FIELD OF INVENTION
This invention relates to an herbal composition for oral care and a process for the preparation thereof. Particularly this invention relates to a novel herbal composition and a process for the preparation thereof. The herbal composition is useful for complete oral care.
BACKGROUND OF THE INVENTION
A number of tooth paste are as such known in the prior art for cleaning the tooth. Even the herbal tooth paste compositions are known in the prior art for cleaning the tooth. One of the herbal tooth paste is disclosed in the Indian patent no. 215567. The tooth paste composition comprises 0.5 to 0.85 weight percent carrageenam, at least 70% of the carrageenam being iota carrageenam, 35 to 50 weight percent water, 35 to 50 weight percent of a calcium based polishing agent or abrasive, 5 to 15 weight percent humectant and 0.5 to 5.0 weight percent surfactant.
In the PCT application no. PCT/EP1999/005362, a tooth paste comprising, in a liquid or pasty medium, particulate calcium carbonate as the main abrasive cleaning agent is disclosed. Characterized in that the particulate calcium carbonate comprises a mixture of 75 - 92.5 % by weight of the mixture fine of particulate calcium carbonate with a weight average particle size of between 1 and 15 microns, and 7.5 - 25 % by weight of the mixture of coarse particulate calcium carbonate with a weight average particle size of between 30 and 120 microns.
In the US patent no. 7083779, a process for the preparation of a formulation is disclosed. The formulation comprises 2 to 5.5% w/v (Azadirachta indica from bark and leaves); 0.5 to 2.5% w/v (Citrullus colocynthis); 0.1 to 0.4% w/v (Cucumis sativus): 82-97% w/v of carrier or additive.

There are disadvantages associated with the herbal tooth paste known in the prior art. One of the disadvantages is that the conventional herbal tooth paste comprises only few herbs and therefore is incapable of taking due oral care.
Another disadvantages is that so many useful herbs have not been used so far and therefore the toothpaste is not capable to clean the teeth and gums completely.
Yet another disadvantages is that the convention tooth paste are incapable to keep oral cleanness and freshness for a long time.
Therefore, there is a need to develop an herbal tooth paste comprising aloe vera and other efficacious natural and active herbs for oral care.
OBJECTIVE OF THE INVENTION
Therefore, an object of the present invention is to provide an herbal composition for oral care which obviates the disadvantages associated with the prior art.
Another object of the present invention is to provide an herbal composition for oral care which is safe to use orally as the components used in the oral care composition are of herbal origin.
Yet another object of the present invention is to provide an herbal composition for oral care which do not have any adverse effect on the teeth and gums.
Still another object of the present invention is to provide an herbal composition for oral care which can be prepared in the form of paste, powder, gel, liquid and / or crystal.
Further object of the present invention is to provide a process for the preparation of herbal composition for oral care.

Another object of the present invention is to provide an herbal composition for complete oral care which is eco-friendly and economically viable.
STATEMENT OF THE INVENTION
According to this invention there is provided an herbal composition for complete oral care comprising 0.01 - 1 % by weight of neem bark extract, 0.01 - 1 % by weight of vajradanti extract, 0.01 - 1 % by weight of bakul (moulsari) extract, 0.01
- 1 % by weight of majufal extract, 0.01 - 1 % by weight of vidang extract, 0.01 - 1 % by weight of babool bark extract, 0.01 - 1 % by weight of pilu bark extract, 0.01
- 1 % by weight of tomar seed extract, 0.01 - 1 % by weight of pudina leaf extract, 0.01 - 1 % long bud extract, 0.01 - 1 % by weight of haldi rhizome extract, 0.01 -1 % by weight of pipli chhoti fruit extract and 0.01 - 1 % by weight of akarkara root extract, 0.01 to 1 % by weight Sodium Benzoate, 15-22 % by weight Sorbitol 70 %, 4.05 - 8.05 % by weight Glycerine, 0.1-1 % by weight Polyethylene Glycol (PEG) - 400, 0.2 - 1 % by weight Sodium Saccharin, 0.01 - 1 % by weight Sodium monofluorophosphate (SMFP), 0.1-1 % by weight Tri Sodium Ortho Phosphate (TSOP), 0.01 - 1 % by weight Sphatic Bhasma, 2.03 - 4 % by weight Thickening silica ppt, 35 - 45 % by weight Calcium Carbonate, 0.1 - 0.1 % by weight Zinc Citrate, 0.2 - 1 % by weight Sodium CMC, 1.5-3 % by weight Sodium Lauryl Sulphate (SLS) Needles, 0.1 - 0.2 % by weight Flavour (Divya dhara) menthol and rest of the demineralized water.
Further according to this invention there is provided an herbal composition for complete oral care comprising;
a. Charging required quantity of demineralized (DM) water in a vessel and heating the same to a temperature of 80-100 °C, adding herbal extracts,

for example, 0.01 -1 % by weight of neem bark extract, 0.01 -1 % by weight of vajradanti extract, 0.01 - 1 % by weight of bakul (moulsari) extract, 0.01 - 1 % by weight of majufal extract, 0.01 - 1 % by weight of vidang extract, 0.01 - 1 % by weight of babool bark extract, 0.01 - 1 % by weight of pilu bark extract, 0.01 - 1 % by weight of tomar seed extract, 0.01 - 1 % by weight of pudina leaf extract, 0.01 - 1 % long bud extract, 0.01 - 1 % by weight of haldi rhizome extract, 0.01 - 1 % by weight of pipli chhoti fruit extract and 0.01 - 1 % by weight of akarkara root extract, under continuous stirring for a period of 50 to 80 minutes so as to obtain a homogenous solution,
b. Adding 15-22 % by weight Sorbitol 70 %, 4.05 - 8.05 % by weight
Glycerine, 0.1-1 % by weight Polyethylene Glycol (PEG) - 400, 0.2 - 1 %
by weight Sodium Saccharin, 0.01 - 1 % by weight Sodium
monofluorophosphate (SMFP), 0.1-1 % by weight Tri Sodium Ortho
Phosphate (TSOP) in the said vessel under continuous stirring with scrapper
for 20 - 40 minutes at 55 - 85 °C and under vacuum at 500 - 800 mmHg,
c. Adding 0.1-1 % by weight Aspatic Bhasma with processed water in the
main vessel under stirring for 5 - 15 minutes at 55 - 80°C,
d. Charging premix 2.03 - 4.95 % by weight Silica ppt., 35 - 45 % by weight
Calcium carbonate, 0.2 - 1 % by weight Sodium CMC and 0.1 - 0.1 % by
weight Zinc citrate in the main vessel under continuous stirring for 30 - 60
minutes at a temperature of 45 - 70°C under vacuum at 500 - 800 mmHg.
e. Charging 1.5-3 % by weight SLS Needle into the main vessel under stirring
for a period of 10 - 30 minutes at a temperature of 50 - 70°C, maintain
vacuum at 500 - 800 mmHg,

f. Cooling the product to less than 40 ° C and de-aerating the same under 500
- 800 mmHg for 40 - 60 minutes,
g. Adding 0.1 - 0.2 % by weight Divya Dhara & Flavour / menthol under
continuous stirring for 10 - 30 minutes to obtain the product,
BRIEF DESCRIPTION OF THE INVENTION
An herbal composition for complete oral care according to a preferred embodiment of the present invention is herein described in the following description and illustrated in the accompanying examples.
DESCRIPTION OF THE INVENTION
According to this invention an herbal composition for complete oral care comprises active ingredients, for example, 0.01 -1 % by weight of neem bark extract, 0.01 -1 % by weight of vajradanti extract, 0.01 -1 % by weight of bakul (moulsari) extract, 0.01 - 1 % by weight of majufal extract, 0.01 - 1 % by weight of vidang extract, 0.01 - 1 % by weight of babool bark extract, 0.01 - 1 % by weight of pilu bark extract, 0.01 - 1 % by weight of tomar seed extract, 0.01 - 1 % by weight of pudina leaf extract, 0.01 - 1 % long bud extract, 0.01 - 1 % by weight of haldi rhizome extract, 0.01 -1 % by weight of pipli chhoti fruit extract and 0.01 -1 % by weight of akarkara root extract, and base ingredients, for example 0.01 to 1 % by weight Sodium Benzoate, 15-22 % by weight Sorbitol 70 %, 4.05 - 8.05 % by weight Glycerine, 0.1-1 % by weight Polyethylene Glycol (PEG) - 400, 0.2 - 1 % by weight Sodium Saccharin, 0.01 - 1 % by weight Sodium monofluorophosphate (SMFP), 0.1-1 % by weight Tri Sodium Ortho Phosphate (TSOP), 0.01 - 1 % by weight Sphatic Bhasma, 2.03 - 4 % by weight Thickening silica ppt, 35 - 45 % by weight Calcium Carbonate, 0.1 - 0.1 % by weight Zinc Citrate, 0.2 - 1 % by weight Sodium CMC,

1.5 - 3 % by weight Sodium Lauryl Sulphate (SLS) Needles, 0.1 - 0.2 % by weight Flavour (Divya dhara) menthol and rest of the demineralized water.
The process for the preparation of herbal toothpaste for oral care, according to this invention, comprises;
a. Charge required quantity of demineralized (DM) water in a vessel and heat
it up to a temperature of 80 - 100 °C. Add herbal extracts, for example, 0.01
- 1 % by weight of neem bark extract, 0.01 - 1 % by weight of vajradanti extract, 0.01 -1 % by weight of bakul (moulsari) extract, 0.01 -1 % by weight of majufal extract, 0.01 - 1 % by weight of vidang extract, 0.01 - 1 % by weight of babool bark extract, 0.01 - 1 % by weight of pilu bark extract, 0.01
- 1 % by weight of tomar seed extract, 0.01 - 1 % by weight of pudina leaf extract, 0.01 - 1 % long bud extract, 0.01 - 1 % by weight of haldi rhizome extract, 0.01 - 1 % by weight of pipli chhoti fruit extract and 0.01 - 1 % by weight of akarkara root extract, under continuous stirring at a speed of 2200
- 3200 rpm for a period of 50 to 80 minutes at a temperature of 50 - 90 °C so as to obtain a homogenous solution,
b. Add 15-22 % by weight Sorbitol 70 %, 4.05 - 8.05 % by weight Glycerine,
0.1-1 % by weight Polyethylene Glycol (PEG) - 400, 0.2 - 1 % by weight
Sodium Saccharin, 0.01 - 1 % by weight Sodium monofluorophosphate
(SMFP), 0.1-1 % by weight Tri Sodium Ortho Phosphate (TSOP), under
continuous stirring with scrapper for 20 - 40 minutes at 55 - 85 °C and under
vacuum at 500 - 800 mmHg,
c. Add 0.1-1 % by weight Aspatic Bhasma with processed water is added into
the main vessel under stirring for 5 - 15 minutes at 55 - 80°C,

d. Charge premix 2.03 - 4.95 % by weight Silica ppt., 35 - 45 % by weight
Calcium carbonate, 0.2 - 1 % by weight Sodium CMC and 0.1 - 0.1 % by
weight Zinc citrate into the main vessel under continuous stirring for 30 - 60
minutes at a temperature of 45 - 70°C under vacuum at 500 - 800 mmHg.
e. Charge 1.5-3 % by weight SLS Needle into the main vessel under stirring
for a period of 10 - 30 minutes at a temperature of 50 - 70°C, maintain
vacuum at 500 - 800 mmHg,
f. Cool the product to less than 40 ° C and de-aerate under 500 - 800 mmHg
for 40-60 minutes,
g. Add 0.1-0.2 % by weight Divya Dhara & Flavour / menthol under continuous
stirring for 10 - 30 minutes to obtain the product,
h. Check the product so obtained for QC and fill the same in the tubes for sale.
The herbal composition for oral care and a process for the preparation thereof is described herein below with the help of the following example.
Example -1
a. 39.86 kg demineralized (DM) water was added in a vessel and heated up to a temperature of 90 °C. 0.01 kg neem bark extract, 0.01 kg vajradanti extract, 0.01 kg bakul (moulsari) extract, 0.01 kg majufal extract, 0.01 kg vidang extract, 0.01 kg babool bark extract, 0.01 kg pilu bark extract, 0.01 kg tomar seed extract, 0.01 kg pudina leaf extract, 0.01 kg long bud extract, 0.01 kg haldi rhizome extract, 0.01 kg pipli chhoti fruit extract and 0.01 kg akarkara root extract were added under continuous stirring at a speed of 2200 - 3200 rpm for a period of 50 to 80 minutes at a temperature of 50 - 90 °C so as to obtain a homogenous solution,

b. 15 kg Sorbitol 70 %, 4 kg Glycerine, 0.5 kg polyethylene Glycol (PEG) - 400,
0.45 kg Sodium Saccharin, 0.07 kg Sodium monofluorophosphate (SMFP),
0.1 kg Tri Sodium Ortho Phosphate (TSOP) were added in the above
solution under continuous stirring with scrapper for 30 minutes at 70 °C and
under vacuum at 650 mmHg,
c. 0.1 Kg Aspatic Bhasma with processed water was added in the main vessel
under stirring for 10 minutes at 70 °C.
d. premixof 3 kg thickening Silica ppt, 35 kg Calcium carbonate, 0.2 kg Sodium
CMC and 0.1 Kg Zinc citrate was added in the main vessel under continuous
stirring for 45 minutes at a temperature of 60 °C under vacuum 650 mmHg.
e. 1.5 kg SLS Needle was added into the main vessel under stirring for a period
of 20 minutes at a temperature of 60 °C, maintain vacuum at 650 mmHg.
f. the product so obtained was cooled to less than 40 ° C and de-aerate under
650 mmHg for 50 minutes.
g. 0.1 kg Divya Dhara & flavours were added into the product under continuous
stirring for 20 minutes to obtain the product.
h. The final product is checked for QC and filled in the tubes for sale.
Example - 2
a. 11.7 kg demineralized (DM) water was added in a vessel and heated up to a temperature of 90 °C. 0.01 kg neem bark extract, 0.01 kg vajradanti extract, 0.01 kg bakul (moulsari) extract, 0.05 kg maju fal extract, 0.01 kg vidang extract, 0.2 kg babool bark extract, 0.01 kg pilu bark extract, 0.02 kg tomar seed extract, 0.01 kg pudina leaf extract, 0.01 kg long bud extract, 0.01 kg haldi rhizome extract, 0.01 kg pipli chhoti fruit extract and 0.2 kg akarkara root extract were added under continuous stirring at a speed of 2200 - 3200

rpm for a period of 50 to 80 minutes at a temperature of 50 - 90 °C so as to obtain a homogenous solution,
b. 18 kg Sorbitol 70 %, 6 kg Glycerine, 0.5 kg polyethylene Glycol (PEG) - 400,
0.45 kg Sodium Saccharin, 0.07 kg Sodium monofluorophosphate (SMFP),
0.3 kg Tri Sodium Ortho Phosphate (TSOP) were added in the above
solution under continuous stirring with scrapper for 30 minutes at 70 °C and
under vacuum at 650 mmHg,
c. 0.3 Kg Aspatic Bhasma with processed water was added in the main vessel
under stirring for 10 minutes at 70 °C.
d. premix of 5 kg thickening Silica ppt., 50 kg Calcium carbonate, 1 kg Sodium
CMC and 1 Kg Zinc citrate was added in the main vessel under continuous
stirring for 45 minutes at a temperature of 60 °C under vacuum 650 mmHg.
e. 3 kg SLS Needle was added into the main vessel under stirring for a period
of 20 minutes at a temperature of 60 °C, maintain vacuum at 650 mmHg.
f. the product so obtained was cooled to less than 40 ° C and de-aerate under
650 mmHg for 50 minutes.
g. 0.2 kg Divya Dhara & flavours were added into the product under continuous
stirring for 20 minutes to obtain the product.
h. The final product is checked for QC and filled in the tubes for sale.
Certain features of the invention have been described with reference to the example embodiments. However, the description is not intended to be construed in a limiting sense. Various modifications of the example embodiments as well as other embodiments of the invention, which are apparent to the persons skilled in the art to which the invention pertains, are deemed to lie within the spirit and scope of the invention.

We Claim:
1. Herbal composition for complete oral care comprising 0.01 -1 % by weight of neem bark extract, 0.01 - 1 % by weight of vajradanti extract, 0.01 - 1 % by weight of bakul (moulsari) extract, 0.01 - 1 % by weight of majufal extract, 0.01 - 1 % by weight of vidang extract, 0.01 - 1 % by weight of babool bark extract, 0.01 - 1 % by weight of pilu bark extract, 0.01 - 1 % by weight of tomar seed extract, 0.01 - 1 % by weight of pudina leaf extract, 0.01 - 1 % long bud extract, 0.01 - 1 % by weight of haldi rhizome extract, 0.01 - 1 % by weight of pipli chhoti fruit extract and 0.01 - 1 % by weight of akarkara root extract, 0.01 to 1 % by weight Sodium Benzoate, 15-22 % by weight Sorbitol 70 %, 4.05 - 8.05 % by weight Glycerine, 0.1-1 % by weight Polyethylene Glycol (PEG) - 400, 0.2 - 1 % by weight Sodium Saccharin, 0.01 - 1 % by weight Sodium monofluorophosphate (SMFP), 0.1-1 % by weight Tri Sodium Ortho Phosphate (TSOP), 0.01 - 1 % by weight Sphatic Bhasma, 2.03 - 4 % by weight Thickening silica ppt, 35 - 45 % by weight Calcium Carbonate, 0.1 - 0.1 % by weight Zinc Citrate, 0.2 - 1 % by weight Sodium CMC, 1.5-3 % by weight Sodium Lauryl Sulphate (SLS) Needles, 0.1 - 0.2 % by weight Flavour (Divya dhara) menthol and rest of the demineralized water.
2. A process for the preparation of an herbal toothpaste for oral care comprising;
a. Charging required quantity of demineralized (DM) water in a vessel and heating the same to a temperature of 80 - 100 °C, adding herbal extracts, for example, 0.01 - 1 % by weight of neem bark extract, 0.01 - 1 % by weight of vajradanti extract, 0.01 - 1 % by weight of bakul (moulsari)

extract, 0.01 - 1 % by weight of majufal extract, 0.01 - 1 % by weight of vidang extract, 0.01 - 1 % by weight of babool bark extract, 0.01 - 1 % by weight of pilu bark extract, 0.01 - 1 % by weight of tomar seed extract, 0.01 - 1 % by weight of pudina leaf extract, 0.01 - 1 % long bud extract, 0.01 - 1 % by weight of haldi rhizome extract, 0.01 - 1 % by weight of pipli chhoti fruit extract and 0.01 -1 % by weight of akarkara root extract, under continuous stirring for a period of 50 to 80 minutes so as to obtain a homogenous solution,
b. Adding 15-22 % by weight Sorbitol 70 %, 4.05 - 8.05 % by weight
Glycerine, 0.1-1 % by weight Polyethylene Glycol (PEG) - 400, 0.2 - 1
% by weight Sodium Saccharin, 0.01 - 1 % by weight Sodium
monofluorophosphate (SMFP), 0.1-1 % by weight Tri Sodium Ortho
Phosphate (TSOP) in the said vessel under continuous stirring with
scrapper for 20 - 40 minutes at 55 - 85 °C and under vacuum at 500 -
800 mmHg,
c. Adding 0.1-1 % by weight Aspatic Bhasma with processed water in the
main vessel under stirring for 5 - 15 minutes at 55 - 80°C,
d. Charging premix 2.03-4.95 % by weight Silica ppt., 35-45 % by weight
Calcium carbonate, 0.2 - 1 % by weight Sodium CMC and 0.1 - 0.1 %
by weight Zinc citrate in the main vessel under continuous stirring for 30
- 60 minutes at a temperature of 45 - 70°C under vacuum at 500 - 800
mmHg.
e. Charging 1.5-3 % by weight SLS Needle into the main vessel under
stirring for a period of 10 - 30 minutes at a temperature of 50 - 70°C,
maintain vacuum at 500 - 800 mmHg,

f. Cooling the product to less than 40 ° C and de-aerating the same under
500 - 800 mmHg for 40 - 60 minutes,
g. Adding 0.1 - 0.2 % by weight Divya Dhara & Flavour / menthol under
continuous stirring for 10 - 30 minutes to obtain the product.
3. A process for the preparation of an herbal composition for complete oral care as claimed in claim 2, wherein the step of stirring is done at a speed of 2200 -3200rpm.
4. A process for the preparation of an herbal composition for complete oral care as claimed in claim 2, wherein the step of stirring is done at a temperature of 50 - 90 °C.