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"A Method Of Producing Magnetic Nano Materials For Forming A Solid Core For Transformer With High Saturation Magnetic Flux Density Including Zero Hysteresis Loss"

Abstract: The present invention relates to a method of producing magnetic nano materials for forming a solid core for transformer with high saturation magnetic flux density including zero hysteresis toss, the method comprising the steps of preparing nano powder sample of Fe70Co30-SiO2 by Co-precipitation combined with H2 reduction process, wherein FeCl2.4H2O and CoCl2.6H2O is dissolved in equal proportion in de-ionized water the molar ratio of Fe2+ to Co2+ being about 70:30, wherein NaOH solution is introduced with rapid stirring to maintain the pH value in the range of 12

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Notices, Deadlines & Correspondence

Patent Information

Application #
Filing Date
16 March 2012
Publication Number
35/2016
Publication Type
INA
Invention Field
PHYSICS
Status
Email
Parent Application
Patent Number
Legal Status
Grant Date
2022-03-04
Renewal Date

Applicants

TATA STEEL LIMITED
RESEARCH AND DEVELOPMENT AND SCIENTIFIC SERVICES DIVISION, JAMSHEDPUR-831001, INDIA.

Inventors

1. KRISHNA SABAREESH R
C/O. TATA STEEL LIMITED RESEARCH AND DEVELOPMENT AND SCIENTIFIC SERVICES DIVISION, JAMSHEDPUR-831001, INDIA.
2. SUMITESH DAS
C/O. TATA STEEL LIMITED RESEARCH AND DEVELOPMENT AND SCIENTIFIC SERVICES DIVISION, JAMSHEDPUR-831001, INDIA.

Specification

FIELD OF THE INVENTION The present invention relates to a method for producing a transformer core formed of magnetic nano materials having very high saturation magnetic flux density and almost zero hysteresis loss. The invention further relates to an improved transformer with solid core formed of Fe70Co30 nanomaterials encapsulated with SiO2. BACKGROUND OF THE INVENTION It is known that a transformer is a device that transfers electrical energy from one circuit to another through inductively coupled coils. It works on the principle of electromagnetic induction. A varying alternating current applied in the primary winding of the transformer creates a varying magnetic flux in the transformer's core which in turn creates a varying magnetic field through the secondary winding. This varying magnetic field induces a varying electromotive force (EMF), in the secondary winding. Soft magnetic materials with low coercivity are major components of electromagnetic devices such as transformers, magnetic sensors, step motors, and magnetic recording heads. The miniaturization of such devices needs materials that can develop higher saturation magnetic flux density, so that the necessary flux densities can be obtained with reduced device dimensions, while simultaneously possessing a low coercivity. In conventional transformers, the primary and secondary coils are wound on the core, which is made of laminated grain oriented silicon steel. The magnetic flux density presently possible with these transformers is about 1.6 Tesla. Magnetic alloy materials, such as FePt, CoPt, FeCo and NiCo, have been widely studied because of their multiple functionalities as well as extensive applications [1-4]. FeCo is an intermetallic compound and it is a soft magnetic material with unique properties such as large permeability, low magnetostriction, high Curie temperature, small cohesive forces and largest saturation magnetization [5]. FeCo nanocrystals are building blocks of many magnetic materials and thin films [6-8]. They can also be used in biomedical systems [9]. Among the FeCo nanomaterials, it has been estimated that Fe70Co30 has the maximum saturation magnetic flux density. These nanomaterials are coated with SiO2 to prevent agglomeration of magnetic nanomaterials [10]. The non-patent literature published on 27.03.2007 entitled "structure and magnetic properties of FeCo-SiO2 nanocomposite synthesized by wet chemical method", by Xue gang Lu et al teaches a soft magnetic nanocomposite with FeCo particles encapsulated by amorphous SiO2 was synthesized using a co- precipitation combined H2 reduction method. The saturation magnetization of the (Fe70Co30)(SiO2)10 nanocomposite is as high as 200 emu/g, which is 4-5 times larger than that of traditional spinel ferrites. The frequency dependence of the complex initial permeability is intensely dependent upon the content of SiO2 insulating phase. With increasing the content of SiO2 to 10 wt.%, the cut-off frequency is drastically increased to over 1 GHz. The results show that a new high-frequency soft magnetic material with high saturation manetization (Ms) can be achieved by introducing FeCo/SiO2 nanocomposite. US2010040503 describes a soft magnetic alloy that in an FeCo nanocrystal soft magnetic material, exhibits a high saturation magnetic flux density of 1.85 T or more, and that ensures prolonged nozzle life and easy ribbon production; an amorphous alloy ribbon for use in production thereof; and magnetic parts utilizing the soft magnetic alloy. The soft magnetic alloy has the composition of the formula Fe100-x-y-aCoaCuxBy (in the formula, x, y and a each represent atomic % and satisfy the relationships 1

Documents

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Section Controller Decision Date

Application Documents

# Name Date
1 298-Kol-2012-(16-03-2012)SPECIFICATION.pdf 2012-03-16
1 298-KOL-2012-13-09-2023-CORRESPONDENCE.pdf 2023-09-13
2 298-Kol-2012-(16-03-2012)GPA.pdf 2012-03-16
2 298-KOL-2012-13-09-2023-FORM-27.pdf 2023-09-13
3 298-KOL-2012-13-09-2023-POWER OF ATTORNEY.pdf 2023-09-13
3 298-Kol-2012-(16-03-2012)FORM-3.pdf 2012-03-16
4 298-KOL-2012-Response to office action [20-05-2023(online)].pdf 2023-05-20
4 298-Kol-2012-(16-03-2012)FORM-2.pdf 2012-03-16
5 298-KOL-2012-PROOF OF ALTERATION [21-02-2023(online)].pdf 2023-02-21
5 298-Kol-2012-(16-03-2012)FORM-1.pdf 2012-03-16
6 298-KOL-2012-IntimationOfGrant04-03-2022.pdf 2022-03-04
6 298-Kol-2012-(16-03-2012)DRAWINGS.pdf 2012-03-16
7 298-KOL-2012-PatentCertificate04-03-2022.pdf 2022-03-04
7 298-Kol-2012-(16-03-2012)DESCRIPTION (COMPLETE).pdf 2012-03-16
8 298-KOL-2012-Written submissions and relevant documents [22-12-2021(online)].pdf 2021-12-22
8 298-Kol-2012-(16-03-2012)CORRESPONDENCE.pdf 2012-03-16
9 298-Kol-2012-(16-03-2012)CLAIMS.pdf 2012-03-16
9 298-KOL-2012-Correspondence to notify the Controller [06-12-2021(online)].pdf 2021-12-06
10 298-Kol-2012-(16-03-2012)ABSTRACT.pdf 2012-03-16
10 298-KOL-2012-US(14)-HearingNotice-(HearingDate-09-12-2021).pdf 2021-11-09
11 298-KOL-2012-(20-06-2013)-PETITION UNDER RULE 137.pdf 2013-06-20
11 298-KOL-2012-COMPLETE SPECIFICATION [03-09-2019(online)].pdf 2019-09-03
12 298-KOL-2012-(20-06-2013)-OTHERS.pdf 2013-06-20
12 298-KOL-2012-DRAWING [03-09-2019(online)].pdf 2019-09-03
13 298-KOL-2012-(20-06-2013)-FORM-5.pdf 2013-06-20
13 298-KOL-2012-FER_SER_REPLY [03-09-2019(online)].pdf 2019-09-03
14 298-KOL-2012-(20-06-2013)-FORM-13.pdf 2013-06-20
14 298-KOL-2012-OTHERS [03-09-2019(online)].pdf 2019-09-03
15 298-KOL-2012-(20-06-2013)-FORM-1.pdf 2013-06-20
15 298-KOL-2012-FER.pdf 2019-03-12
16 298-KOL-2012-(20-06-2013)-ASSIGNMENT.pdf 2013-06-20
16 298-KOL-2012-(20-06-2013)-CORRESPONDENCE.pdf 2013-06-20
17 298-KOL-2012-(20-06-2013)-CORRESPONDENCE.pdf 2013-06-20
17 298-KOL-2012-(20-06-2013)-ASSIGNMENT.pdf 2013-06-20
18 298-KOL-2012-(20-06-2013)-FORM-1.pdf 2013-06-20
18 298-KOL-2012-FER.pdf 2019-03-12
19 298-KOL-2012-(20-06-2013)-FORM-13.pdf 2013-06-20
19 298-KOL-2012-OTHERS [03-09-2019(online)].pdf 2019-09-03
20 298-KOL-2012-(20-06-2013)-FORM-5.pdf 2013-06-20
20 298-KOL-2012-FER_SER_REPLY [03-09-2019(online)].pdf 2019-09-03
21 298-KOL-2012-(20-06-2013)-OTHERS.pdf 2013-06-20
21 298-KOL-2012-DRAWING [03-09-2019(online)].pdf 2019-09-03
22 298-KOL-2012-(20-06-2013)-PETITION UNDER RULE 137.pdf 2013-06-20
22 298-KOL-2012-COMPLETE SPECIFICATION [03-09-2019(online)].pdf 2019-09-03
23 298-Kol-2012-(16-03-2012)ABSTRACT.pdf 2012-03-16
23 298-KOL-2012-US(14)-HearingNotice-(HearingDate-09-12-2021).pdf 2021-11-09
24 298-KOL-2012-Correspondence to notify the Controller [06-12-2021(online)].pdf 2021-12-06
24 298-Kol-2012-(16-03-2012)CLAIMS.pdf 2012-03-16
25 298-KOL-2012-Written submissions and relevant documents [22-12-2021(online)].pdf 2021-12-22
25 298-Kol-2012-(16-03-2012)CORRESPONDENCE.pdf 2012-03-16
26 298-KOL-2012-PatentCertificate04-03-2022.pdf 2022-03-04
26 298-Kol-2012-(16-03-2012)DESCRIPTION (COMPLETE).pdf 2012-03-16
27 298-KOL-2012-IntimationOfGrant04-03-2022.pdf 2022-03-04
27 298-Kol-2012-(16-03-2012)DRAWINGS.pdf 2012-03-16
28 298-KOL-2012-PROOF OF ALTERATION [21-02-2023(online)].pdf 2023-02-21
28 298-Kol-2012-(16-03-2012)FORM-1.pdf 2012-03-16
29 298-KOL-2012-Response to office action [20-05-2023(online)].pdf 2023-05-20
29 298-Kol-2012-(16-03-2012)FORM-2.pdf 2012-03-16
30 298-KOL-2012-13-09-2023-POWER OF ATTORNEY.pdf 2023-09-13
30 298-Kol-2012-(16-03-2012)FORM-3.pdf 2012-03-16
31 298-Kol-2012-(16-03-2012)GPA.pdf 2012-03-16
31 298-KOL-2012-13-09-2023-FORM-27.pdf 2023-09-13
32 298-Kol-2012-(16-03-2012)SPECIFICATION.pdf 2012-03-16
32 298-KOL-2012-13-09-2023-CORRESPONDENCE.pdf 2023-09-13

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