Abstract: ABSTRACT An improved process for the preparation of 2-(3, 4-Dimethylphenyl)-5-methyI-lH-pyrazol-3(2H)-one having the structural formula (I).
WE CLAIM:
1. An improved process for the preparation of 2-(3, 4-Dimethylphenyl)-5-methyl-lH-pyrazol-3(2H)-one having the structural Formula I,
Formula I
which comprises:
1. condensation of 3,4-dimethylphenylhydrazine hydrochloride
3,4-Dimethylphenylhydrazine.HCl with ethyl acetoacetate in presence of suitable salt and solvent or mixture of organic solvents to obtained 2-(3, 4-dimethylphenyl)-5-methyl-lH-pyrazol-3(2H)-one compound of Formula I.
2. The process claimed in claim 1, wherein said base is selected from group consisting of sodium acetate, Ammonium acetate or Ammonium formate.
3. The process claimed in claim 1, wherein said solvent is selected from Aromatic, organic solvent or Alcoholic solvent
4. The process as claimed in claim 3, wherein aromatic organic solvents such as toluene, xylene or mixture of xylenes.
5. The process according to claim 3, wherein alcoholic solvents such as methanol, ethanol, n-butanol, propanol or isopropanol.
| # | Name | Date |
|---|---|---|
| 1 | 202141040285-Form5_As Filed_06-09-2021.pdf | 2021-09-06 |
| 1 | 401499-Form 27.pdf | 2023-11-20 |
| 2 | 202141040285-FORM 4 [30-10-2023(online)].pdf | 2023-10-30 |
| 2 | 202141040285-Form3_As Filed_06-09-2021.pdf | 2021-09-06 |
| 3 | 202141040285-Form28_Small Entity_06-09-2021.pdf | 2021-09-06 |
| 3 | 202141040285-FORM-26 [28-10-2023(online)].pdf | 2023-10-28 |
| 4 | 202141040285-IntimationOfGrant18-07-2022.pdf | 2022-07-18 |
| 4 | 202141040285-Form2 Title Page_Complete_06-09-2021.pdf | 2021-09-06 |
| 5 | 202141040285-PatentCertificate18-07-2022.pdf | 2022-07-18 |
| 5 | 202141040285-Form1_As Filed_06-09-2021.pdf | 2021-09-06 |
| 6 | 202141040285-Description Complete_As Filed_06-09-2021.pdf | 2021-09-06 |
| 6 | 202141040285-Abstract_FER Reply_14-03-2022.pdf | 2022-03-14 |
| 7 | 202141040285-Correspondence_MSME Certificate_06-09-2021.pdf | 2021-09-06 |
| 7 | 202141040285-Amended Pages Of Specification_FER Reply_14-03-2022.pdf | 2022-03-14 |
| 8 | 202141040285-Correspondence_As Filed_06-09-2021.pdf | 2021-09-06 |
| 8 | 202141040285-Claims_FER Reply_14-03-2022.pdf | 2022-03-14 |
| 9 | 202141040285-Claims_As Filed_06-09-2021.pdf | 2021-09-06 |
| 9 | 202141040285-Correspondence_FER Reply_14-03-2022.pdf | 2022-03-14 |
| 10 | 202141040285-Abstract_As Filed_06-09-2021.pdf | 2021-09-06 |
| 10 | 202141040285-Form5_FER Reply_14-03-2022.pdf | 2022-03-14 |
| 11 | 202141040285-FER.pdf | 2022-01-24 |
| 11 | 202141040285-Form9_Early Publication_05-01-2022.pdf | 2022-01-05 |
| 12 | 202141040285-Correspondence_05-01-2022.pdf | 2022-01-05 |
| 12 | 202141040285-FORM 18A [15-01-2022(online)].pdf | 2022-01-15 |
| 13 | 202141040285-FORM28 [15-01-2022(online)].pdf | 2022-01-15 |
| 13 | 202141040285-MSME CERTIFICATE [15-01-2022(online)].pdf | 2022-01-15 |
| 14 | 202141040285-FORM28 [15-01-2022(online)].pdf | 2022-01-15 |
| 14 | 202141040285-MSME CERTIFICATE [15-01-2022(online)].pdf | 2022-01-15 |
| 15 | 202141040285-Correspondence_05-01-2022.pdf | 2022-01-05 |
| 15 | 202141040285-FORM 18A [15-01-2022(online)].pdf | 2022-01-15 |
| 16 | 202141040285-FER.pdf | 2022-01-24 |
| 16 | 202141040285-Form9_Early Publication_05-01-2022.pdf | 2022-01-05 |
| 17 | 202141040285-Form5_FER Reply_14-03-2022.pdf | 2022-03-14 |
| 17 | 202141040285-Abstract_As Filed_06-09-2021.pdf | 2021-09-06 |
| 18 | 202141040285-Claims_As Filed_06-09-2021.pdf | 2021-09-06 |
| 18 | 202141040285-Correspondence_FER Reply_14-03-2022.pdf | 2022-03-14 |
| 19 | 202141040285-Claims_FER Reply_14-03-2022.pdf | 2022-03-14 |
| 19 | 202141040285-Correspondence_As Filed_06-09-2021.pdf | 2021-09-06 |
| 20 | 202141040285-Amended Pages Of Specification_FER Reply_14-03-2022.pdf | 2022-03-14 |
| 20 | 202141040285-Correspondence_MSME Certificate_06-09-2021.pdf | 2021-09-06 |
| 21 | 202141040285-Abstract_FER Reply_14-03-2022.pdf | 2022-03-14 |
| 21 | 202141040285-Description Complete_As Filed_06-09-2021.pdf | 2021-09-06 |
| 22 | 202141040285-Form1_As Filed_06-09-2021.pdf | 2021-09-06 |
| 22 | 202141040285-PatentCertificate18-07-2022.pdf | 2022-07-18 |
| 23 | 202141040285-Form2 Title Page_Complete_06-09-2021.pdf | 2021-09-06 |
| 23 | 202141040285-IntimationOfGrant18-07-2022.pdf | 2022-07-18 |
| 24 | 202141040285-FORM-26 [28-10-2023(online)].pdf | 2023-10-28 |
| 24 | 202141040285-Form28_Small Entity_06-09-2021.pdf | 2021-09-06 |
| 25 | 202141040285-Form3_As Filed_06-09-2021.pdf | 2021-09-06 |
| 25 | 202141040285-FORM 4 [30-10-2023(online)].pdf | 2023-10-30 |
| 26 | 401499-Form 27.pdf | 2023-11-20 |
| 26 | 202141040285-Form5_As Filed_06-09-2021.pdf | 2021-09-06 |
| 27 | 202141040285-FORM 4 [07-10-2025(online)].pdf | 2025-10-07 |
| 1 | 3,4-dimethylhydrazenehydrochloride;pyrazol-3-one-GooglePatentsE_24-01-2022.pdf |