause deterioration, reduce bond strength, and compromise structural integrity. Engineered Cementitious Composites (ECC), known for their superior ductility and crack resistance, are promising materials for enhancing concrete durability. However, their performance under freeze-thaw exposure, especially in hybrid applications with Self-Compacting Concrete (SCC), remains a critical area of study. This research investigates the bond strength of ECC incorporating Ground Granulated Blast Furnace Slag (GGBS) and Nano-Silica as partial cement replacements, subjected to repeated freeze-thaw cycles. The study examines different layered configurations of ECC and SCC, analyzing their mechanical and structural performance. The inclusion of GGBS improves long-term strength by refining the pore structure, while Nano-Silica enhances the interfacial transition zone (ITZ), improving bond durability. By testing cube, cylindrical, and beam specimens under freeze-thaw conditions, this study aims to optimize material design for sustainable infrastructure in extreme weather conditions. The findings will contribute to developing hybrid concrete systems with improved freeze-thaw resistance, ensuring longevity and structural efficiency in modern construction applications.
The primary objective of this research is to evaluate the impact of freeze-thaw cycles on the bond strength of Engineered Cementitious Composites (ECC) incorporating Ground Granulated Blast Furnace Slag (GGBS) and Nano-Silica as partial cement replacements. The study aims to develop an optimized ECC mix and assess its mechanical and structural performance when combined with Self-Compacting Concrete (SCC) in various layered configurations. The research objectives are outlined as follows:
1. To develop a novel ECC mix using GGBS/Cement ratio and Nano-Silica as cementitious material, and Hybrid Fibre (Steel Fibre + Polyvinyl Alcohol (PVA) Fibre combination): The study aims to enhance the mechanical properties and durability of ECC by partially replacing cement with GGBS and Nano-Silica. GGBS helps in refining the pore structure, improving long-term strength, and reducing permeability, while Nano-Silica enhances the interfacial transition zone (ITZ), leading to improved bond strength. The incorporation of hybrid fibers (a combination of steel fibers and PVA fibers) aims to improve the tensile strength, ductility, and crack resistance of ECC, making it more resilient under freeze-thaw exposure.
2. To investigate the mechanical properties of the proposed bendable concrete and evaluate the ductility enhancement characteristics: ECC is known for its strain-hardening behavior and superior ductility compared to conventional concrete. This research investigates its mechanical properties, such as compressive strength, split tensile strength, flexural strength, and shear bond strength, particularly under the effects of cyclic freezing and thawing. The study aims to quantify how GGBS, Nano-Silica, and hybrid fibers contribute to enhancing the bending capacity and deformation characteristics of ECC, making it a promising material for cold climate applications.
3. To investigate the structural performance of RCC beams using ECC under simply supported and two-point load conditions: The study includes experimental testing of reinforced concrete (RCC) beams incorporating ECC, SCC, and hybrid ECC-SCC layers under simply supported conditions with two-point loading. The research evaluates the load-bearing capacity, flexural behavior, and failure mechanisms of these beams under freeze-thaw cycles. By comparing fully ECC beams, fully SCC beams, and hybrid ECC-SCC beams, the study aims to determine the bond integrity between ECC and SCC, ensuring that the combination provides structural efficiency without premature bond failure.
4. To intend the validity of the investigation results with an ANSYS-based analytical model: The experimental findings will be validated using an ANSYS-based finite element model (FEM) to simulate the mechanical and structural behavior of ECC and ECC-SCC composite systems under freeze-thaw conditions. The analytical model will provide further insights into stress distribution, crack propagation, and bond strength degradation, ensuring the reliability and applicability of the experimental results in real-world structural applications.
SUMMARY OF THE INVENTION
This summary is provided to introduce a selection of concepts, in a simplified format, that are further described in the detailed description of the invention.
This summary is neither intended to identify key or essential inventive concepts of the invention and nor is it intended for determining the scope of the invention.
To further clarify advantages and features of the present invention, a more particular description of the invention will be rendered by reference to specific embodiments thereof, which is illustrated in the appended drawings. It is appreciated that these drawings depict only typical embodiments of the invention and are therefore not to be considered limiting of its scope. The invention will be described and explained with additional specificity and detail with the accompanying drawings.
This study evaluates the impact of freeze-thaw cycles on the bond strength of ECC incorporating GGBS and Nano-Silica, optimizing durability and structural performance in hybrid concrete systems.
BRIEF DESCRIPTION OF THE DRAWINGS
The illustrated embodiments of the subject matter will be understood by reference to the drawings, wherein like parts are designated by like numerals throughout. The following description is intended only by way of example, and simply illustrates certain selected embodiments of devices, systems, and methods that are consistent with the subject matter as claimed herein, wherein:
Fig 1: Curing of cubes and cylinder in freezer and oven failure specimen’s cubes and cylinders under UTM machine and failure patterns
Fig 2: Beam Specimens casting and testing
The figures depict embodiments of the present subject matter for the purposes of illustration only. A person skilled in the art will easily recognize from the following description that alternative embodiments of the structures and methods illustrated herein may be employed without departing from the principles of the disclosure described herein.
DETAILED DESCRIPTION OF THE INVENTION
The detailed description of various exemplary embodiments of the disclosure is described herein with reference to the accompanying drawings. It should be noted that the embodiments are described herein in such details as to clearly communicate the disclosure. However, the amount of details provided herein is not intended to limit the anticipated variations of embodiments; on the contrary, the intention is to cover all modifications, equivalents, and alternatives falling within the scope of the present disclosure as defined by the appended claims.
It is also to be understood that various arrangements may be devised that, although not explicitly described or shown herein, embody the principles of the present disclosure. Moreover, all statements herein reciting principles, aspects, and embodiments of the present disclosure, as well as specific examples, are intended to encompass equivalents thereof.
The terminology used herein is for the purpose of describing particular embodiments only and is not intended to be limiting of example embodiments. As used herein, the singular forms “a",” “an” and “the” are intended to include the plural forms as well, unless the context clearly indicates otherwise. It will be further understood that the terms “comprises,” “comprising,” “includes” and/or “including,” when used herein, specify the presence of stated features, integers, steps, operations, elements and/or components, but do not preclude the presence or addition of one or more other features, integers, steps, operations, elements, components and/or groups thereof.
It should also be noted that in some alternative implementations, the functions/acts noted may occur out of the order noted in the figures. For example, two figures shown in succession may, in fact, be executed concurrently or may sometimes be executed in the reverse order, depending upon the functionality/acts involved.
In addition, the descriptions of "first", "second", “third”, and the like in the present invention are used for the purpose of description only, and are not to be construed as indicating or implying their relative importance or implicitly indicating the number of technical features indicated. Thus, features defining "first" and "second" may include at least one of the features, either explicitly or implicitly.
Unless otherwise defined, all terms (including technical and scientific terms) used herein have the same meaning as commonly understood by one of ordinary skill in the art to which example embodiments belong. It will be further understood that terms, e.g., those defined in commonly used dictionaries, should be interpreted as having a meaning that is consistent with their meaning in the context of the relevant art and will not be interpreted in an idealized or overly formal sense unless expressly so defined herein.
This study investigates the impact of freeze-thaw cycles on the bond strength of Engineered Cementitious Composites (ECC) incorporating Ground Granulated Blast Furnace Slag (GGBS) and Nano-Silica as partial cement replacements. The research aims to enhance the durability and structural performance of ECC by optimizing its mix design with a GGBS/cement ratio and the inclusion of hybrid fibers (Steel and Polyvinyl Alcohol (PVA) fibers) to improve ductility and crack resistance. To assess the mechanical and structural behavior of these materials, different specimen types are prepared, including 150 × 150 mm cube specimens and 100 × 200 mm cylindrical specimens for evaluating compressive, split tensile, and shear bond strength. Additionally, 750 × 150 × 150 mm beam specimens are tested to analyze flexural performance under freeze-thaw conditions. The study evaluates three beam configurations: fully ECC beams, fully SCC beams, and hybrid beams with ECC forming one layer and Self-Compacting Concrete (SCC) forming the other. Freeze-thaw cycling is conducted to assess the durability, crack propagation, and interfacial bond integrity between ECC and SCC. The findings provide insights into how GGBS and Nano-Silica influence the microstructure, enhance freeze-thaw resistance, and improve the bond strength of ECC and hybrid ECC-SCC systems. Furthermore, an ANSYS-based finite element model (FEM) is developed to validate the experimental results, ensuring the reliability and applicability of the study’s outcomes for designing durable concrete structures in cold climates. This research contributes to the advancement of sustainable, high-performance cementitious materials with superior resistance to environmental degradation.This study evaluates the impact of freeze-thaw cycles on the bond strength of ECC incorporating GGBS and Nano-Silica, optimizing durability and structural performance in hybrid concrete systems.
Methodology:
The study involves preparing ECC, SCC, and hybrid ECC-SCC specimens, subjecting them to freeze-thaw cycles, and evaluating their mechanical properties through compression, shear bond, split bond, and flexural strength tests. An ANSYS-based finite element model (FEM) is used to validate experimental results and analyze stress distribution and bond strength degradation.
1. The study examines the effect of freeze-thaw cycles on the bond strength of Engineered Cementitious Composites (ECC) incorporating Ground Granulated Blast Furnace Slag (GGBS) and Nano-Silica as partial cement replacements.
2. Different specimen configurations, including ECC, Self-Compacting Concrete (SCC), and hybrid ECC-SCC layered beams, are tested to evaluate their mechanical and structural performance under cyclic freezing and thawing.
3. GGBS enhances durability by refining the pore structure and reducing permeability, while Nano-Silica improves the interfacial transition zone (ITZ), strengthening the bond between cementitious materials.
4. Experimental tests, including compression, split bond, shear bond, and flexural strength evaluations, are conducted on cube, cylindrical and beam specimens to analyze material behavior under freeze-thaw exposure.
5. The study assesses the interface bond between ECC and SCC in hybrid specimens, ensuring structural stability and durability in extreme weather conditions.
6. An ANSYS-based finite element model (FEM) is developed to validate the experimental results, providing predictive analysis of stress distribution, crack propagation, and bond strength degradation.
7. The findings contribute to the development of hybrid concrete systems with enhanced freeze-thaw resistance, ensuring sustainable and long-lasting infrastructure in cold climates.
NOVELTY:
This research introduces a novel approach by integrating GGBS and Nano-Silica in ECC to enhance freeze-thaw durability, while also evaluating the bond strength of hybrid ECC-SCC systems, a rarely explored area in extreme weather conditions.
ADVANTAGES OF THE INVENTION
The proposed solution improves upon previous methods by incorporating Ground Granulated Blast Furnace Slag (GGBS) and Nano-Silica as partial cement replacements in Engineered Cementitious Composites (ECC), significantly enhancing durability under freeze-thaw conditions. Unlike conventional ECC or Self-Compacting Concrete (SCC) approaches, this study evaluates hybrid ECC-SCC configurations, offering insights into bond strength and interface performance. The use of hybrid fibers (Steel and Polyvinyl Alcohol) further increases ductility, crack resistance, and ultimate strain capacity, addressing structural degradation issues common in cold climates. Additionally, an ANSYS-based finite element model (FEM) validates the experimental findings, ensuring a more reliable predictive analysis for long-term infrastructure performance.

, Claims:1. A method for Enhancing Bond Strength of Engineered Cementitious Composites Under Freeze-Thaw, comprising: Ground Granulated Blast Furnace Slag (GGBS) and Nano-Silica.
2. The method as claimed as claim 1, wherein the method explores optimized ECC mix designs using various GGBS/cement ratios and hybrid fiber reinforcements (Steel and Polyvinyl Alcohol fibers) to improve ductility and crack resistance.
3. The method as claimed as claim 1, wherein the Freeze-thaw cycling is applied to analyze durability, crack propagation, and interfacial bond integrity.
4. The method as claimed as claim 1, wherein the incorporation of GGBS and Nano-Silica refines the ECC microstructure, significantly enhances freeze-thaw resistance, and improves the overall mechanical and durability performance of both ECC and ECC-SCC hybrid systems.

Documents

Application Documents

# Name Date
1 202541050028-STATEMENT OF UNDERTAKING (FORM 3) [24-05-2025(online)].pdf 2025-05-24
2 202541050028-REQUEST FOR EARLY PUBLICATION(FORM-9) [24-05-2025(online)].pdf 2025-05-24
3 202541050028-POWER OF AUTHORITY [24-05-2025(online)].pdf 2025-05-24
4 202541050028-FORM-9 [24-05-2025(online)].pdf 2025-05-24
5 202541050028-FORM FOR SMALL ENTITY(FORM-28) [24-05-2025(online)].pdf 2025-05-24
6 202541050028-FORM 1 [24-05-2025(online)].pdf 2025-05-24
7 202541050028-EVIDENCE FOR REGISTRATION UNDER SSI(FORM-28) [24-05-2025(online)].pdf 2025-05-24
8 202541050028-EVIDENCE FOR REGISTRATION UNDER SSI [24-05-2025(online)].pdf 2025-05-24
9 202541050028-EDUCATIONAL INSTITUTION(S) [24-05-2025(online)].pdf 2025-05-24
10 202541050028-DRAWINGS [24-05-2025(online)].pdf 2025-05-24
11 202541050028-DECLARATION OF INVENTORSHIP (FORM 5) [24-05-2025(online)].pdf 2025-05-24
12 202541050028-COMPLETE SPECIFICATION [24-05-2025(online)].pdf 2025-05-24