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An Improved Process For The Preparation Of Boehmite

Abstract: The present invention relates to an improved process for the preparation of boehmite from aluminium hydroxide of Bayer process comprising the steps of: (a) pre-calcining aluminium hydroxide to remove chemically bound water partially; (b) subjecting the pre-calcined powder in an autoclave, to which water is added followed by stirring to make a slurry; (c) treating the slurry to a hydrothermal reaction for a period of 1-15 hours; (d) removing the slurry from the autoclave and filtering of the water to produce boehmite. The boehmite prepared by the invented process has reduced soda content and utilized in the production of sintered alumina abrasive with superior properties.

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Patent Information

Application #
Filing Date
31 March 2016
Publication Number
40/2017
Publication Type
INA
Invention Field
CHEMICAL
Status
Email
patent@depenning.com
Parent Application
Patent Number
Legal Status
Grant Date
2019-11-11
Renewal Date

Applicants

Carborundum Universal Limited
of Parry House, 6th Floor, No: 43, Moore Street, Chennai 600 001, Tamilnadu, India

Inventors

1. Premanshu Jana
of Pyanadth House, Ambattukavu, Thaikattukara P.O., Aluva-683106, Ernakulam, India
2. Ponnarassery Sukumaran Jayan
of KRSNA, 153 Alfia Nagar, Cochin University P O, Ernakulam -683109, India

Specification

We Claim:
1. An improved process for the preparation of boehmite from aluminium hydroxide of
Bayer process comprising the steps of:
(a) pre-calcining aluminium hydroxide to remove chemically bound water partially;
(b) subjecting the pre~calcined powder in an autoclave, to which water is added
followed by stirring to make a slurry;
(c) treating the slurry to a hydrothermal reaction for a period of 1-15 hours;
(d) removing the slurry from the autoclave and filtering of the water to produce
boehmite.
2. The process as claimed in claim 1 wherein the pre-calcining is carried out in a batch type or rotary furnace.
3. The process as claimed in claim 1 wherein the pre-calcining is performed at a temperature of 150 °C to 350 °C.
4. The process as claimed in claim 3 wherein the pre-calcining is performed at a temperature of 200 °C to 300 °C.
5. The process as claimed in claim 1 wherein the pre-calcining is done for a residence time of 30 minutes to 10 hours.
6. The process as claimed in claim 5 wherein the pre-calcining is done for a residence time of 30 minutes to 5 hours.
7. The process as claimed in claim 1 wherein the removal of chemically bound water in the pre-calcining step is 10-30 weight percent.
8. The process as claimed in claim 7 wherein the removal of chemically bound water in the pre-calcining step is 15-25 weight percent.

9. The process as claimed in claim 1 wherein in step (b) the ratio of water to pre-calcined powder is 1:1 to 1:8.
10. The process as claimed in claim 9 wherein in step (b) the ratio of water to pre-calcined powder is 1:3 to 1:5.
11. The process as claimed in claim 1 wherein the hydrothermal reaction in step (c) is carried out for a period of 5 to 10 hours.
12. The process as claimed in claim 1 wherein the hydrothermal reaction in step (c) is carried out at a temperature of 120 °C to 250 °C.
13. The process as claimed in claim 12 wherein the hydrothermal reaction in step (c) is carried out at a temperature of 150 °C to 200 °C.
14. The process as claimed in claim 1 wherein filtered slurry in step (d) is washed multiple times.
15. A process for preparing sintered alumina abrasives from the boehmite obtained by the process as claimed in claim 1.

Documents

Application Documents

# Name Date
1 Power of Attorney [31-03-2016(online)].pdf 2016-03-31
2 Form 3 [31-03-2016(online)].pdf 2016-03-31
3 Form 18 [31-03-2016(online)].pdf 2016-03-31
4 Form 1 [31-03-2016(online)].pdf 2016-03-31
5 Drawing [31-03-2016(online)].pdf 2016-03-31
6 Description(Complete) [31-03-2016(online)].pdf 2016-03-31
7 201641011478-FER.pdf 2018-08-29
8 201641011478-Proof of Right (MANDATORY) [13-02-2019(online)].pdf 2019-02-13
9 201641011478-PETITION UNDER RULE 137 [13-02-2019(online)].pdf 2019-02-13
10 201641011478-OTHERS [13-02-2019(online)].pdf 2019-02-13
11 201641011478-FER_SER_REPLY [13-02-2019(online)].pdf 2019-02-13
12 201641011478-DRAWING [13-02-2019(online)].pdf 2019-02-13
13 201641011478-CLAIMS [13-02-2019(online)].pdf 2019-02-13
14 Correspondence by Agent_Proof of Right_26-02-2019.pdf 2019-02-26
15 201641011478_Drawings_Granted 324866_11-11-2019.pdf 2019-11-11
16 201641011478_Description_Granted 324866_11-11-2019.pdf 2019-11-11
17 201641011478_Claims_Granted 324866_11-11-2019.pdf 2019-11-11
18 201641011478_Abstract_Granted 324866_11-11-2019.pdf 2019-11-11
19 201641011478-PatentCertificate11-11-2019.pdf 2019-11-11
20 201641011478-IntimationOfGrant11-11-2019.pdf 2019-11-11
21 201641011478-FORM 4 [11-03-2020(online)].pdf 2020-03-11

Search Strategy

1 Search_Strategy_201641011478_28-05-2018.PDF

ERegister / Renewals

3rd: 11 Mar 2020

From 31/03/2018 - To 31/03/2019

4th: 11 Mar 2020

From 31/03/2019 - To 31/03/2020

5th: 11 Mar 2020

From 31/03/2020 - To 31/03/2021

6th: 22 Dec 2020

From 31/03/2021 - To 31/03/2022

7th: 11 Mar 2022

From 31/03/2022 - To 31/03/2023

8th: 21 Feb 2023

From 31/03/2023 - To 31/03/2024

9th: 07 Mar 2024

From 31/03/2024 - To 31/03/2025

10th: 27 Mar 2025

From 31/03/2025 - To 31/03/2026