Abstract: The instant disclosure provides a low total fatty matter (TFM) soap bar, which besides being cost effective, meets all the aesthetical and performance quality of conventional soap. The soap bar includes (a) at least one soap; (b) at least one surfactant; and (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; and (f) at least one humectant, wherein the at least one polyethylene glycol to the at least one humectant weight ratio is in the range of 1:40-1:70. The present disclosure also relates to a process of preparing the low total fatty matter soap bar.
FIELD OF THE INVENTION
[0001] The present disclosure relates to the field of personal care beauty products, in particular a sensorially superior low total fatty matter (TFM) soap bar and a process for preparation of the same. 5
BACKGROUND OF THE INVENTION
[0002] Soap bars are graded according to the content of total fatty matter (TFM). Toilet grade formulations contain high TFM are known as Grade 1 and Grade 2 formulations. There has been considerable research undertaken to reduce the TFM in
0 soap bars without majorly affecting their cleansing properties. Soap bars with high
surface active agents and low TFM contain low amount of sodium salt of fatty acids (C12–C18).
[0003] Soap bars with low TFM suffer from drawbacks such as reduced moisture retention, high cracking tendency, and soap breakage. Cracking of soap, also referred
5 to as wet-cracking is generally a result of repeated contact of soap bar with water and
subsequent drying; something that will inevitably happen when soap is used. In addition, there are many other factors that play a crucial role in cracking of soap which include shape of the bar, and process parameters involved in the manufacture of soap, such as extrusion temperature, imperfect mixing of components during extrusion, and
0 lower concentration of C12–C18 fatty acid salts. The cracks which develop on a soap
impart an unpleasant appearance to the soap bar. Moreover, at times, if the cracks develop sharp edges they can also be irritating, if not harmful, to the human skin, especially to the more tender parts. Thus, it is important to ensure that soaps are designed in such a way that they do not develop cracks on usage. Efforts in that
5 direction have been made in the past. One of the ways to tackle this peculiar problem
is addition of structurants to the soap. Different polysaccharides such as starches and celluloses have been used as structurants in order to address the above issue, but each one of them suffers from one limitation or the other.
[0004] Several attempts have been made in the past to reduce the amount of fatty acids
and various auxiliary and active substances.
[0005] WO2011080101 discloses a low TFM extruded personal washing bar
comprising a continuous phase, said continuous phase being substantially free of water
soluble detergent builder.
[0006] WO2010089269 discloses another low TFM extruded personal washing bar
comprising having a continuous phase including 20% to less than 45% fatty acid soap
in which the fatty acid soap comprises at least 30% saturated fatty acid soaps based on
the total weight of the soap. Further, the inert fillers were tried to replace the fatty
acids and other essential substances, however, these attempts reduced the desired skin
feel and other sensorial properties.
[0007] WO2001/042418 and WO2006/094586 disclose the use of amorphous alumina
or inorganic aluminum silicates. Further, US6440908 discloses the use of borates as
fillers. Still further, US2007/0021314 and US2007/0155639 describe use of starch and
synthetic surfactants together with hydrocarbons, moisturizers and free fatty acid and
mixtures thereof.
[0008] WO2013076047 discloses a soap bar composition comprising, in addition to
fatty acid soap and other ingredients, such as an adjuvant selected from suitable
starchy materials such as natural starch (from corn, wheat, rice, potato, tapioca and the
like), pre-gelatinzed starch, various physically and chemically modified starches and
mixtures thereof.
[0009] However, it has been observed that starches, specifically cornstarch, when used
in soap bar formulations impart a drag feel during soap usage on body. Also, the fillers
like corn starch and kaolin affects the properties of the soap bar and may not be able to
impart the desired level of efficacy, with regards anti-cracking properties and sensorial
aesthetics.
[0010] There is a need for soap bars which do not have problems as mentioned in the
prior art. Moreover, it is desirable that soap bars should not suffer from the defect of
cracking and also have a composition which contains relatively low levels of the significantly more expensive components rendering the soap bar as cost effective. [0011] Accordingly, it is the object of the present invention to manufacture a soap bar using low cost raw materials without affecting the desired properties of soap bar.
SUMMARY OF THE INVENTION
[0012] In an aspect of present disclosure, there is provided a low total fatty matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; and (f) at least one humectant, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 – 1:70.
[0013] In an aspect of present disclosure, there is provided a process for the preparation of a low total fatty matter (TFM) soap bar, comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; and (f) at least one humectant, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 – 1:70, said process comprising the steps of (a) contacting at least one soap, at least one surfactant, at least one polyethylene glycol, at least one humectant, at least one binder, and at least one filler to obtain a mixture; (b) milling the mixture to obtain a uniform homogeneous product; (c) extruding the uniform homogeneous product to obtain plodded slug; and (d) cutting the plodded slug into a pre-determined size and stamping to obtain low total fatty matter (TFM) soap bar.
[0014] These and other features, aspects, and advantages of the present subject matter will be better understood with reference to the following description and appended claims. This summary is provided to introduce a selection of concepts in a simplified form. This summary is not intended to identify key features or essential features of the claimed subject matter, nor is it intended to be used to limit the scope of the claimed subject matter.
DETAILED DESCRIPTION OF THE INVENTION
[0015] Those skilled in the art will be aware that the present disclosure is subject to
variations and modifications other than those specifically described. It is to be
understood that the present disclosure includes all such variations and modifications.
The disclosure also includes all such steps, features, compositions and compounds
referred to or indicated in this specification, individually or collectively, and any and
all combinations of any or more of such steps or features.
Definitions:
[0016] For convenience, before further description of the present disclosure, certain
terms employed in the specification, and examples are collected here. These
definitions should be read in the light of the remainder of the disclosure and
understood as by a person of skill in the art. The terms used herein have the meanings
recognized and known to those of skill in the art, however, for convenience and
completeness, particular terms and their meanings are set forth below.
[0017] The articles “a”, “an” and “the” are used to refer to one or to more than one
(i.e., to at least one) of the grammatical object of the article.
[0018] The terms “comprise” and “comprising” are used in the inclusive, open sense,
meaning that additional elements may be included. It is not intended to be construed as
“consists of only”.
[0019] Throughout this specification, unless the context requires otherwise the word
“comprise”, and variations such as “comprises” and “comprising”, will be understood
to imply the inclusion of a stated element or step or group of element or steps but not
the exclusion of any other element or steps.
[0020] The term “including” is used to mean “including but not limited to”,
“including” and “including but not limited to” are used interchangeably.
[0021] Unless defined otherwise, all technical and scientific terms used herein have
the same meaning as commonly understood to one of ordinary skill in the art to which
this disclosure belongs. Although methods and materials similar or equivalent to those
described herein can be used in the practice or testing of the disclosure, the preferred
methods, and materials are now described. All publications mentioned herein are incorporated herein by reference.
[0022] The term “soap noodles” refers to soap in the form of noodles. Soap noodles are made through the blending of oils, with base, such as caustic soda (NaOH) coupled with moisture (water) and other raw materials in minute (small) quantities. Soap noodles are made from vegetable oils, such as palm oil, coconut oil or olive oil, and/or animal fats (tallow). These are 'saponified', usually using sodium hydroxide, to form a sodium salt of the fatty acids. Soap noodles constitute the very basic form of soap. Different specifications of soap noodles are used depending on the type of soap to be manufactured e.g. toilet soap, laundry soap, translucent soaps, high-lather, medicated, etc. Soap noodles are blended with other raw materials such as fragrances and coloring to eventually make soap as the final product.
[0023] The term ‘stamping’ refers to the stamping step which is conducted during the formation of soap wherein around 50-60 or more bars per minute are stamped in a conventional soap line having several bars stamped in parallel. Stamping speed of 55-60 strokes/minute is considered as good stamping speed, whereas stamping speed of 30-35 strokes / minute is considered as disappointing.
[0024] Grade 2 soap is a soap with minimum 70 % total fatty matter and alcohol insoluble matters not more than 10%.
[0025] The present disclosure is not to be limited in scope by the specific embodiments described herein, which are intended for the purposes of exemplification only. Functionally equivalent products, compositions, and methods are clearly within scope of the disclosure, as described herein.
[0026] In order to tackle the problems mentioned in prior art, the present invention discloses formulations with low total fatty matter (TFM) which significantly reduce bar stickiness while maintaining the sensorial aesthetics provided by the soap bar. Moreover, the composition contains relatively low levels of the more expensive components, rendering the soap bar cost effective without compromising on the structural and sensorial attributes of the soap bar.
[0027] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c)
at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; and (f) at
least one humectant, wherein the at least one polyethylene glycol to at least one
humectant weight ratio is in the range of 1:40 – 1:70.
[0028] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the at least one polyethylene
glycol to at least one humectant weight ratio is in the range of 1:45 – 1:65.
[0029] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap comprises C12 to C18
fatty acid soaps.
[0030] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap comprises at least 75 %
w/w of C16 to C18 fatty acids and less than 25 % w/w of C12 to C14 fatty acids.
[0031] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap is grade 2 soap
comprising soap noodle having weight percentage of 92% with respect to the soap bar;
talc having weight percentage of 5% with respect to the soap bar; glycerin having
weight percentage of 2% with respect to the soap bar; and, fragrance having weight
percentage of 1% with respect to the soap bar.
[0032] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap bar comprises surfactant
having weight percentage in the range of 0.5-15% with respect to the soap bar.
[0033] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap bar comprises surfactant
having weight percentage in the range of 8-12% with respect to the soap bar.
[0034] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap bar comprises surfactant
having weight percentage of 10.1% with respect to the soap bar.
[0035] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, wherein the soap bar comprises surfactant having weight percentage of 10.5 % with respect to the soap bar.
[0036] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, wherein the surfactant is selected from the group consisting of alkyl sulfates, alkyl ether sulfates, alkyl glucosides, anionic acyl sarcosinates, N-acyl glutamates, alkyl sulfosuccinates, alkyl betaines, alpha olefin sulfonates, and combinations thereof. The alkyl sulfates contemplated by the present invention include C10-C16 alkyl sulfates; exemplified by compounds like sodium lauryl sulphate. Similarly, alkyl ether sulfates are sulfates derived from ethoxylated fatty alcohols. Examples include ammonium laureth sulfate, sodium laureth sulfate, ammonium myreth sulfate, sodium myreth sulfate, and sodium trideceth sulfate. Alkyl glucosides as described herein refer to C4-C20 alkyl glucosides, commonly used in cosmetic products, and exemplified by compounds like lauryl glucoside and decyl glucoside. Anionic acyl sarcosinates comprise C4 to C22 N-acyl sarcosinates; examples of which include compounds like oleoyl sarcosinate and lauroyl sarcosinate. N-acyl glutamates refer to salts of glutamic acid, wherein the alpha nitrogen of glutamic acid is acylated with an aliphatic acyl group of chain length between C10-C20, for example sodium/disodium lauroyl glutamate. These are well known in the art as mild surfactants. Alkyl sulfosuccinates refer to C4 - C20 alkyl esters of sulfosuccinic acid, exemplified by disodium laureth sulfosuccinate. Alkyl betaines contemplated by the present invention are the ones represented by general formula RN+(CH3)2CH2COO-, wherein R is an C4-C20 straight chain or a branched alkyl group. Alpha olefin sulfonates in context of the present invention comprise alkali metal salts of alpha olefin sulfonates, wherein the olefin carbon chain length is in the range of C4-C20. Examples include sodium C12-14 olefin sulfonate, sodium C14-16 olefin sulfonate, and sodium C14-18 olefin sulfonate. With reference to the definitions provided herein, any chain of carbon atoms includes both, straight chain as well as branched chains.
[0037] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the surfactant is alpha olefin
sulfonates
[0038] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap bar comprises
polyethylene glycol having weight percentage in the range of 0.005-0.05 % with
respect to the soap bar.
[0039] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap bar comprises
polyethylene glycol having weight percentage in the range of 0.010-0.04% with
respect to the soap bar.
[0040] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap bar comprises
polyethylene glycol having weight percentage in the range of 0.015-0.03% with
respect to the soap bar.
[0041] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap bar comprises
polyethylene glycol having weight percentage of 0.027% with respect to the soap bar.
[0042] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the polyethylene glycol is a high
molecular weight polyethylene glycol selected from the group consisting of PEG-2M,
PEG-5M, PEG-90M, PEG-7M, PEG-14M, PEG-32 M, PEG-45M, and combinations
thereof.
[0043] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the high molecular weight
polyethylene glycol is PEG-90M
[0044] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap bar comprises filler
having weight percentage in the range of 15-25% with respect to the soap bar.
[0045] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap bar comprises filler
having weight percentage in the range of 18-22% with respect to the soap bar.
[0046] . In an mbodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap bar comprises filler
having weight percentage of 20%with respect to the soap bar.
[0047] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the filler is talc
[0048] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap bar comprises binder
having weight percentage in the range of 0.5-4% with respect to the soap bar.
[0049] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap bar comprises binder
having weight percentage in the range of 1-3% with respect to the soap bar.
[0050] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap bar comprises binder
having weight percentage of 2% with respect to the soap bar.
[0051] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap bar comprises binder
having weight percentage of 1.85% with respect to the soap bar
[0052] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the binder is selected from the
group consisting of sodium silicate, calcium carbonate, aluminium silicate, and
combinations thereof
[0053] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the binder is sodium silicate.
[0054] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap bar comprises humectant
having weight percentage in the range of 0.5-5 % with respect to the soap bar.
[0055] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap bar comprises humectant
having weight percentage in the range of 1-3 % with respect to the soap bar.
[0056] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap bar comprises humectant
having weight percentage in the range of 1.3 % with respect to the soap bar.
[0057] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the soap bar comprises humectant
having weight percentage in the range of 1.7 % with respect to the soap bar.
[0058] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the humectant is selected from the
group consisting of glycerin, propylene glycol, sorbitol, and combinations thereof.
[0059] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the humectant is glycerin.
[0060] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, further comprising at least one
cosmetically acceptable excipient selected from the group consisting of salt,
emollients, opacifiers, preservatives, colors, fragrances, builder, and combinations
thereof.
[0061] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c)
at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at
least one humectant; and (g) at least one salt, wherein the at least one polyethylene
glycol to at least one humectant weight ratio is in the range of 1:40 – 1:70.
[0062] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c)
at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at
least one humectant; and (g) at least one salt, wherein the at least one polyethylene
glycol to at least one humectant weight ratio is in the range of 1:45 – 1:65.
[0063] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c)
at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at
least one humectant; and (g) at least one emollient, wherein the at least one
polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 –
1:70.
[0064] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c)
at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at
least one humectant; and (g) at least one emollient, wherein the at least one
polyethylene glycol to at least one humectant weight ratio is in the range of 1:45 –
1:65.
[0065] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c)
at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at
least one humectant; and (g) at least one opacifier, wherein the at least one
polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 –
1:70.
[0066] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c)
at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at
least one humectant; and (g) at least one opacifier, wherein the at least one
polyethylene glycol to at least one humectant weight ratio is in the range of 1:45 –
1:65.
[0067] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c)
at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at least one humectant; (g) at least one salt; (h) at least one emollient; and (i) at least one opacifier, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 – 1:70.
[0068] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at least one humectant; (g) at least one salt; (h) at least one emollient; and (i) at least one opacifier, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:45 – 1:65.
[0069] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at least one humectant; and (g) at least one preservative, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 – 1:70.
[0070] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at least one humectant; and (g) at least one preservative, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:45 – 1:65.
[0071] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at least one humectant; (g) at least one salt; (h) at least one emollient; (i) at least one opacifier; and (j) at least one preservative, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 – 1:70.
[0072] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at least one humectant; (g) at least one salt; (h) at least one emollient; (i) at least one opacifier; and (j) at least one preservative, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:45 – 1:65.
[0073] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at least one humectant; and (g) at least one color, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 – 1:70. [0074] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at least one humectant; and (g) at least one color, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:45 – 1:65. [0075] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at least one humectant; (g) at least one salt; (h) at least one emollient; (i) at least one opacifier; and (j) at least one preservative; and (k) at least one color, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 – 1:70.
[0076] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at least one humectant; (g) at least one salt; (h) at least one emollient; (i) at least one opacifier; and (j) at least one preservative; and (k) at least one color, wherein the at
least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:45 – 1:65.
[0077] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c)
5 at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at
least one humectant; and (g) at least one fragrance, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 – 1:70. [0078] In an embodiment of present disclosure, there is provided a low total fatty
0 matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c)
at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at least one humectant; and (g) at least one fragrance, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:45 – 1:65.
5 [0079] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at least one humectant; (g) at least one salt; (h) at least one emollient; (i) at least one opacifier; (j) at least one preservative; (k) at least one color; and (l) at least one
0 fragrance, wherein the at least one polyethylene glycol to at least one humectant
weight ratio is in the range of 1:40 – 1:70.
[0080] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at
5 least one humectant; (g) at least one salt; (h) at least one emollient; (i) at least one
opacifier; (j) at least one preservative; (k) at least one color; and (l) at least one fragrance, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:45 – 1:65.
[0081] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at least one humectant; and (g) at least one builder, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 – 1:70. [0082] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at least one humectant; and (g) at least one builder, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:45 – 1:65. [0083] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at least one humectant; (g) at least one salt; (h) at least one emollient; (i) at least one opacifier; (j) at least one preservative; (k) at least one color; (l) at least one fragrance; and (m) at least one builder, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 – 1:70.
[0084] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; (f) at least one humectant; (g) at least one salt; (h) at least one emollient; (i) at least one opacifier; (j) at least one preservative; (k) at least one color; (l) at least one fragrance; and (m) at least one builder, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:45 – 1:65.
[0085] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar comprising: (a) soap comprising at least 75% C16 to C18 fatty acids and less than 25% C12 to C14 fatty acids; (b) alpha olefin sulfonate; (c) polyethylene glycol-90M; (d) talc; (e) sodium silicate; (f) glycerin; (g) sodium chloride; (h) at least one emollient; (i) titanium dioxide; (j) at least one preservative;
(k) at least one color; (l) at least one fragrance; and (m) soda-ash,, wherein the polyethylene glycol-90M to glycerin weight ratio is in the range of 1:40 – 1:70. [0086] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar comprising: (a) soap comprising at least 75% C16 to C18 fatty acids and less than 25% C12 to C14 fatty acids; (b) alpha olefin sulfonate; (c) polyethylene glycol-90M; (d) talc; (e) sodium silicate; (f) glycerin; (g) sodium chloride; (h) at least one emollient; (i) titanium dioxide; (j) at least one preservative; (k) at least one color; (l) at least one fragrance; and (m) at least one builder, wherein the polyethylene glycol-90M to glycerin weight ratio is in the range of 1:45 – 1:65. [0087] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, (a) at least one soap having weight percentage in the range of 30-80% with respect to the soap bar; (b) at least one surfactant having weight percentage in the range of 0.5-15% with respect to the soap bar; (c) at least one polyethylene glycol having weight percentage in the range of 0.005-0.05% with respect to the soap bar; (d) at least one filler having weight percentage in the range of 15-25 % with respect to the soap bar; (e) at least one binder having weight percentage in the range of 0.5-4 % with respect to the soap bar; and (f) at least one humectant having weight percentage in the range of 0.5-5 % with respect to the soap bar.
[0088] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, (a) at least one soap having weight percentage in the range of 30-80% with respect to the soap bar; (b) at least one surfactant having weight percentage in the range of 0.5-15% with respect to the soap bar; (c) at least one polyethylene glycol having weight percentage in the range of 0.005-0.05% with respect to the soap bar; (d) at least one filler having weight percentage in the range of 15-25 % with respect to the soap bar; (e) at least one binder having weight percentage in the range of 0.5-4 % with respect to the soap bar; and (f) at least one humectant having weight percentage in the range of 0.5-5 % with respect
to the soap bar, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 – 1:70.
[0089] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, (a) at least one soap having weight percentage in the range of 30-80% with respect to the soap bar; (b) at least one surfactant having weight percentage in the range of 0.5-15% with respect to the soap bar; (c) at least one polyethylene glycol having weight percentage in the range of 0.005-0.05% with respect to the soap bar; (d) at least one filler having weight percentage in the range of 15-25 % with respect to the soap bar; (e) at least one binder having weight percentage in the range of 0.5-4 % with respect to the soap bar; and (f) at least one humectant having weight percentage in the range of 0.5-5 % with respect to the soap bar, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:45 – 1:65.
[0090] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, (a) soap comprising at least 75% C16 to C18 fatty acids and less than 25% C12 to C14 fatty acids, having weight percentage in the range of 30-80% with respect to the soap bar; (b) alpha olefin sulfonate having weight percentage in the range of 0.5-15% with respect to the soap bar; (c) polyethylene glycol-90M having weight percentage in the range of 0.005-0.05% with respect to the soap bar; (d) talc having weight percentage in the range of 15-25 % with respect to the soap bar; (e) sodium silicate having weight percentage in the range of 0.5-4 % with respect to the soap bar; and (f) glycerin having weight percentage in the range of 0.5-5 % with respect to the soap bar, wherein the polyethylene glycol-90M to glycerin weight ratio is in the range of 1:40 – 1:70.
[0091] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, (a) soap comprising at least 75% C16 to C18 fatty acids and less than 25% C12 to C14 fatty acids, having weight percentage in the range of 30-80% with respect to the soap bar; (b) alpha olefin sulfonate having weight percentage in the range of 0.5-15% with respect to the soap bar; (c)
polyethylene glycol-90M having weight percentage in the range of 0.005-0.05% with respect to the soap bar; (d) talc having weight percentage in the range of 15-25 % with respect to the soap bar; (e) sodium silicate having weight percentage in the range of 0.5-4 % with respect to the soap bar; and (f) glycerin having weight percentage in the range of 0.5-5 % with respect to the soap bar, wherein the polyethylene glycol-90M to glycerin weight ratio is in the range of 1:45 – 1:65.
[0092] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, (a) soap comprising at least 75% C16 to C18 fatty acids and less than 25% C12 to C14 fatty acids, having weight percentage in the range of 30-80% with respect to the soap bar; (b) alpha olefin sulfonate having weight percentage in the range of 0.5-15% with respect to the soap bar; (c) polyethylene glycol-90M having weight percentage in the range of 0.005-0.05% with respect to the soap bar; (d) talc having weight percentage in the range of 15-25 % with respect to the soap bar; (e) sodium silicate having weight percentage in the range of 0.5-4 % with respect to the soap bar; and (f) glycerin having weight percentage in the range of 0.5-5 % with respect to the soap bar, wherein the polyethylene glycol-90M to glycerin weight ratio is 1:48.
[0093] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, (a) soap comprising at least 75% C16 to C18 fatty acids and less than 25% C12 to C14 fatty acids, having weight percentage in the range of 30-80% with respect to the soap bar; (b) alpha olefin sulfonate having weight percentage in the range of 0.5-15% with respect to the soap bar; (c) polyethylene glycol-90M having weight percentage in the range of 0.005-0.05% with respect to the soap bar; (d) talc having weight percentage in the range of 15-25 % with respect to the soap bar; (e) sodium silicate having weight percentage in the range of 0.5-4 % with respect to the soap bar; and (f) glycerin having weight percentage in the range of 0.5-5 % with respect to the soap bar, wherein the polyethylene glycol-90M to glycerin weight ratio is 1:63.
[0094] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, (a) at least one soap having weight percentage in the range of 30-80% with respect to the soap bar; (b) at least one surfactant having weight percentage in the range of 0.5-15% with respect to the soap bar; (c) at least one polyethylene glycol having weight percentage in the range of 0.005-0.05% with respect to the soap bar; (d) at least one filler having weight percentage in the range of 15-25 % with respect to the soap bar; (e) at least one binder having weight percentage in the range of 0.5-4 % with respect to the soap bar; and (f) at least one humectant having weight percentage in the range of 0.5-5 % with respect to the soap bar, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:45 – 1:65.
[0095] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, (a) at least one soap having weight percentage in the range of 30-80% with respect to the soap bar; (b) at least one surfactant having weight percentage in the range of 0.5-15% with respect to the soap bar; (c) at least one polyethylene glycol having weight percentage in the range of 0.005-0.05% with respect to the soap bar; (d) at least one filler having weight percentage in the range of 15-25 % with respect to the soap bar; (e) at least one binder having weight percentage in the range of 0.5-4 % with respect to the soap bar; and (f) at least one humectant having weight percentage in the range of 0.5-5 % with respect to the soap bar; (g) at least one salt having weight percentage in the range of 0.1-2% with respect to the soap bar; (h) at least one emollient having weight percentage in the range of 0.1-2% with respect to the soap bar; (i) at least one opacifier having weight percentage in the range of 0.05-1% with respect to the soap bar; (j) at least one preservative having weight percentage in the range of 0.0001-0.1% with respect to the soap bar; (k) at least one colors having weight percentage in the range of 0.0001-0.1% with respect to the soap bar; (l) at least one fragrance having weight percentage in the range of 0.5-2% with respect to the soap bar; and (m) at least one builder having weight percentage in the range of 0.05-0.5 % with respect to the soap bar, wherein the
at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 – 1:70.
[0096] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, (a) at least one soap having weight percentage in the range of 30-80% with respect to the soap bar; (b) at least one surfactant having weight percentage in the range of 0.5-15% with respect to the soap bar; (c) at least one polyethylene glycol having weight percentage in the range of 0.005-0.05% with respect to the soap bar; (d) at least one filler having weight percentage in the range of 15-25 % with respect to the soap bar; (e) at least one binder having weight percentage in the range of 0.5-4 % with respect to the soap bar; and (f) at least one humectant having weight percentage in the range of 0.5-5 % with respect to the soap bar; (g) at least one salt having weight percentage in the range of 0.1-2% with respect to the soap bar; (h) at least one emollient having weight percentage in the range of 0.1-2% with respect to the soap bar; (i) at least one opacifier having weight percentage in the range of 0.05-1% with respect to the soap bar; (j) at least one preservative having weight percentage in the range of 0.0001-0.1% with respect to the soap bar; (k) at least one colors having weight percentage in the range of 0.0001-0.1% with respect to the soap bar; (l) at least one fragrance having weight percentage in the range of 0.5-2% with respect to the soap bar; and (m) at least one builder having weight percentage in the range of 0.05-0.5 % with respect to the soap bar, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:45 – 1:65.
[0097] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, wherein the salt is inorganic salt selected from the group consisiting of sodium chloride, magnesium sulfate, and combinations thereof.
[0098] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, wherein the salt is sodium chloride.
[0099] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the preservative is selected from
the group consisiting of phenoxyethanol; parabens; and methylisothiazolinone (and)
methyl paraben (and) phenoxyethanol (and) propyl paraben, and combinations thereof.
[0100] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the opacifier is selected from the
group consisting of titanium dioxide, zinc oxide, and combinations thereof.
[0101] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the emollient is selected from the
group consisting of hydrophilic emollients, hydrophobic emollients, and combinations
thereof.
[0102] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the hydrophilic emollients is
selected from the group consisting of glycerin, propylene glycol, water soluble or
dispersible alcohols or polyols, and combinations thereof.
[0103] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the hydrophobic emollients is
selected from the group consisting of fatty esters, triglycerides, silicones or other oil
soluble or oil dispersible types of materials, and combinations thereof.
[0104] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein the color is a dye selected from
the group consisting of nitroso, monoazo, diazo, carotenoid, triaryl methane, xanthene,
quinolone, azine, oxazine, anthraquinone, indigoid, thionindigoid, quinacridone,
phthalocyanine, and combinations thereof.
[0105] In an embodiment of present disclosure, there is provided a low total fatty
matter (TFM) soap bar as described herein, wherein fragrance is selected from the
group consisting of blend of essential oils, blend of synthetic aroma compounds, and
combinations thereof.
[0106] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, wherein builder is selected from the group consisting of carbonates, bicarbonates of sodium and potassium, sodium tripolyphosphates (STPP), tetra sodium pyrophosphates (TSPP), sodium phosphate, and combinations thereof
[0107] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, wherein builder is sodium carbonate (soda-ash).
[0108] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, further comprising water.
[0109] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, wherein binder to water weight ratio is in the range of 1:3-1:20.
[0110] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, wherein binder to water weight ratio is in the range of 1:5-1:15.
[0111] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, wherein sodium silicate to water weight ratio is in the range of 1:3-1:20.
[0112] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, wherein sodium silicate to water weight ratio is in the range of 1:5-1:15.
[0113] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, weight percentage of water in the soap sample is in the range of 15-20 % with respect to the soap bar.
[0114] In an embodiment of present disclosure, there is provided a low total fatty matter (TFM) soap bar as described herein, weight percentage of water in the soap sample is in the range of 16-18 % with respect to the soap bar.
[0115] In an embodiment of present disclosure, there is provided a process for the preparation of low total fatty matter (TFM) soap bar, comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; and (f) at least one humectant, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 – 1:70, said process comprising the steps of (a) contacting at least one soap, at least one surfactant, at least one polyethylene glycol, at least one humectant, at least one binder, and at least one filler to obtain a mixture; (b) milling the mixture to obtain a uniform homogeneous product; (c) extruding the uniform homogeneous product to obtain plodded slug; and (d) cutting the plodded slug into a pre-determined size and stamping to obtain low total fatty matter (TFM) soap bar.
[0116] In an embodiment of present disclosure, there is provided a process for the preparation of low total fatty matter (TFM) soap bar, comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; and (f) at least one humectant, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 – 1:70, said process comprising the steps of: (a) contacting at least one soap, at least one surfactant, at least one polyethylene glycol, at least one humectant, at least one binder, and at least one filler to obtain a mixture is carried out at a temperature in the range of 20-48 °C for a period in the range of 10-60 minutes; (b) milling the mixture at a temperature in the range of 6-10 °C to obtain a uniform homogeneous product; (c) extruding the uniform homogeneous product at a temperature in the range of 30-48 °C to obtained a plodded slug; and (d) cutting the plodded slug into a pre-determined size and stamping to obtain a low total fatty matter (TFM) soap bar.
[0117] In an embodiment of present disclosure, there is provided a process for the preparation of low total fatty matter (TFM) soap bar, comprising: (a) at least one soap; (b) at least one surfactant; (c) at least one polyethylene glycol; (d) at least one filler; (e) at least one binder; and (f) at least one humectant, wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 –
1:70, said process comprising the steps of: (a) contacting soap comprising at least 75% C16 to C18 fatty acids and less than 25% C12 to C14 fatty acids, alpha olefin sulfonate, polyethylene glycol-90M, talc, soda ash, sodium silicate, glycerin, and to obtain a mixture is carried out at a temperature in the range of 20-48 °C for a period in the range of 10-60 minutes; (b) milling the mixture at a temperature in the range of 6-10 °C to obtain a uniform homogeneous product; (c) extruding the uniform homogeneous product at a temperature in the range of 30-48 °C to obtained a plodded slug; and (d) cutting the plodded slug into a pre-determined size and stamping to obtain a low total fatty matter (TFM) soap bar.
EXAMPLES
[0118] The disclosure will now be illustrated with working examples, which is intended to illustrate the working of disclosure and not intended to take restrictively to imply any limitations on the scope of the present disclosure. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood to one of ordinary skill in the art to which this disclosure belongs. Although methods and materials similar or equivalent to those described herein can be used in the practice of the disclosed methods and compositions, the exemplary methods, devices and materials are described herein. It is to be understood that this disclosure is not limited to particular methods, and experimental conditions described, as such methods and conditions may apply.
Example 1
Materials and methods
[0119] Process for the preparation of soap bar: The soap bar was prepared by following process: soap comprising 85% of C16 to C18 fatty acids and 15% of C12 to C14 fatty acid was mixed with alpha olefin sulfonates (solid), alpha olefin sulfonates, PEG-90M, glycerin, sodium silicate, talc, soda ash, titanium dioxide, sodium chloride, and fragrance at a temperature in the range of 20 ᵒC to 48 ᵒC, for a period of 15
minutes to obtain a mixture. The mixture was milled at a temperature in the range of 6 ᵒC to 10 ᵒC by passing through rollers having chilled water circulation system, to obtain a uniform homogeneous product, which was extruded at a temperature in the range of 30 ᵒC to 48 ᵒC to obtain plodded slug. Subsequently, the slug was cut into a pre-determined size and stamped to obtain low total fatty matter soap bar.
Example 2
Soap bars with varying weight percentage of components:
[0120] Skin conditioning is important for consumers as they are bothered if their skin
feels dry as well as consumers are likely to be disappointed if their soap bar does not
last long enough, or if cracks appear too quickly while using the product.
[0121] PEG-90M acts as a foam booster, slip agent and is a water-soluble product
designed to reduce drag & impart a smooth, lubricious after-feel. Glycerin, a
humectant, exhibits good physical properties, and acts as a distinct additive offering
conditioning benefits. It was surprisingly found that the weight ratio of PEG-90:
glycerin is very critical for soap bars. The weight ratio 1:40- 1:70 of PEG-90 and
glycerin in soap bar provided for superior structural and sensorial attributes.
[0122] Different soap bars A, B, C, D, E, and F having compositions as shown in
Table 1 were prepared by a process as discussed in Example 1.
[0123] Table 1
[0124] The weight ratio of PEG-90M: glycerin in soap samples A, B and E falls outside the working range (1:40- 1:70). The aforementioned soap bar samples were sticky in nature which to a large extent affected the stamping efficiency. Additionally the sensorial attribute, i.e., the bar glide was less than the grade 2 benchmark soap. [0125] Bar soap samples C and D were formulated with talc as filler and PEG-90: glycerin weight ratio in the range of 1:40-1:70. Both the samples did not exhibit cracking, therefore not only the sensorial attributes of the soap bar increases but also there was increase in the long-lastingness of soap bars, addressing a major consumer concern of the end users.
[0126] Additional feature in the bar soap sample C and D was the silicate to water ratio. Sodium silicate acts as a binder in the low TFM soap bars having high moisture content and also makes the mass harder and non-sticky which aids for better processability of the soap bar. It was inferred with due experimentation that when the ratio of sodium silicate to water was in the range of 1:3 - 1:20 better results were observed with regards to processability.
[0127] Soap sample F had higher weight percentage of surfactant which led to a soft sticky soap mass in which stamping was difficult. With regards to soap bar property and sensorials lather volume was beyond standard requirements.
Example 3
Soap composition with corn starch and kaolin as binders:
[0128] Binders are also critical component in the manufacturing of soap bars. In order to determine whether the effect of binder in the soap bar, soap bar samples G and H were prepared with corn starch and kaolin as binders respectively as is exemplified in Table 2.
[0130] As is clear from Table 2, that the soap bar sample G, despite the ratio of PEG-90M : glycerin, in the working range, the substitution of binder talc by corn starch resulted in soap bar sample which had cracks in it as well as the sensorial aesthetics were also inferior compared to that of benchmark grade 2 soap.
[0131] With regards to soap bar sample H, kaolin was used as binder, which resulted in reduction of volume of lather and therefore the glide on skin reduced during use thereby reducing the sensorial likeability.
[0132] Thus, based on the aforementioned results of various experiments, it can be concluded that, in soap bars which comprise of high molecular weight PEG’s and glycerin in the weight ratio of 1:40 to 1:70, along with other excipients as mentioned in the working examples, are substantially superior; both structurally and sensorially. There was a significant reduction in bar stickiness while maintaining hardness within acceptable limits. Furthermore, the soap bars of the present invention are also cost effective, as low levels of the expensive components have been used.
[0133] Overall the disclosure provides for a low total fatty matter (TFM) soap bar which has structurally and sensorially superior aesthetics.
[0134] Although the subject matter has been described in considerable detail with reference to certain examples and implementations thereof, other implementations are possible.
Claims:1. A low total fatty matter (TFM) soap bar comprising:
a) at least one soap;
b) at least one surfactant;
c) at least one polyethylene glycol;
d) at least one filler;
e) at least one binder; and
f) at least one humectant,
wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 – 1:70.
2. The soap bar as claimed in claim 1, wherein the soap comprises C12 to C18 fatty acid soaps.
3. The soap bar as claimed in claim 2, wherein the soap comprises at least 75 weight % C16 to C18 fatty acids and less than 25 weight % C12 to C14 fatty acids.
4. The soap bar as claimed in claim 1, wherein the surfactant is selected from the group consisting of alkyl sulfates, alkyl ether sulfates, alkyl glucosides, anionic acyl sarcosinates, N-acyl glutamates, alkyl sulfosuccinates, alkyl betaines, alpha olefin sulfonates, and combinations thereof.
5. The soap bar as claimed in claim 4, wherein the surfactant is alpha olefin sulfonates.
6. The soap bar as claimed in claim 1, wherein the polyethylene glycol is a high molecular weight polyethylene glycol selected from the group consisting of PEG-2M, PEG-5M, PEG-90M, PEG-7M, PEG-14M, PEG-32 M, PEG-45M, and combinations thereof.
7. The soap bar as claimed in claim 6, wherein the high molecular weight polyethylene glycol is PEG-90M.
8. The soap bar as claimed in claim 1, wherein the filler is talc.
9. The soap bar as claimed in claim 1, wherein the binder is selected from the group consisting of sodium silicate, calcium carbonate, aluminium silicate, and combinations thereof.
10. The soap bar as claimed in claim 1, wherein the humectant is selected from the group consisting of glycerin, propylene glycol, sorbitol, and combinations thereof.
11. The soap bar as claimed in claim 1, further comprising at least one cosmetically acceptable excipient selected from the group consisting of salt, emollients, builders, opacifiers, preservatives, colors, fragrances, and combinations thereof.
12. A low total fatty matter (TFM) soap bar comprising:
a) at least one soap having weight percentage in the range of 30-80% with respect to the soap bar;
b) at least one surfactant having weight percentage in the range of 0.5-15% with respect to the soap bar;
c) at least one polyethylene glycol having weight percentage in the range of 0.005-0.05% with respect to the soap bar;
d) at least one filler having weight percentage in the range of 15-25 % with respect to the soap bar;
e) at least one binder having weight percentage in the range of 0.5-4 % with respect to the soap bar; and
f) at least one humectant having weight percentage in the range of 0.5-5 % with respect to the soap bar,
wherein the at least one polyethylene glycol to at least one humectant weight ratio is in the range of 1:40 – 1:70.
13. The soap bar as claimed in claim 1, further comprises water.
14. The soap bar as claimed in claim 13, wherein binder to water weight ratio is in the range of 1:3-1:20.
15. A process for the preparation of a low total fatty matter (TFM) soap bar as claimed in claim 1, said method comprising the steps of (a) contacting at least one soap, at least one surfactant, at least one polyethylene glycol, at least one humectant, at least one binder, and at least one filler to obtain a mixture; (b) milling the mixture to obtain a uniform homogeneous product; (c) extruding the uniform homogeneous product to obtain plodded slug; and (d) cutting the plodded slug into a pre-determined size, and stamping to obtain low total fatty matter (TFM) soap bar.
16. The process as claimed in claim 15, comprising the steps of: (a) contacting at least one soap, at least one surfactant, at least one polyethylene glycol, at least one humectant, at least one binder, and at least one filler at a temperature in the range of 20-48 °C for a period in the range of 10-60 minutes to obtain a mixture; (b) milling the mixture at a temperature in the range of 6-10 °C to obtain a uniform homogeneous product; (c) extruding the uniform homogeneous product at a temperature in the range of 30-48 °C to obtained a plodded slug; and (d) cutting the plodded slug into a pre-determined size and stamping to obtain a low total fatty matter (TFM) soap bar.
, Description:As Attached
| # | Name | Date |
|---|---|---|
| 1 | 201741000423-FER.pdf | 2021-10-17 |
| 1 | Form 5 [04-01-2017(online)].pdf | 2017-01-04 |
| 2 | 201741000423-FORM 18 [21-12-2020(online)].pdf | 2020-12-21 |
| 2 | Form 3 [04-01-2017(online)].pdf | 2017-01-04 |
| 3 | Correspondence by Applicant_Proof Of Right_05-05-2017.pdf | 2017-05-05 |
| 3 | Description(Complete) [04-01-2017(online)].pdf_226.pdf | 2017-01-04 |
| 4 | Description(Complete) [04-01-2017(online)].pdf | 2017-01-04 |
| 4 | Other Patent Document [04-05-2017(online)].pdf | 2017-05-04 |
| 5 | Form 26 [28-04-2017(online)].pdf | 2017-04-28 |
| 5 | Correspondence by Agent_Power of Attorney_03-05-2017.pdf | 2017-05-03 |
| 6 | Correspondence by Agent_Power of Attorney_03-05-2017.pdf | 2017-05-03 |
| 6 | Form 26 [28-04-2017(online)].pdf | 2017-04-28 |
| 7 | Description(Complete) [04-01-2017(online)].pdf | 2017-01-04 |
| 7 | Other Patent Document [04-05-2017(online)].pdf | 2017-05-04 |
| 8 | Correspondence by Applicant_Proof Of Right_05-05-2017.pdf | 2017-05-05 |
| 8 | Description(Complete) [04-01-2017(online)].pdf_226.pdf | 2017-01-04 |
| 9 | 201741000423-FORM 18 [21-12-2020(online)].pdf | 2020-12-21 |
| 9 | Form 3 [04-01-2017(online)].pdf | 2017-01-04 |
| 10 | Form 5 [04-01-2017(online)].pdf | 2017-01-04 |
| 10 | 201741000423-FER.pdf | 2021-10-17 |
| 1 | tpoE_03-02-2021.pdf |