Abstract:
The purpose of the present invention is to provide a brazing joint having excellent tensile strength (TSS and CTS) and a manufacturing method therefor. A brazing joint is manufactured as follows: after a plate assembly (200) constituted by interposing a filler material (230) between steel plates (210 220) is heated to at least the Ac3 temperature of the steel plates (base material) and the Ar3 temperature of regions of the steel plates close to the filler material is raised so as to exceed the Ar3 temperature of the steel plates (base material) a hot stamping step in which a quenching initiation temperature X does not exceed the Ar3 temperature of the steel plates (base material) is performed.
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Notices, Deadlines & Correspondence
c/o NIPPON STEEL & SUMITOMO METAL CORPORATION 6 1 Marunouchi 2 chome Chiyoda ku Tokyo
1008071
2. NISHIBATA Hitomi
c/o NIPPON STEEL & SUMITOMO METAL CORPORATION 6 1 Marunouchi 2 chome Chiyoda ku Tokyo
1008071
3. YASUYAMA Masanori
c/o NIPPON STEEL & SUMITOMO METAL CORPORATION 6 1 Marunouchi 2 chome Chiyoda ku Tokyo
1008071
Specification
DESCRIPTION
Title of Invention: Method of Production of Brazed Joint
and Such a Brazed Joint
Technical Field
[0001] The present invention relates to a method of
production of a brazed joint and to such a brazed joint,
in particular is suitable for use for brazing together
the sheet surfaces of a plurality of ~t~~l sheets.
Background Art
[0002] In the past, the practice had been to produce a
hot stamped part by a hot stamping process. At that time,
a blank comprised of a plurality of steel sheets joined
. ,,. '">··· :· .. o:· ~~·'-''··:· ~(' . at the surfaces- is supplied to· t"he hot stamping pro'c::ess.
Due to this, the strength and rigidity of the hot stamped
part are raised. In this case, one or more steel sheets
are joined at a region of the main steel sheet requiring
larger strength and rigidity than other regions. As
20 applications for such hot stamped parts using such
blanks, for example, there are component parts of
monocoque bodies (unit construction bodies) such as front
side members or center pillars etc.
[0003] To join such a main steel sheet and a
25 reinforcing steel sheet, there is the technique of using
brazing.
[0004] PLT 1 discloses the art of placing a brazing
filler metal (hard solder, same below) between the
surfaces of the main steel sheet and reinforcing steel
30 sheet and welding them to provisionally fasten the steel
sheets and brazing filler metal, then heating the steel
sheets to a temperature higher than the shaping
temperature of the steel sheets and hot press-forming
them and then cooling the steel sheets in the die after
35 shaping so as to cause the brazing filler metal to
solidify.
[0005] PLT 2 discloses the art of clamping a brazing
- 2 -
filler metal with a solidus temperature of 1050°C or less
and a liquidus temperature of 700°C or more between the
surfaces of a main steel sheet and reinforcing steel
sheet, placing the blank in a heating furnace to heat it
5 to 900°C to 1050°C, then quenching and press-forming (hot
stamping) it.
[0006] PLT 3 discloses the art of coating a sheet
surface with a brazing filler metal, heating the coated
main steel sheet for the quenching and making the brazing
10 filler metal melt, joining the surface of the main.steel
sheet and the surface of the reinforcing steel sheet
through this melted brazing filler metal, then quenching
and press-forming (hot stamping) the same.
Citation List
15 Patent Literature
[0007] PLT 1: Japanese Patent Publication No. 2002-
178069A
PLT 2: Japanese Patent Publication No. 2004-141913A
PLT 3: Japanese Patent Publication No. 2011-88484A
20 PLT 4 : Japanese Patent Publication No. 2014-200840A
PLT 5: Japanese Patent Publication No. 2015-166099A
Nonpatent Literature
[0008] NPLT 1: Takedachi, A. ''Prediction of Ac1, Ac3,
and Ms Transformation Points of Steel by Empirical
25 Formula", Heat Treatment, 41 (3), p. 164 to p. 169
NPLT 2: Choquet, P. et al., Mathematical Model for
Predictions of Austenite and Ferrite Microstructures in
Hot Rolling Processes, IRSID Report, St.Germain-en-Laye,
1985.7p.
30 Summary of Invention
Technical Problem
[0009] However, in the arts described in PLTs 1 to 3,
locations arise where the brazing filler metal is not
filled between the steel sheets. Clearances are liable to
35 remain between the steel sheets. Therefore, in the arts
described in PLTs 1 to 3, it is not easy to sufficiently
- 3 -
improve the strength and rigidity of hot stamped parts.
[0010) Therefore, the inventors proposed in PLT 4 the
technique of applying pressure in the thickness direction
to a plurality of metal sheets between which a brazing
5 filler metal is clamped at the time of the heating step
for hot stamping or in the period from the heating step
until transfer to the hot stamping step. According to
this technique, it is possible to prevent clearance from
remaining between the steel sheets as in the arts
10 described in PLTs 1 to 3.
[0011] Further, the inventors proposed in PLT 5 using
a brazing filler metal having a solidus temperature above
the heating temperature and below the solidus temperature
of the metal sheets in the hot stamping step so as to
15 produce a hot, stamped part having a strength and rigidity
substantially equal to a hot stamped part described in
the above-mentioned PLT 4 without making great changes to
the hot stamping process.
[0012) On the other hand, for example, in auto parts
20 etc. where both lighter weight and higher strength are
being sought, further higher strength is being demanded
for application of hot stamped parts (brazed joints}
obtained by brazing together a plurality of steel sheets
and hot stamping them.
25 [0013) However, the specific tensile shear strength
(TSS} and cross tension strength (CTS} of the brazed
joint described in PLTs 1 to 3 are not described, so the
strength of the brazed joint was not sufficiently raised.
Control (management} of the temperature of the steel
30 sheets in the hot stamping step has not been studied from
the viewpoint of raising the joint strength of a brazed
joint.
[0014) Therefore, the present invention has as its
object the provision of a brazed joint having excellent
35 tensile strengths (TSS and CTS} and a method of
production of the same.
Solution to Problem
- 4 -
[0015] To solve the above problem, the inventors took
note of and studied the control (management) of the
temperature of steel sheets in the hot stamping step. As
a result, they discovered that the Ar3 point in a region
5 near the brazing filler metal at the steel sheets becomes
higher than the inherent Ar3 point of the steel sheets.
Further, they discovered that by controlling the
quenching start temperature in the hot stamping step to
the inherent Ar3 point of the steel sheets or less, it is
10 possible to make the degree of quenching at. th~·region
near the brazing filler metal of the steel she~ts and the
degree of quenching at other regions different to form a
softened region in the region near the brazing filler
metal of the steel sheets and thereby raise the tensile
·15 strength of the· brazed joint and thereby completed·· the
present invention.
[0016] The aspects of the present invention are as
follows:
(1) A method of production of a brazed joint comprising a
20 heating step of heating a sheet combination having a
plurality of steel sheets superposed so that the sheet
surfaces face each other and a first brazing filler metal
placed in a predetermined region between the surfaces of
two mutually adjoining steel sheets among the plurality
25 of steel sheets by a heating temperature of an Ac3 point
of the steel sheets or more and a hot stamping step of
quenching and shaping the sheet combination heated by the
heating step, wherein the first brazing filler metal has
a liquidus temperature of less than the heating
30 temperature, before the start of quenching in the hot
stamping step, the Ar3 point in a region near the brazing
filler metal at the steel sheets is higher than the Ar3
point of the steel sheets, and the quenching start
temperature of the sheet combination at the hot stamping
35 step is made a temperature of the Ar3 point of the steel
sheet or less.
(2) The method of production of a brazed joint according
- 5 -
to (1), further comprising a step of obtaining a sheet
combination where instead of the first brazing filler
metal, a second brazing filler metal having a solidus
temperature over the heating temperature in the heating
5 step and less than the solidus temperature of the steel
sheets is placed in a predetermined region between two
steel sheets and a brazing step of heating the sheet
combination to a temperature over a liquidus temperature
of the second brazing filler metal and less than the
10 solidus temperature of the steel sheets before ·the·
heating step, then cooling down to less than the solidus
temperature of the second brazing filler metal to braze
the steel sheets.
(3) The method of production of a brazed joint according
15 to (1) or· (2), wherein the heating step heats· the ·sheet
combination while applying pressure to the sheet
combination in the thickness direction of the steel
sheets.
(4) The method of production of a brazed joint according
20 to (2), wherein the brazing step heats the sheet
combination while applying pressure to the sheet
combination in the thickness direction of the steel
sheets.
(5) The method of production of a brazed joint according
25 to any one of (1) to (4), wherein the plurality of steel
sheets are comprised of one or both of nonplated steel
sheets not plated on their surfaces and galvanized steel
sheets or aluminum plated steel sheets.
[0017] (6) A brazed joint comprising a plurality of
30 steel sheets overlaid so that their surfaces face each
other and a brazing filler metal placed in a
predetermined region between the surfaces of two mutually
adjoining steel sheets in the plurality of steel sheets,
the two steel sheets being joined by the brazing filler
35 metal, in which brazed joint, a relationship between an
average hardness of positions near the brazing filler
metal in the steel sheets contacting the brazing filler
- 6 -
metal and an average hardness of representative positions
of a base metal region in the steel sheets satisfies the
following (A) :
Average hardness of positions near brazing filler metal
5 (HV)+50HV region filler (~m)
(HV) metal (HV) metal
.. (HV) {HV)
1-1 A 454 450 440 335 40
2-2 A 454 450 435 330 35
3 3 502
None
A 495 490 370 40
----4-4 A ·----·-5-0-2- ------ -~9~ ---- 494 350 ---42- -
[0122] Table 3
850°C quenching 700°C quenching
(comparative examples) {invention examples) r- Average Average
Average hardness Average hardness
hardness of of Thickness hardness of of Thickness
Cb~~inaticin B_razing J:t!p_:de~;ent,\ ti Vi:' positions of L·epresenta ti ve positions o::::
filler positions of near softened positions of near softened
of sheets
metal base metal brazing region base metal brazing region
region filler (~) region filler I~)
(HV) metal {HV) metal
(HV) (HV)
5 5 A 550 545 530 380 40
6 6 550
None
A 543 535 400 36
[0123] In Table 2 and Table 3, the "Combination of
sheets" corresponds to the numbers shown in Table 1
("No.") "Combinations of sheets" of "1-1", "2-2", "3-3",
''4-4", ''5-5", and "6-6'' respectively show use of two of
the No. 1, No. 2, No. 3, No. 4, No. 5, and No. 6 steel
10 sheets shown in Table 1. The same is true in the later
explained Table 4 and Table 5 as well.
[0124] Further, in Table 2 and Table 3, ''A'' in the
column of "brazing filler metal" shows use of Cu-Sn20%
braze (solidus temperature 770°C, liquidus temperature
15 930°C) as the brazing filler metal. The same is true in
the later explained Table 4 and Table 5 as well.
[0125] Further, in Table 2, "850°C quenching" shows
that the quenching start temperature X in the hot
stamping step was made 850°C. "700°C quenching" shows that
20 the quenching start temperature X in the hot stamping
step was made 700°C. As explained above, lhe Ar3 points of
- 35 -
the No. 1 steel sheet and No. 2 steel sheei are 727"C,
while the Ar3 points of the No. 3 steel sheet and No. 4
steel sheet are 7ll"C. Therefore, ''850"C quenching'' are
examples not satisfying the condition of the above-
5 mentioned formula (2) (are comparative examples). On the
other hand, "700"C quenching" are examples satisfyin::; the
condition of the above-mentioned formula (2) (are
invention examples).
[0126] Similarly, in Table 3, ''850"C quenching" shows
. - -· ·- -- ·--
10 that the quenching start temperature X in the hot
stamping step was made 850"C. "650"C quenching" shows that
the quenching start temperature X in the hot stamping
step was made 650"C. As explained above, the Ar3 point of
the No. 5 -steel '3ll'E!cc-t is 680"C, wnile-the 'Ar3 p1oint''Of the
15 No. 6 steel sheet is 693"C. Therefore, "850"C quenching"
are examples not satisfying the condition of the abovementioned
formula (2) (are comparative examples). On the
other hand, "650"C quenching" are examples satisfying the
condition of the above-mentioned formula (2) (are
20 invention examples).
[0127] In addition, in Table 2 and Table 3, "Average
hardness of representative positions of base metal
region", "Average hardness of positions near brazing
filler metal", and "Thickness of softened region'' were
25 all explained in the present embodiment. The same is true
in the later explained Table 6 and Table 7 as well.
[0128] However, here, the region satisfying the abovementioned
formula (9) is designated as the softened
region. That is, a region with a value of the Vicker's
30 hardness smaller than the value of the average hardness
(HV) of representative positions of the base metal region
minus 50HV was specified as the ''softened region''.
[0129] As shown in Table 2 and Table 3, it will be
understood that if the condition of formula (2) is not
35 satisfied, the average hardness of positions near the
brazing filler metal will not fall much at all from the
- 36 -
average hardness of the representative positions of the
base metal region. Further, the softened region is not
formed. On the other hand, if the condition of formula
(2) is satisfied, the average hardness of positions near
5 the brazing filler metal falls 50HV or more from the
average hardness of representative positions of the base
metal region. Further, it will be understood that a.
softened region having a thickness of 30 ~m or more is
formed.
10 [0130] Evaluation of Hot Stamped Part
FIG. 5 is a view showing the shape of a test piece of a
tensile shear test. Between the surfaces of two steel
sheets of the same number ("No.") in Table 1 (for
example, No. 1 steel sheets), thickness 30 ~brazing
15 filler metal was placed to produce a sheet combin.ad_on
(test piece of tensile shear test).
[0131] As shown in the top figure of FIG. 5, two steel
sheets of widths of 25 mm and lengths of 90 mm were set
so that the entireties of the regions in the width
20 direction were overlaid and regions of 25 mm were
overlaid from the front end along the long direction. A
brazing filler metal was placed at the entire overlapping
region (25 mmx25 mm region).
[0132] FIG. 6 is a view showing the shape of a test
25 piece of a cross tensile test. Between the surfaces of
two steel sheets of the same number ("No.") in Table 1
(for example, No. 1 steel sheets), thickness 30 ~m
brazing filler metal was placed to produce a sheet
combination (test piece of cross tensile test).
30 [0133] As shown in the top figure of FIG. 6, two steel
sheets of widths 50 mm and lengths 150 mm were placed so
that 50 mmx50 mm square regions at their centers
overlapped. A brazing filler metal was placed at the
entire overlapping region (50 mmx50 mm region) .
35 [0134] The thus produced sheet assemblies (test pieces
for tensile shear tests and test pieces for cross tensile
5
- 37 -
tests) were subjected to heating steps and hot stamping
steps under the same conditions as the above-mentioned
brazed joint (see section on ''Evaluation of Brazed
Joint")
[0135] A brazed joint obtained by the hot stamping
step (test piece for tensile strength test) was subjected
to a tensile shear test by a technique based on JIS Z3136
to measure the tensile shear strength (TSS). Further, the
direction of tension at the time of the tensile shear
10 ~test: was the di.cection of the white arrows shown in the
bottom figure of FIG. 5.
[0136] Further, a brazed joint obtained by the same
hot stamping step ·(test piece for· cross tensile test) was
subje~ted to a cross tensile test by a technique based on
15 JIS Z3i37 ·to m~asure the cross tensile strength (CTS).
Further, the direction of tension at the time of the
cross tensile test was the direction of the white arrows
shown in the bottom figure of FIG. 6.
[0137] In a hot stamped part such as the hat shaped
20 member 110 shown in FIG. 1, the form of the imparted
stress differs depending on the location. The form of the
stress can be approximated by the combination of stresses
when force acts in the directions of the white arrows
shown in the bottom figures of FIG. 5 and FIG. 6.
25 Therefore, when satisfying the above-mentioned formula
(2), compared with when not, if both the tensile shear
strength (TSS) and cross tensile strength (CTS) are
improved, it can be said that the joint strength is
improved no matter how the brazed joint is shaped.
30 Therefore, here, a hot stamped part is evaluated by
evaluating the tensile shear strength (TSS) and the cross
tensile strength (CTS) . The results are shown in Table 4
to Table 7.
- 38 -
[0138] Table 4
TSS (kN) I CTS (kN)
Combination Brazing Quenching start temp_erature (oC)
of sheets filler metal 850 700 850 700
(comparative (invention (comparative (invention
examples) examples) examples) examples)
1-1 A 31.8 40.5 3.3 4.7
2-2 A 34.55 46.5 3.7 5.22
3-3 A 33.6 42.3 3.5 4
4-4 A 35.7 48.2 3 3.5
1-1 8 36.1 40.5 4. 4 6.7
2-2 B 40.3 45.1 4. 2 6.2
3-3 8 38.5 42.6 4.6 7
4-'l B 43.7 4'1. 5 3 .·6 '' ,. ·.;· 5.5
[0139] Table 5
TSS (kN) .CTS (kN)
Combination Brazing Quenching start temperature (OC)
of sheets filler metal 850 650 850 650
(comparative .( inyent ion ~-comp.tt:r;:at.igs; .(invent ion
examples) examples) examples) examples)
5-5 A 32.6 38.3 3.2 4.5
6-6 A 30.5 36.6 2.9 4.4
5-5 8 33.2 49.6 3.1 4
6-6 B 34.5 47.5 2.7 3.3
5 [0140] Table 6
Average
Average hardness
Quenching hardness of of Thickness
representative positions of
start TSS
positions of near softened temperature Remarks (kN)
base metal brazing region
(oC)
region filler (Jlm)
(HV) metal
(HV)
850 34.55 4 60 460 0 Comparative example
770 31.9 455 454 0 Comparative example
735 33.3 450 440 0 Comparative example
718 39.05 440 388 23 Invention example
694 46.5 435 330 35 Invention example
670 54.1 430 300 40 Invention example
635 49.9 420 2 98 60 Invention example
620 35 370 270 100 Reference example
580 32 350 250 130 Reference example
- 39 -
[0141] Table 7
Average
Average hardness
Quenching hardness of of Thickness
representative positions of
start CTS
positions softened
temperature of near Remarks
(kN)
base metal brazing region
('C) region filler (f!m)
(HV) metal
(HV)
~50 3.7 460 460 0 Comparative example
765 3.8 455 454 0 Comparative example
740 3.7 445 440 0 Comparative example
:-- 720 5 440 388 20 Invention example ·-
696 5.4 435 330 35 Invention example
671 6.5 . 430 300 40 Invention example
633 5.5 420 2 98 65 Invention example
623 3.9 370 270 100 Reference example
581 3.7 350 250 130 Reference example
[01.42]· ·. In:·.--.Tab1c~ -1 and Table ~; "R" in the co_l-umn .. ;f
''brazing filler metal'' shows use of Cu-Zn30% braze
5 (solidus temperature 900°C, liquidus temperature 930°C) as
the brazing filler metal.
[0143] The "quenching (start) temperature" in Table 4
to Table 7 shows the quenching start temperature X at the
hot stamping step. Table 4 shows the measurement results
10 for the tensile shear strength (TSS) and the cross
tensile strength (CTS) for the cases where the "quenching
(start) temperature" is 850°C and 700°C. As explained
while referring to Table 2, the measurement results when
the "quenching (start) temperature" is 850°C are examples
15 not satisfying the condition of the above-mentioned
formula (2) (are comparative examples). On the other
hand, the measurement results when the "quenching (start)
temperature" is 700°C are examples satisfying the
condition of the above-mentioned formula (2) (are
20 invention examples). Further, Table 5 shows the
measurement results of the tensile shear strength (TSS)
and cross tensile strength (CTS) for the cases where the
"quenching (start) temperature" is 850°C and is 650°C. As
explained while referring to Table 3, the measurement
- 40 -
results when the "quenching (start) temperature" is 850°C
are examples not satisfying the condition of the abovementioned
formula (2) (are comparative examples). On the
other hand, the measurement results when the "quenching
5 (start) temperature" is 650°C are examples satisfying the
condition of the above-mentioned formula (2) (are
invention examples).
[0144] As shown in Table 4 and Table 5, it will be
understood that regardless of the combination of the
10 sheets and the type of the brazin-g fiiler ·metai, -compared
with when the condition of the formula (2) is not
satisfied, when it is satisfied, both the tensile shear
strength (TSS) and cross tensile strength (CTS) can be
15
improved.
~;.,_),,:,; ;~-· !'.:~r,·:~
[0145] Further, Table 6 and Table 7 show the
measurement results of the tensile shear strength (TSS)
and cross tensile strength (CTS) for the cases where the
"quenching temperature" (quenching start temperature X in
hot stamping step) differs for the case of the
20 "combination of sheets" of "2-2". The measurement results
of Tables 6 and 7 are graphed and shown in FIGS. 7 and 8.
[0146] As shown in Table 6 and Table 7, it will be
understood that if the "quenching temperature" becomes
lower, both the tensile shear strength (TSS) and cross
25 tensile strength (CTS) tend to become larger.
[0147] As explained above, the Ar3 point of the No. 2
steel sheet is 727°C. In Table 6 and Table 7, the
measurement results when the "quenching temperature"
exceeds this temperature become examples not satisfying
30 formula (2) (are comparative examples). On the other
hand, the measurement results when the "quenching
temperature" is this temperature or less become examples
satisfying formula (2) (are invention examples) .
[0148] As shown in Table 6 and Table 7, when changing
35 the range of the "quenching temperature", as explained
with reference to Table 2 and Table 3, it will be
- 41 -
understood that if the condition of formula (2) is not
satisfied, the average hardness of positions near the
brazing filler metal will not fall much at all from the
average hardness of representative positions of the base
5 metal region. This will be visually apparent from FIGS. 7
and B. Further, the softened region was not formed. On
the other hand, it will be understood that if the
condition of formula (2) is satisfied, the average
hardness of positions near the brazing filler metal falls
10 50 HV or more from·the average hardness of representative
positions of the base metal region. This will be visually
apparent from FIGS. 7 and B. Further, it will be
understood that a softened region having a thickness of
10 ~ or more is formed.
15 [0149] In particular, wl1en the quenching start
temperature X is (Ar3 point -100) (°C) to the Ar3 point
(°C), the base metal region is sufficiently quenched and
the hardness rises. Further, the softened region formed
can ease the stress concentration at the brazing filler
20 metal, so both the tensile shear strength (TSS) and cross
tensile strength (CTS) become larger. This will be
visually understood from FIGS. 7 and B.
[0150] Further, in the present embodiment, the results
of combinations of the same types of sheets are shown.
25 Other explanations of the combinations of sheets will be
omitted. However, the inventors confirmed that a similar
trend is obtained as explained in the present embodiment
for the combination of different types of sheets.
[0151] Summary
30 In the above way, in the present embodiment, the sheet
combination 200 comprised of the steel sheets 210, 220
between which a brazing filler metal 231 rs sandwiched is
heated by a temperature of the Ac3 point of the steel
sheets (matrix) or more, then is hot stamped using as the
35 quenching start temperature X the temperature of the Ar3
point of the steel sheet (matrix) to thereby produce the
- 42 -
brazed joint. By doing this, it is possible to make the
Vicker's hardness at positions of the steel sheets 210,
220 near the brazing filler metal 230 (average hardness
of positions near brazing filler metal) smaller than the
5 value of the inherent Vicker's hardness of the steel
sheets 210, 200 (average hardness of representative
positions of base metal region) minus 50 HV. That is, it
is possible to lower the hardness of regions near the
brazing filler metal 231 of the steel sheets 210, 220
10 (softened regions.) l Therefore, it .is possible to· .control
the temperature of the steel sheets at the hot stamping
step so as to raise the joint strength of the brazed
joint. Accordingly, it is possible to produce a high
strength brazed joint without greatly changing the
15 · conventional process of production'· of· hot stamped parl:s.
[0152] Modification
In the present embodiment, in the heating step, the sheet
combination 200 being heated was pressed in the thickness
direction of the steel sheets 210, 220. However, as
20 described in the specification of PLT 4, this pressing
operation may be performed after the heating step and
before the hot stamping step. Further, if performing the
above such pressing operation, it is possible to reliably
keep a clearance from forming between the steel sheets
25 210, 220 and the brazing filler metal 231, so this is
preferable, but this pressing operation does not
necessarily have to be performed.
[0153] Further, in the present embodiment, the
explanation was given with reference to the example of
30 the case of brazing in the heating step like in the art
described in the specification of PLT 4. However, as
shown in the art described in the specification of PLT 5,
it is also possible to perform the brazing before the
heating step.
35 [0154] That is, instead of the first brazing filler
metal 231 having a liquidus temperature lower than the
heating temperature at the heating step, a second brazing
- 43 -
filler metal 232 having a solidus temperature higher than
the heating temperature in the hot stamping heating step
("heating step" in the present embodiment) and lower than
the solidus temperature of the steel sheets 210, 220 is
5 used to braze the steel sheets 210, 220 (brazing step).
The second brazing filler metal 232 is an example of the
brazing filler metal 230. It differs from the first
brazing filler metal 231 in the liquidus temperature and
solidus temperature, but may be the same or different in
10 oth,~r propert'ies, shape, etc. Further, regarding, i:he
placement of the brazing filler metal 232 in the brazing
step or the provision of the softened region, in FIGS. 2
to 4, read the description ''brazing filler metal 230" as
"brazing filler metal 232''.
15 {\Ji!:>Sj ·'·in t:he bl"azing step,· the· sheet· combination 200
set in the fixture is heated so that the temperature of
the brazing filler metal 232 becomes a temperature
exceeding the liquidus temperature of the brazing filler
metal 232 and lower than the solidus temperature of the
20 steel sheets 210, 220. Further, at this time, in the same
way as explained while referring to FIG. 3, the sheet
combination 200 is preferably heated while applying
pressure. The sheet combination 200 heated in this way is
cooled until the temperature of the brazing filler metal
25 232 falls below the solidus temperature of the brazing
filler metal 232.
[0156] After that, the heating step, hot stamping
step, and shot blasting step explained in the present
embodiment are performed in that order. Even if heating
30 the brazed sheet combination 200 in the heating step,
since the solidus temperature of the brazing filler metal
232 is higher than the heating temperature, the brazing
filler metal 232 does not become a liquid phase and the
solid phase state can be maintained. Further, in the same
35 way as when using the first brazing filler metal 231,
before the start of quenching at the hot stamping step,
the Ar3 point of the regions near the brazing filler
- 44 -
metal in the steel sheets becomes higher than the Ar3
point of the steel sheets.
[0157] Therefore, it is possible to form the abovementioned
softened region at the steel sheets and not
5 only raise the tensile strength of the brazed joint, but
also reliably prevent liquid metal embrittlement cracking
at the time of hot stamping. Further, the brazing is
performed as a separate step from the heating step before
the hot stamping, so management of the brazing becomes
J.O ·easy and the. brazing conditions cari be ·kept·. from becoming
restricted. Further, even if the atmosphere of the
heating step before the hot stamping is a nonreducing
atmosphere, it is possible to prevent oxidation of the
brazing filler metal from making brazing impossible. Due
15 to the above, it· is possible to r'aT's'"e" 'the joint· 'Strength
of the brazed joint without making major changes in the
conventional hot stamping process. The above effect
obtained by using such a second brazing filler metal was
confirmed by experiments by the present inventors.
20 Further, when performing this, the brazing is completed
when starting the heating step, so in the heating step,
it is also possible not to apply the above-mentioned
pressure.
[0158] Further, in the present embodiment, the
25 explanation was given with reference to the example of a
case of two steel sheets joined planarly. However, the
number of steel sheets joined planarly may be three or
more as well. In this case, brazing filler metal is
placed between each two facing steel sheets.
30 [0159] Further, the measurement positions of
temperature explained in the present embodiment,
including the examples and modifications as well, were
all positions of the center of the brazing filler metal
in the thickness direction of the steel sheets.
35 [0160] Further, the present embodiments, including the
examples and modifications, all only show examples of
specific means for working the present invention. The
- 45 -
technical scope of the present invention must not be
!imitatively interpreted based on the same. That is, the
present invention can be worked in various ways without
departing from its technical idea or main features.
CLAIMS
Claim 1. A method of production of a brazed joint
comprising
a heating step of heating a sheet combination
5 having a plurality of steel sheets superposed so that the
sheet surfaces face each other and a first brazing filler
metal placed in a predetermined region between the
surfaces of two mutually adjoining steel sheets among the
plurality of steel sheets by a heating temperature of an
10 Ac3 point of the steel sheets or more and
·15
a hot stamping step of quenching and shaping
the sheet combination heated by the heating step, wherein
the first brazing filler metal has a liquidus
temperature of less than the heating temperature,
before the start of quenching in the hot
stamping step, the Ar3 point in the region near the
brazing filler metal at the steel sheets is higher than
the Ar3 point of the steel sheets, and
the quenching start temperature of the sheet
20 combination at the hot stamping step is made a
temperature of the Ar3 point of the steel sheet or less.
Claim 2. The method of production of a brazed joint
according to claim 1, further comprising:
a step of obtaining a sheet combination where
25 instead of the first brazing filler metal, a second
brazing filler metal having a solidus temperature over
the heating temperature in the heating step and less than
the solidus temperature of the steel sheets is placed in
the predetermined region between two steel sheets and
30 a brazing step of heating the sheet combination
to a temperature over a liquidus temperature of the
second brazing filler metal and less than the solidus
temperature of the steel sheets before the heating step,
then cooling down to less than the solidus temperature of
35 the second brazing filler metal to braze the steel
sheets.
Claim 3. The method of production of a brazed joint
- 47 -
according to claim 1 or 2, wherein the heating step heats
the sheet combination while applying pressure to the
sheet combination in the thickness direction of the steel
sheets.
5 Claim 4. The method of production of a brazed joint
according to claim 2, wherein the brazing step heats the
sheet combination while applying pressure to the sheet
combination in the thickness direction of the steel
sheets.
10 Claim 5. The method of production of a brcfzced· joint
15
according to any one of claims 1 to 4, wherein the
plurality of steel sheets are comprised of one or both of
nonplated steel .sheets not plated on their surfaceB and
galvanized steel sheets or aluminum plated steel sheets.
Claim 6. i\ brazed joint comprising
a plurality of steel sheets overlaid so that
their surfaces face each other and
a brazing filler metal placed in a
predetermined region between the surfaces of two mutually
20 adjoining steel sheets in the plurality of steel sheets,
the two steel sheets being joined by the
brazing filler metal,
in which brazed joint, a relationship between
an average hardness of positions near the brazing filler
25 metal in the steel sheets contacting the brazing filler
metal and an average hardness of representative positions
of a base metal region in the steel sheets satisfies the
following (A) :
Average hardness of positions near brazing
30 filler metal (HV)+50HV
Documents
Application Documents
#
Name
Date
1
Translated Copy of Priority Document [28-04-2017(online)].pdf