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A Formulation For Enhancing Lubricity Of Fuels

Abstract: The present disclosure relates to a formulation of diesel additive comprising 2-ethylhexanoic acid, at least one alkylene glycol and at least one alkanolamine which at specific weight ratios, is able to enhance the lubricity of a fuel. Also provided are the methods of preparation and usage of the same. It further relates to the fuel composition comprising the fuel, and the formulation of present disclosure, and the method of preparing the fuel composition.

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Notices, Deadlines & Correspondence

Patent Information

Application #
Filing Date
02 June 2017
Publication Number
49/2018
Publication Type
INA
Invention Field
CHEMICAL
Status
Email
iprdel@lakshmisri.com
Parent Application
Patent Number
Legal Status
Grant Date
2020-12-31
Renewal Date

Applicants

HINDUSTAN PETROLEUM CORPORATION LIMITED
Hindustan Petroleum Green R&D Centre, KIADB Industrial Area, Tarabanahalli, Devanagundi, Hoskote Taluk, Bangalore-560067, India

Inventors

1. BHOWMIK, Sandip
Analytical division, Hindustan Petroleum Green R&D center, Devanagonthi, Bangalore 560067, India
2. SIVA KESAVA RAJU, Chintalapati
Analytical division, Hindustan Petroleum Green R&D center, Devanagonthi, Bangalore 560067, India
3. KANALA, Raghava Krishna
Crude and Fuel research laboratory, Hindustan Petroleum Green R&D center, Devanagonthi, Bangalore 560067, India
4. SRINIVASA RAO, Ganagalla
Hydroprocessing department, Hindustan Petroleum Green R&D center, Devanagonthi, Bangalore 560067, India
5. MANGALA, Ramkumar
Crude and Fuel research laboratory, Hindustan Petroleum Green R&D center, Devanagonthi, Bangalore 560067, India
6. CHALAPATHI RAO, Peddy Venkata
Hindustan Petroleum Green R&D center, Devanagonthi, Bangalore 560067, India
7. VENKATESWARLU CHOUDARY, Nettam
Hindustan Petroleum Green R&D center, Devanagonthi, Bangalore 560067, India
8. SRIGANESH, Gandham
Hindustan Petroleum Green R&D center, Devanagonthi, Bangalore 560067, India

Specification

Claims:1. A lubricity additive formulation for enhancing lubricity of a fuel, the formulation comprising:
(a) 2-ethylhexanoic acid;
(b) at least one alkylene glycol; and
(c) at least one alkanolamine.
2. The lubricity additive formulation as claimed in claim 1, wherein 2-ethylhexanoic acid to the at least one alkylene glycol weight ratio is in the range of 1:0.03-1:0.4.
3. The lubricity additive formulation as claimed in claim 1, wherein 2-ethylhexanoic acid to the at least one alkanolamine weight ratio is in the range of 1:0.06-1:0.4.
4. The lubricity additive formulation as claimed in claim 1, wherein the at least one alkylene glycol has ‘n’ carbon atoms, wherein ‘n’ is an integer in the range of 2-10.
5. The lubricity additive formulation as claimed in claim 1, wherein the at least one alkanolamine has ‘m’ carbon atoms, wherein ‘m’ is an integer in the range of 1-10.
6. The lubricity additive formulation as claimed in claim 1, comprising:
(a) 2-ethylhexanoic acid having weight percentage in the range of 50-90% with respect to the formulation;
(b) at least one alkylene glycol having weight percentage in the range of 3-20% with respect to the formulation; and
(c) at least one alkanolamine having weight percentage in the range of 5-20% with respect to the formulation.
7. A process for preparation of lubricity additive formulation as claimed in claim 1, comprising: (a) contacting 2-ethylhexanoic acid, and at least one alkanolamine to obtain mixture-1; and (b) contacting the mixture-1, and at least one alkylene glycol to obtain the lubricity additive formulation.
8. The process as claimed in claim 7, wherein (a) contacting 2-ethylhexanoic acid, and the at least one alkanolamine to obtain mixture-1 is carried out a temperature in the range of 25-35 °C for a period in the range of 5-15 minutes at a stirring speed in the range of 200-500 rpm; (b) contacting the mixture-1 and the at least one alkylene glycol to obtain lubricity additive formulation is carried out a temperature in the range of 25-35 °C for a period in the range of 50-80 minutes at a stirring speed in the range of 200-500 rpm.
9. A method for enhancing lubricity of a fuel, the method comprising, contacting the lubricity additive formulation as claimed in any of the claims 1-6 with a fuel to obtain a fuel composition with enhanced lubricity.
10. The method as claimed in claim 9, wherein the lubricity additive formulation has concentration in the range of 20–120 ppm in the fuel composition.
11. The method as claimed in claim 9, wherein the fuel is a diesel having sulphur content in the range of 5–50 ppm.
12. A fuel composition comprising: (a) fuel; and (b) lubricity additive formulation as claimed in any of the claims 1–6.
13. The fuel composition as claimed in claim 12, wherein the fuel is a diesel having sulphur content in the range of 5–50 ppm.
14. A method for preparation of a fuel composition as claimed in claim 12, the method comprising steps of:
(a) obtaining lubricity additive formulation as claimed in any of claims 1-6;
(b) obtaining a fuel; and
(c) contacting the lubricity additive formulation and the fuel to obtain the fuel composition.

15. The method as claimed in claim 14, wherein the fuel is a diesel having sulphur content in the range of 5–50 ppm.
, Description:AS ATTACHED

Documents

Application Documents

# Name Date
1 201741019502-RELEVANT DOCUMENTS [27-09-2023(online)].pdf 2023-09-27
1 Form 5 [02-06-2017(online)].pdf 2017-06-02
2 201741019502-RELEVANT DOCUMENTS [27-09-2022(online)].pdf 2022-09-27
2 Form 3 [02-06-2017(online)].pdf 2017-06-02
3 Description(Complete) [02-06-2017(online)].pdf_226.pdf 2017-06-02
3 201741019502-PROOF OF ALTERATION [01-11-2021(online)].pdf 2021-11-01
4 Description(Complete) [02-06-2017(online)].pdf 2017-06-02
4 201741019502-US(14)-ExtendedHearingNotice-(HearingDate-01-12-2020).pdf 2021-10-17
5 201741019502-US(14)-HearingNotice-(HearingDate-25-11-2020).pdf 2021-10-17
5 201741019502-Proof of Right (MANDATORY) [28-08-2017(online)].pdf 2017-08-28
6 201741019502-IntimationOfGrant31-12-2020.pdf 2020-12-31
6 201741019502-FORM-26 [28-08-2017(online)].pdf 2017-08-28
7 Correspondence by Agent_POA,POR_29-08-2017.pdf 2017-08-29
7 201741019502-PatentCertificate31-12-2020.pdf 2020-12-31
8 201741019502-Written submissions and relevant documents [15-12-2020(online)].pdf 2020-12-15
8 201741019502-FORM 18 [14-09-2017(online)].pdf 2017-09-14
9 201741019502-CERTIFIED COPIES TRANSMISSION TO IB [10-05-2018(online)].pdf 2018-05-10
9 201741019502-Correspondence to notify the Controller [23-11-2020(online)].pdf 2020-11-23
10 201741019502-FORM 3 [09-04-2020(online)].pdf 2020-04-09
10 201741019502-FORM 3 [24-10-2018(online)].pdf 2018-10-24
11 201741019502-CLAIMS [23-09-2019(online)].pdf 2019-09-23
11 201741019502-FER.pdf 2019-03-26
12 201741019502-FER_SER_REPLY [23-09-2019(online)].pdf 2019-09-23
12 201741019502-OTHERS [23-09-2019(online)].pdf 2019-09-23
13 201741019502-FORM 3 [23-09-2019(online)].pdf 2019-09-23
13 201741019502-Information under section 8(2) (MANDATORY) [23-09-2019(online)].pdf 2019-09-23
14 201741019502-FORM 3 [23-09-2019(online)].pdf 2019-09-23
14 201741019502-Information under section 8(2) (MANDATORY) [23-09-2019(online)].pdf 2019-09-23
15 201741019502-FER_SER_REPLY [23-09-2019(online)].pdf 2019-09-23
15 201741019502-OTHERS [23-09-2019(online)].pdf 2019-09-23
16 201741019502-CLAIMS [23-09-2019(online)].pdf 2019-09-23
16 201741019502-FER.pdf 2019-03-26
17 201741019502-FORM 3 [24-10-2018(online)].pdf 2018-10-24
17 201741019502-FORM 3 [09-04-2020(online)].pdf 2020-04-09
18 201741019502-CERTIFIED COPIES TRANSMISSION TO IB [10-05-2018(online)].pdf 2018-05-10
18 201741019502-Correspondence to notify the Controller [23-11-2020(online)].pdf 2020-11-23
19 201741019502-FORM 18 [14-09-2017(online)].pdf 2017-09-14
19 201741019502-Written submissions and relevant documents [15-12-2020(online)].pdf 2020-12-15
20 201741019502-PatentCertificate31-12-2020.pdf 2020-12-31
20 Correspondence by Agent_POA,POR_29-08-2017.pdf 2017-08-29
21 201741019502-FORM-26 [28-08-2017(online)].pdf 2017-08-28
21 201741019502-IntimationOfGrant31-12-2020.pdf 2020-12-31
22 201741019502-Proof of Right (MANDATORY) [28-08-2017(online)].pdf 2017-08-28
22 201741019502-US(14)-HearingNotice-(HearingDate-25-11-2020).pdf 2021-10-17
23 201741019502-US(14)-ExtendedHearingNotice-(HearingDate-01-12-2020).pdf 2021-10-17
23 Description(Complete) [02-06-2017(online)].pdf 2017-06-02
24 201741019502-PROOF OF ALTERATION [01-11-2021(online)].pdf 2021-11-01
24 Description(Complete) [02-06-2017(online)].pdf_226.pdf 2017-06-02
25 Form 3 [02-06-2017(online)].pdf 2017-06-02
25 201741019502-RELEVANT DOCUMENTS [27-09-2022(online)].pdf 2022-09-27
26 Form 5 [02-06-2017(online)].pdf 2017-06-02
26 201741019502-RELEVANT DOCUMENTS [27-09-2023(online)].pdf 2023-09-27

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