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A Fuel Additive Composition And The Process Of Preparing The Same

Abstract: The present invention relates to a fuel additive composition. More particularly, the present invention relates to the fuel additive composition which is prepared by using is a combination of various organic compound. This invention also relates to the fuel additive composition which contains Mineral Turpentine Oil, Nonyl Phenol ethylene Oxide condensate, Di-ethylene Glycol Laurate etc. Moreover this invention relates to the process for the preparation of the above composition. This invention also relates the fuel additive composition by which the engine deterioration is effectively prevented, the fuel combustion efficiency are is improved, and the exhaust emission pollution is reduced.

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Patent Information

Application #
Filing Date
03 October 2018
Publication Number
42/2018
Publication Type
INA
Invention Field
CHEMICAL
Status
Email
Parent Application
Patent Number
Legal Status
Grant Date
2021-03-30
Renewal Date

Applicants

NISHANTA ENVIRONMENTAL TECHNOLOGY CO LTD
30, CREEK ROW, GROUND FLOOR, KOLKATA-700014, WEST BENGAL, INDIA

Inventors

1. AMAL KANTI CHAKRABARTI
'BANI' JOGENDRA NATH BALIKA VIDYAMANDIR ROAD, PO-NABAPALLY, BARASAT, KOLKATA-700126
2. MANAS CHAKRABARTI
3A, EDEN ORCHID, 2944, BUDERHAT ROAD, NAYABAD, KOLKATA-700094

Specification

Field of the Invention
The present invention relates to a fuel additive composition. More particularly,
the present invention relates to the fuel additive composition which is prepared
by using a combination of various organic compound. This invention also
relates to the fuel additive composition which contains Mineral Turpentine Oil,
Nonyl Phenol ethylene Oxide condensate, Di-ethylene Glycol Laurate etc.
Moreover this invention relates to the process for the preparation of the above
composition. This invention also relates the fuel additive composition by which
the engine deterioration is effectively prevented, the fuel combustion efficiency
is improved, and the exhaust emission pollution is reduced.
Background of the invention and related prior Art
Fuel oils can be divided into two primary classifications, i.e., distillate fuel oils,
and residual fuel oils. Distillate oils are composed entirely of material
vaporized in refinery distillation towers; consequently, they are clean and free
of sediments, relatively low in viscosity, and they contain no inorganic ash.
Residual fuel oils, however, contain fractions that cannot be readily vaporized
by heating. These fractions are black and viscous, and they include any organic
ash components originally present in the crude. In some cases, the whole crude
itself is used as a residual fuel.

Distillate fuel oils, being low in sulfur, free of ash, and relatively easy to
handle, are used in applications where such qualities are more important than
fuel prices, for example, in home heating. However, where cost is an important
consideration, and large volumes of fuel are required, for instance, in electric
power generation, in producing industrial steam, for process heating and the
like, residual oils are usually employed as the fuels of choice. The single largest
source of energy of energy in India after coal is petroleum. About two-third of
which is imported. The petroleum derived fuel, i.e. motor gasoline and diesel
are being used almost by the entire road transport vehicles. The diesel fuel is
also being used in agriculture operations. The high dependence on important
outside source of energy is an issue related to energy security of the country. In
the recent time, the combustion of these fossil fuels has been recognized as a
major cause of air pollution in Indian cities.
The document CN105567349 has illustrated an organic compound fuel oil
additive. The additive comprises, by volume, 20-50 % of diesel oil, 10-20 % of
butyl lactate, 20-40 % of naphtha, 2-15 % of turpentine, 20-40 % of petroleum
ether, 10-20 % of dimethyl acetamide, 1-10 % of ethyl acetate, 1-3 % of cerium
stearate, 1-2.5 % of cerium naphthenate, 10-30 % of acetone, 1-6 % of
butanone, 5-15 % of ethanol, 20-40 % of methanol, 10-20 % of isopropanol,
10-30 % of dimethyl ether, 10-30"% of xylene, 10-30 % of trimethylbehzene,
10-25 % of 1,3-xylene and 1-5 % of perfluorooctanoate sulfonyl chloride.

The invention of CN101541937 states a method for refining vegetable oils, in
particular cottonseed oil or a possible mixture of it with others, as substitute of
diesel fuel remarkable in that a sequence of treatment steps to be performed on
crude vegetable oil, including: a) a pre-treatment thereof consisting of the
removal of oil insoluble impurities from the crude oil, b) removal of oil soluble
impurities therefrom, c) a free acid neutralization thereof, and d) a drying,
bleaching and filtration thereof. This invention also relates to an Additive of
organic basis, containing ether, ketone, toluene, hexane, turpentine, alcohols in
specific concentrations.
The other document CA2650333 states an emulsified biofuel composition
comprising: (A) a continuous phase comprising about 50-95 wt% of at least one
liquid oil of vegetable or animal origin or mixtures thereof; (B) a water-
containing dispersed phase comprising about 1-50 wt% water; (C) about 1-25
wt% of hydroxyl-containing organic compound selected from the group
consisting of mono-, di-, tri- and polyhydric alcohols, provided that when a
monohydric alcohol is used there is also present at least one of tert-butyl
alcohol, at least one C2-C4 alkylene glycol or a mixture of both; (D) about
0.05-10 wt% of at least one emulsifier; wherein the dispersed water-containing
droplets have an average particle size of less than about 20 microns. The
biofuel is prepared from these components by mixing under high shear
conditions, preferably with ultrasonic energy. The emulsifier(s) preferably
exhibit a hydrophilic-lipophilic balance of about 8.5 to about 18 and the biofuel

includes a cetane enhancer and mixture of an alcohol and mono- or poly-
alkylene glycol.
The document EP2044178 describes the Fuel formulations may be produced
from vegetable oil without the need to remove glycerin from the vegetable oil
prior to use. The fuel formulations may be used in diesel fuel vehicles and/or as
a home heating oil. The fuel formulations may include vegetable oil, kerosene,
a fuel stabilizer, and a cetane boost additive.
This invention of WO2006095219 relates to a fuel for a diesel engine,
comprising more than 60 % by weight of a vegetable oil and 1-5 % by weight
of a vegetable based organic solvent comprising a terpene compound, a method
for producing a vegetable based fuel, use of a vegetable based fuel in a diesel
engine, a method for operating a diesel engine using a vegetable based fuel, and
a fuel system for providing a diesel engine with a vegetable based fuel.
A herbal composition as stated in document J. KISHORE KUMAR et al (2016
describes Pollution from the petroleum oil is increasing day by day in terms of
C02, CO, NOX, and many other gases and particles. Price difference and
economy leads people toward the use of alternative fuels. To overcome this
problem turpentine oil is mixed with petrol and diesel and taken as different
samples. Then the properties like flash point, fire point, cloud and pour point,
calorific value, carbon content test, ash content test, copper corrosion test are
analyzed at various proportions of turpentine oil (5%, 10%, 15%, 20% of 100
ml sample) blended with petrol and Diesel fuels. Any other type of substance,

can be assigned some physical and chemical properties (e.g. density, thermal
capacity, vapour pressure, chemical formula, etc). However, most of the times,
combustion properties are also assigned to blended fuels, in spite of the fact
that these properties depend on the oxidizer (e.g. air, pure oxygen) and the
actual process (e.g. the explosion limits depend on the boundary conditions for
a given fuel/oxidizer pair). Fuel price, availability, risk, and so on, could also
be considered fuel properties (attributes).
This invention of the document Phan et al. (2008) relates to the Alkali-
catalyzed transesterification of waste cooking oils, collected within Ho Chi
Minh City, Vietnam, with methanol was carried out in a laboratory scale
reactor. The effects of methanol/waste cooking oils ratio, is on potassium
hydroxide concentration and temperature.
Curran et al., (2001) describes IZmission standards for diesel engines in
vehicles have been steadily reduced in recent years, and a great deal of research
and development effort has been focused on reducing particulate and nitrogen
oxide emissions. One promising approach to reducing emissions involves the
addition of oxygen to the fuel, generally by adding an oxygenated compound to
the normal diesel fuel. Miyamoto et al. showed experimentally that particulate
levels can be significantly reduced by adding oxygenated species to the fuel.
They found the Bosch smoke number (a measure of the particulate or soot
levels in diesel exhaust) falls from about 55% for conventional diesel fuel to
less than 1% when the oxygen content of the fuel is above about 25% by mass,

Current theories and models have been quite successful in understanding the
reaction paths for the early % of this process, namely the cyclization of the
smaller fragments into aromatic hydrocarbons with one, two and three rings.
The subsequent production of real soot remains a subject for continued study.
The present model indicates that when significant fractions of diesel fuel are
replaced by oxygenated species, the carbon atoms already bonded to oxygen
atoms cannot provide soot precursors, and this process is responsible for the
observed results. Since the fractions of oxygenates required to completely
eliminate soot precursor production are so large, approaching 75-80%, it is
probably unrealistic to attempt this degree of fuel modification in actual diesel
engine practice, but the insights into the processes leading to soot provided by
the model, supported by the excellent qualitative agreement between
experimental and model results, can be very valuable in future studies of diesel
combustion chemistry..
The invention stated in the document US20080005957, describes a biodiesel
handling and blending system using varying parameters of biodiesel/distillate
blend ratio, temperature, and amount of mixing occurring in the batch, to obtain
positive results. The results showed that when zero (0) degree petroleum
distillate was blended with fifty (50) degree biodiesel, and thoroughly mixed;
the resulting homogeneous blend did not contain wax crystals. The results also
showed that once the biodiesel had been distributed homogeneously throughout

the sample, the resulting mixture exhibited properties more like a petroleum
distillate than like a methyl ester.
The document US5820640 states a novel diesel engine fuel is in the form of a
pyrolysis liquid-in-diesel oil microemulsion fuel comprising: (a) diesel oil in an
amount sufficient to form a continuous phase in the composition; (b) a
pyrolysis liquid forming a discontinuous phase in the composition, this
pyrolysis liquid being a liquid obtained by rapid pyrolysis of biomass; and (c)
at least one emulsifier selected from nonionic hydrophilic surfactants with HLB
between 4 and 18, derived from fatty acids and polyoxyethylene glycol, or fatty
acids, sorbitol and polyoxyethylene or polyethoxylated alcohols with long
aliphatic chains. This fuel has excellent stability and physical properties similar
to those of regular diesel fuel.
The document IN 235992 describes Petro - Diesel Catalyst Additive, an Eco-
friendly fuel additive comprising of:- Aliphatic Hydrocarbons of molecular
formula (CnH2n-2); n= 8 to 18 — 60 - 80% (v/v) Ethylene Diamine Dilaurate
— 5 - 15% (v/v) Butyl Ricinoleate — 0.5 - 3% (v/v) Benzoyl Peroxide — 0.3 -
3% (v/v) Cyclohexylnitrate — 7-15% (v/v) Isobutelene Succinimide — 2 - 6%
(v/v) Barium Petroleum Sulphonate — 0.3 - 0.5% (v/v) 5-ethoxy Nonyl Phenol
— 0.5-1% (v/v) which is added to fuel oil at at 1 : 100 ratio. This composition
enhances thermal efficiency of Internal Combustion engines with profound
effect in lowering the exhaust pollution. Higher efficiency of the combustion

engine promotes to fuel savings, leading to conservation of non-renewable
energy sources. The finished catalytic additive product shows synergistic effect
with any kind of liquid fuel.
The other document 201817005385 describes a lubricating composition for use
in heavy duty diesel engines which is formulated to allow the use of
organomolybdnem compounds but which overcomes the issue of Cu and/or Pb
corrosion. The lubricant is characterized by having a synergistic additive
composition comprising (A) a sulfur free organo molybdenum compound (B) a
sulfur containing organo molybdenum compound and (C) a triazole derivative
prepared by reacting 1 2 4 triazole a formaldehyde source and an amine; (A)
(B) and (C) being present in an amount sufficient to allow the lubricating
composition to pass the High Temperature Corrosion Bench Test ASTM D
6594 with respect to Cu and/or Pb corrosion.
The document 201847015965 discloses a diesel additive. The diesel additive
comprises 80-100 wt.% of a nonylphenol polyether amine and 0-20 wt.% of a
diluent, based on the total weight of the diesel additive. The diesel additive
provided by the present invention can be used to remove carbon deposits at the
nozzle of a diesel engine.
Therefore, attention is being paid to find alternative approaches. It is the object
of the present invention to develop a suitable blend of a pyrolysis liquid

obtained by rapid pyrolysis of biomass with diesel oil that can be used as diesel
engine fuel.
Summary of the invention
The present invention relates to a fuel additive composition. More particularly,
the present invention relates to the fuel additive composition which is prepared
by using a combination of various organic compound. This invention also
relates to the fuel additive composition which contains Mineral Turpentine Oil,
Nonyl Phenol ethylene Oxide condensate, Di-ethylene Glycol Laurate etc.
Moreover this invention relates to the process for the preparation of the above
composition. This invention also relates the fuel additive composition by which
the engine deterioration is effectively prevented, the fuel combustion efficiency
is improved, and the exhaust emission pollution is reduced.
Detailed description of the invention
The control of emission from internal combustion engines has received
substantially continuous attention worldwide for many years attempting
reduction of emission of carbon monoxide (CO), Nitrogen oxides (NOx),
unburnt hydrocarbons (HC), and other pollutants like P.M. (particulate matter)
from the combustion of fuels but generally have met with limited success.
Still other object of the present invention is to provide the fuel additive
composition which is prepared by using a combination of various organic
compound.

Another object of the present invention is to provide the fuel additive
composition which comprises the aliphatic hydrocarbon having higher carbon
chain is 15-25 % by volume; Mineral Turpentine oil having lower carbon
chain is 15 - 30 % by vol; Nonyl phenol ethoxylate is 3 - 10 % by volume; 2 -
Ethylhexyl nitrate is 10- 30 % by vol; tert amyl ethyl ether is 3 - 7 % by vol;
Di-ethylene Glycol laurate is 5 - 15 % by vol; Butyl Recinoleate is 3 - 8 % by
vol; p-Xylene is 3-7 % by vol. and Mesitylene is 5 - 15 % by vol.
Still other object of the present invention to provide the fuel additive
composition wherein the surfactant is Nonyl phenol ethoxylate.
Another object of the present invention is to provide the process for the
preparation of the fuel additive composition which comprises
a) 15 - 25 % by volume of the aliphatic hydrocarbon having higher carbon
chain, 15-30 % by vol Mineral Turpentine oil and 3 - 10 % by volume
of Nonyl phenol ethoxylate are blended properly;
b) 10- 30 % by vol of 2 - Ethylhexyl nitrate followed by 3 - 7 % by vol of
tert amyl ethyl ether are mixed with above composition;
c) Then 5 - 15 % by vol of Di-ethylene Glycol laurate and 3 - 8 % by vol
of Butyl Recinoleate are mixed;
d) Finally 3-7 % by vol of p-Xylene between and 5 - 15 % by vol
Mesitylene. are mixed with above composition.

Another object of the present invention is to provide the process for the
preparation of the fuel additive composition wherein the cetane improver is 2 —
Ethylhexyl nitrate.
Still other object of the present invention to provide the fuel additive
composition which will improve the diesel fuel with increase in efficiency by
10 - 16 % and is reducing emission pollution by 40 - 50 %.
Still other object of the present invention to provide the fuel additive
composition wherein mineral turpentine oil will improve ignition efficiency of
the fuel.
The object of the present invention is to provide a fuel additive composition
which when added to diesel fuel, will provide clean and more efficient
combustion in internal combustion engines there by reducing pollution and
saving of fuel.
Still other object of the present invention to provide the fuel additive
composition wherein Alkylene glycol ester along with Butyl recinoleate
lubricates the upper portion of the cylinders.
Still other object of the present invention to provide the fuel additive
composition wherein the concentrate mother mixture is diluted with proper
succussion with BS VI diesel in the ratio 1:100.

The control of emission from internal combustion engines has received
substantially continuous attention worldwide for many years attempting
reduction of emission of carbon monoxide (CO), Nitrogen oxides (NOx),
unburnt hydrocarbons (HC), and other pollutants like P.M. (particulate matter)
from the combustion of fuels but generally have met with limited success.
It is accordingly the fuel additive composition which when added to diesel fuel,
will provide clean and more efficient combustion in internal combustion
engines thereby reducing pollution and increasing mileage and to provide a
multifunctional fuel additive which will not have any harmful effect over
engines.
The fuel additive also provide fully miscible with any other additive (like
biodiesel, alcohol etc.) if present in the diesel fuel.
On additive which on mixing with the diesel fuel in proper ratio will improve
the diesel fuel with increase in efficiency by 10 - 16 % and reducing emission
pollution by 40 - 50 %.
The improved diesel fuel composition which has the capability of reducing
polluting emission substantially and will reduce fuel cost which is much more
than the cost of the additive.
The fuel additive which is easily applicable, highly economic as it reduces fuel
expenditure by at least 10 - 16 % depending on the engine HP, Torque and
other factors like engine condition, age, load etc. As the additive helps to burn

the fuel more efficiently, better combustion naturally creates less emission and
increases mileage. According to the concept the fuel additive particularly
reduces carbon monoxide (CO), Hydro Carbon (HC) and unburnt carbon
emission (particulate matter / Smoke).
The fuel additive composition is formulated to contain aliphatic hydrocarbon of
carbon range C8 - C20, Mineral Turpentine Oil, Alkylene glycol esters, Alkyl
ester, Liquid Nonionic surfactant, cetane improver like 2 ethyl hexyl nitrate,
Oxygenates like Tert. Amyl Ethyl Ether, and synergistic compounds like
Mesitylene and p-Xylene.
The cetane improver reduces the ignition delay where mineral turpentine oil
appear to improve ignition efficiency of the fuel. Alkylene glycol ester along
with Butyl recinoleate help to lubricate the upper portion of the cylinders as
well as in combination with non-ionic surfactant disperse water contained in
the fuel system so as not to interfere with the complete combustion of the fuel
system. Tert amyl ethyl ether acts as oxygenate whereas Mesitylene and p-
Xylene provide synergistic effect.
The total concentrated mixture is then diluted with proper succussion with BS
VI diesel in the ratio 1:100 for use as the final additive which again
dramatically increases the efficiency of the engine and fuel duly observed with
prolonged experimentation as noted below with the following dosage:-
4 ml /10 litre of diesel fuel for use in engines up to 100 HP
5 ml /10 litre of diesel fuel for use in engines over 100 HP

It is now a known fact that presence of sulphur in Diesel, although a source of
emission pollutant like SOx; also can impact substantial lubricity to engines.
So, lower sulphur concentrations as stipulated in BSVI (Equivalent to Euro VI)
specification has lower lubricity effect. This multifunctional Diesel additive has
shown to improve the lubricity notably when tested using High Frequency
Reciprocating Rig (HFRR) method. Several experimentation of the Diesel
additive in very old passenger buses (which travelled more than 500 thousand
kilometers) showed drastic cut in emission pollution through engine exhaust by
more than 65 - 70 % particularly in terms of CO & HC emissions.
Experimentation of the Diesel additive is SUV & Buses including Volvo buses,
High capacity Diesel Generator. (750 KV) show savings of fuel by about 10 -
16 % by volume.
When mixed with Diesel (commercially available in petrol Pumps), it has
shown remarkable increase in Cetane No, Cetane Index , improved CFPP, pour
point etc. thus establishing that the Diesel fuel quality is improved & did not
have any adverse effect on its original quality.
The fuel additive composition of the present invention is formulated to include
as one component thereof Diesel BS VI, as a mediator to mix properly with
Diesel in the second stage as the additive is solely meant for Diesel fuel.
Another component used in the fuel additive composition is Mineral Turpentine
oil, which is an aliphatic hydrocarbon in the range (C7 - C12) and having
boiling range (150°C - 200°C)is believed to help at least in part the initial
ignition of the Diesel fuel.

One cetane improver 2 - ethyl hexyl nitrate having molecular formula
(C8H17NO3) has been used to boost the cetane no. For improved cetane no
ignition delay time is drastically reduced providing much better combustion,
automatically effecting reduction of emission
is used as a
generating supply
Another component tert amyl Ethyl Ether
fuel oxygenate which helps in combustion
of oxygen.
Another compound a nonionic surfactant, Nonyl Phenol poly
ethoxylate (C9H19C6H4(OCH2CH2)nOH) is used where it is
believed that surfactant and the ether (acting as a coupling
agent) cooperate each other to minimize the effect of water
contained in the diesel fuel during the combustion process.
Such surfactants are commercially available in the market as
NPEO 4.5, NPEO 9.5 etc.
Other two compounds Diethylene glycol laurate and Butyl recinoleate are used
in the fuel additive having formula (C16H32O4) & (C22H42O3) specifically have
both surfactant effect as well as lubricating effect on the upper part of the
cylinder. Both laurate and Recinoleate % having lubricating property, provide
the required upper cylinder lubrication and controlled oxidation.
Two other compounds p-Xylene and Mesitylene are used for synergistic effect
which not limiting to theory are believed to provide miraculous effect in
combination with the other chemicals.
In general the composition of the present invention is somewhat sensitive to
variation in the amount. In general the aliphatic hydrocarbon having higher
carbon chain may vary from 15-25 % by volume whereas Mineral Turpentine
oil having lower carbon chain also may vary from 15-30 % by vol. (surfactant
Nonyl phenol ethoxylate will vary from 3 - 10 % by volume, 2 - Ethylhexyl
nitrate is used between 10- 30 % by vol. followed by tert amyl ethyl ether
between 3 - 7 % by vol. Then Di-ethylene Glycol laurate between 5 - 15 % by

vol. and Butyl Recinoleate 3 - 8 % by vol. are mixed. Finally p-Xylene
between 3-7 % by vol. & Mesitylene 5 - 15 % by vol. are mixed for synergistic
effect.
Finally after mixing the components in the most conventional technique, the
concentrate mother additive is diluted with proper succussion with BS VI
equivalent to Euro VI diesel.
Though in precise manner how the diluted and agitated components function in
combination is fully not understood at the present time, yet it has been observed
that the diluted mixture after proper succussion in the expert way which
dramatically improves the property of the additive. This procedure of mixing
using succussion probably resembles the well known potentisation process.
The additive when mixed in the ratio mentioned before with diesel fuel initiates
internal combustion of the engine increasing its efficiency and reducing
pollution enormously.
Different combinations have been tried which are illustrated by the following
examples.
However, this should not be construed to limit the scope of the present
invention. The present invention is illustrated by the following examples, which
is not intended to limit the effective scope of the invention. Out of five
examples given below, example V is found to be most suitable because it
obviates the drawbacks.

Example I :
The process for the preparing the fuel additive composition which comprises 25
- 45 % by volume of the aliphatic hydrocarbon having higher carbon chain, 25
- 30 % by vol Mineral Turpentine oil and 3 - 10 % by volume of Nonyl phenol
ethoxylate are blended properly; 5- 10 % by vol of 2 - Ethylhexyl nitrate
followed by 3 - 7 % by vol of tert amyl ethyl ether are mixed with above
composition; Then 5 - 15 % by vol of Di-ethylene Glycol laurate and 6 - 8 %
by vol of Butyl Recinoleate are mixed; Finally 6 -7 % by vol of p-Xylene
between and 12 - 15 % by vol Mesitylene. are mixed with above composition.
Example II:
The process for the preparing the fuel additive composition which comprises 10
- 16 % by volume of the aliphatic hydrocarbon having higher carbon chain, 15
- 30 % by vol Mineral Turpentine oil and 3 - 10 % by volume of Nonyl phenol
ethoxylate are blended properly; 15- 20 % by vol of 2 - Ethylhexyl nitrate
followed by 3 - 6 % by vol of tert amyl ethyl ether are mixed with above
composition; Then 5 - 10 % by vol of Di-ethylene Glycol laurate and 3 - 5 %
by vol of Butyl Recinoleate are mixed; Finally 3-4 % by vol of p-Xylene
between and 5 - 8 % by vol Mesitylene. are mixed with above composition.
Example III :
The process for the preparing the fuel additive composition which comprises 20
- 25 % by volume of the aliphatic hydrocarbon having higher carbon chain, 15

- 25 % by vol Mineral Turpentine oil and 3 - 10 % by volume of Nonyl phenol
ethoxylate are blended properly; 10- 30 % by vol of 2 - Ethylhexyl nitrate
followed by 4 - 6 % by vol of tert amyl ethyl ether are mixed with above
composition; Then 5 - 9 % by vol of Di-ethylene Glycol laurate and 3 - 6 % by
vol of Butyl Recinoleate are mixed; Finally 3-5 % by vol of p-Xylene between
and 5 - 8 % by vol Mesitylene. are mixed with above composition.
Example IV :
The process for the preparing the fuel additive composition which comprises 12
- 15 % by volume of the aliphatic hydrocarbon having higher carbon chain, 15
- 20 % by vol Mineral Turpentine oil and 3 - 6 % by volume of Nonyl phenol
ethoxylate are blended properly; 10- 15 % by vol of 2 - Ethylhexyl nitrate
followed by 3 -6 % by vol of tert amyl ethyl ether are mixed with above
composition; Then 5-12 % by vol of Di-ethylene Glycol laurate and 3 - 5 %
by vol of Butyl Recinoleate are mixed; Finally 3-6 % by vol of p-Xylene
between and 5 - 10 % by vol Mesitylene are mixed with above composition.
Example V :
The process for the preparing the fuel additive composition which comprises 15
- 25 % by volume of the aliphatic hydrocarbon having higher carbon chain, 15
- 30 % by vol Mineral Turpentine oil and 3 - 10 % by volume of Nonyl phenol

ethoxylate are blended properly; 10- 30 % by vol of 2 - Ethylhexyl nitrate
followed by 3 - 7 % by vol of tert amyl ethyl ether are mixed with above
composition; Then 5 - 15 % by vol of Di-ethylene Glycol laurate and 3 - 8 %
by vol of Butyl Recinoleate are mixed; Finally 3-7 % by vol of p-Xylene
between and 5 - 15 % by vol Mesitylene are mixed with above composition.
Finally the concentrate mother mixture is diluted with proper succussion with
BS VI equivalent to Euro VI diesel in a proportion of 1:100 to get this actual
additive.
The result of the experiment of the example V was excellent and the
formulation had excellent fuel additive composition to make it synergistic
effect and improved efficacy with respect to other fuel additive.
ADVANTAGES OF THE INVENTION
The fuel additive composition of the impugned invention has the following
advantages:
1. The fuel additive composition is user friendly and cost effective;
2. It has high fuel oil efficiency, good fuel economy and less air pollution.
3. It improves the fuel combustion efficiency and reduce emission pollution.
Modifications and variations of the present invention relating to a fuel additive
composition and an alternative fuel derived from the composition will be
obvious to those skilled in the art from the foregoing detailed description of the
invention. Such modifications and variations are intended to come within the
scope of the appended claims.

We claim:
1) A fuel additive composition which comprises an effective amount of the
aliphatic hydrocarbon having higher carbon chain; Mineral Turpentine
oil having lower carbon chain; Nonyl phenol ethoxylate; 2 - Ethylhexyl
nitrate; tert amyl ethyl ether; Di-ethylene Glycol laurate; Butyl
Recinoleate; p-Xylene and Mesitylene.
2) The fuel additive composition which comprises the aliphatic
hydrocarbon having higher carbon chain is 15 - 25 % by volume;
Mineral Turpentine oil having lower carbon chain is 15 - 30 % by vol;
Nonyl phenol ethoxylate is 3 - 10 % by volume; 2 - Ethylhexyl nitrate
is 10- 30 % by vol; tert amyl ethyl ether is 3 - 7 % by vol; Di-ethylene
Glycol laurate is 5 - 15 % by vol; Butyl Recinoleate is 3 - 8 % by vol; p-
Xylene is 3-7 % by vol. and Mesitylene is 5 - 15 % by vol.
3) The fuel additive composition wherein the surfactant is Nonyl phenol
ethoxylate.
4) The fuel additive composition wherein the cetane improver is 2 —
Ethylhexyl nitrate.
5) A process for the preparation of the fuel additive composition which
comprises

a) 15 - 25 % by volume of the aliphatic hydrocarbon having higher
carbon chain, 15 - 30 % by vol Mineral Turpentine oil and 3 - 10 %
by volume of Nonyl phenol ethoxylate are blended properly;
b) 10-30 % by vol of 2 - Ethylhexyl nitrate followed by 3 - 7 % by
vol of tert amyl ethyl ether are mixed with above composition;
c) Then 5 - 15 % by vol of Di-ethylene Glycol laurate and 3-8 % by
vol of Butyl Recinoleate are mixed;
d) Finally 3-7 % by vol of p-Xylene between and 5 - 15 % by vol
Mesitylene. are mixed with above composition.
6) The fuel additive composition as claimed in claim 1 which is mixed with
BS VI quality of diesel with proper succussion in 1:100 proportion to
get the additive for use.
7) The process for the preparation of composition as claimed in claim 5
wherein the surfactant is Nonyl phenol ethoxylate.
8) The process for the preparation of the fuel additive composition as
claimed in claim 5 wherein the cetane improver is 2 - Ethylhexyl
nitrate.
9) The fuel additive composition as claimed in claim 1 which will improve
the diesel fuel with increase in efficiency by 10 - 16 % and reducing
emission pollution by 40 - 50 % when mixed with diesel fuel at a
dosage:-

4 ml / 10 litre of diesel fuel for use in engines up to 100 HP
5 ml /10 litre of diesel fuel for use in engines over 100 HP
10)The fuel additive composition wherein Alkylene glycol ester along with
Butyl recinoleate lubricates the upper portion of the cylinders.

Documents

Application Documents

# Name Date
1 201831037272-(03-10-2018)-SPECIFICATION.pdf 2018-10-03
2 201831037272-(03-10-2018)-FORM-9.pdf 2018-10-03
3 201831037272-(03-10-2018)-FORM-3.pdf 2018-10-03
4 201831037272-(03-10-2018)-FORM-2.pdf 2018-10-03
5 201831037272-(03-10-2018)-FORM-18.pdf 2018-10-03
6 201831037272-(03-10-2018)-FORM-1.pdf 2018-10-03
7 201831037272-(03-10-2018)-DESCRIPTION (COMPLETE).pdf 2018-10-03
8 201831037272-(03-10-2018)-CORRESPONDENCE.pdf 2018-10-03
9 201831037272-(03-10-2018)-CLAIMS.pdf 2018-10-03
10 201831037272-(03-10-2018)-ABSTRACT.pdf 2018-10-03
11 201831037272-FER.pdf 2019-10-29
12 201831037272-(04-05-2020)-REPLY TO FER.pdf 2020-05-04
13 201831037272-(04-05-2020)-OTHERS.pdf 2020-05-04
14 201831037272-(04-05-2020)-FORM-1.pdf 2020-05-04
15 201831037272-NBA PERMISSION-(27-01-2021).pdf 2021-01-27
16 201831037272-(25-03-2021)-PUBLIC NOTICE.pdf 2021-03-25
17 201831037272-(25-03-2021)-PETITION FOR CONDONING DELAY.pdf 2021-03-25
18 201831037272-(25-03-2021)-MARKED-UP COPY.pdf 2021-03-25
19 201831037272-(25-03-2021)-CORRESPONDENCE.pdf 2021-03-25
20 201831037272-(25-03-2021)-CLAIMS.pdf 2021-03-25
21 201831037272-PatentCertificate30-03-2021.pdf 2021-03-30
22 201831037272-IntimationOfGrant30-03-2021.pdf 2021-03-30
23 201831037272-(25-05-2021)-RENEWAL FEES.pdf 2021-05-25
24 201831037272-US(14)-HearingNotice-(HearingDate-16-03-2021).pdf 2021-10-18
25 201831037272-15-09-2022-RENEWAL FEES.pdf 2022-09-15
26 201831037272-RELEVANT DOCUMENTS [29-09-2022(online)].pdf 2022-09-29

Search Strategy

1 2019-10-2410-37-24_24-10-2019.pdf

ERegister / Renewals

3rd: 25 May 2021

From 03/10/2020 - To 03/10/2021

4th: 25 May 2021

From 03/10/2021 - To 03/10/2022

5th: 25 May 2021

From 03/10/2022 - To 03/10/2023

6th: 15 Sep 2022

From 03/10/2023 - To 03/10/2024

7th: 06 Apr 2023

From 03/10/2024 - To 03/10/2025