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Eco Friendly Water Based Aerosol Glitter Paint Composition

Abstract: The present invention relates to an eco-friendly, water-based aerosol glitter spray paint composition comprising water as a base solvent, solid components such as glitter which is the main ingredient, a resin system to hold the main ingredient, a rheology modifier to maintain the right rheology of the suspension, film forming polymers, anti-foaming agent, other ingredients and dimethyl ether as the propellant.

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Patent Information

Application #
Filing Date
23 July 2021
Publication Number
33/2021
Publication Type
INA
Invention Field
POLYMER TECHNOLOGY
Status
Email
Parent Application
Patent Number
Legal Status
Grant Date
2022-02-18
Renewal Date

Applicants

People Paints Amore Private Limited
601, Ace Business Centre, Gokul Nagar, Thane - 400601, Maharashtra, India.

Inventors

1. KABRA, Puneet
People Paints Amore Private Limited, 601, Ace Business Centre, Gokul Nagar, Thane - 400601, Maharashtra, India.
2. YADAV, Sanjog
People Paints Amore Private Limited, 601, Ace Business Centre, Gokul Nagar, Thane - 400601, Maharashtra, India.

Specification

Claims:1. A water-based glitter aerosol spray paint composition, wherein the composition comprises of water, resin system, rheology modifier, non-oxidative glitter particles, anti-foaming agent, polyol, and dimethyl ether propellant;
characterized in that:
- the composition is free from odor-producing organic solvents;
- the composition is odorless eco-friendly composition; and
- the composition can be used on a variety of surfaces.
2. The composition as claimed in claim 1, wherein the glitter particle has a size ranging from about 5 to about 70 µm.
3. The composition as claimed in claim 1, wherein the glitter particle is selected from alumina, pigment coated alumina, polyester, pigment coated polyester, or combinations thereof.
4. The composition as claimed in claim 1, wherein the film former is acrylic styrene copolymer having acrylic content below 50% or below 20%.
5. The composition as claimed in claim 1, wherein the resin comprises aqueous polyurethane dispersion having NCO-content below 10% or below 5%, and polyurethane content below 99% or below 95%.
6. The composition as claimed in claim 1, wherein the rheology modifier comprises carboxyvinyl polymer.
7. The composition as claimed in claim 1, wherein the anti-foaming agent comprising modified silane below 80% or below 60%.
8. The composition as claimed in claim 1, wherein the polyol is glycerol comprising 4 to 36 carbon atoms.
9. A water-based glitter paint composition, wherein the composition is aerosol spray composition comprising,
a. water ranging from about 40% w/w to about 50% w/w;
b. acrylic Styrene Copolymer ranging from about 10% w/w to about 30% w/w;
c. polyurethane dispersion ranging from about 10% w/w to about 20% w/w;
d. coated alumina powder ranging from about 5% w/w to about 20% w/w;
e. modified silane ranging from about 0.2% w/w to about 1% w/w;
f. synthetic Thickener ranging from about 0.1% w/w to about 2% w/w;
g. propylene glycol ranging from about 0.01% w/w to about 2% w/w;
h. glycerine ranging from about 0.05% w/w to about 2% w/w; and
i. dimethyl ether ranging from about 10% w/w to about 50% w/w;
characterized in that:
- the composition is odorless eco-friendly composition; and
- the composition is can be used on a variety of surfaces.
10. An aerosol spray container comprising the composition as claimed in claim 1 or claim 9, wherein the aerosol spray container is tin container or coated aluminium container comprising actuator orifice of size more than 0.15 mm.

, Description:FIELD OF THE INVENTION
[0001] The present disclosure generally relates to the field of coating compositions. Specifically, it relates to eco-friendly, water-based glitter spray paint composition which enables broad scope for spray application on variety of surfaces like textile, paper, metal, plastic, and glass.

BACKGROUND OF THE INVENTION
[0002] Background description includes information that may be useful in understanding the present invention. It is not an admission that any of the information provided herein is prior art or relevant to the presently claimed invention, or that any publication specifically or implicitly referenced is prior art.
[0003] Water-based aerosol spray paints which are prepared by mixing metallic pigments and resin compositions in water are known and extensively used as top coating material. Such water-based aerosol spray paints play a key role in reducing environmental pollution, but have their own defects.
[0004] Patent No: US8916181B1 describes composition of mixture of volatile organic solvent, binder polymer, glitter particles, rheology modifier and propellant. This composition contains hydrocarbons as propellant which is highly flammable. The volatile organic solvents used in this composition are toxic and have adverse effect on the environment and the user. Limitation: Synergistic use of volatile organic solvent with hydrocarbons makes the composition highly flammable and unsafe for indoor application. Volatile organic solvents used in the composition makes it adverse for the environment and the user and also restricts the use of the composition in the indoor environment. Substrate suitability is not mentioned.
[0005] Patent No: 6649686 describes the composition of decorative component along with mixture of solvents, alkali swellable adhesive, a surfactant, biocide, glycol and a defoamer. The composition is completely washable from fabric which is undesirable for the art users. It also uses PVA as one of the adhesives in the composition. Limitation: The composition limits the user to achieve wash durable effect on textile. Propellant free composition is not suitable for substrates other than textile due to their low vertical cling property (sagging behaviour) after spraying. PVA hardens the textile surfaces and makes it rough for touch.
[0006] Patent No: US3819119A describes the use of different colours of glitter particles and use of binder system, propellant and solvent in the formulation. Limitations: Use of hydrocarbon as propellant along with solvent creates the composition unsafe for indoor application. Substrate suitability is not mentioned.
[0007] Patent No: US5071900A describes a composition of a film former, a thickening agent, water, pigment and propellant. The propellant used is Dimethyl ether. The composition is water based. Limitations: The invention does not speak about the suitability of glitter particles in the aerosol composition. Substrate suitability is not mentioned.
[0008] Patent No: US4859242A describes a composition that comprises a water-soluble paint, water, polymeric thickener, sparkle or glitter, water soluble wax and colouring agents. The composition is focused on water-based glitter formulations. Limitations: The invention is not focused on the aerosol spray formulation application
[0009] Patent No: US20160002475A1 describes a water-based paint composition for aerosol cans with the use of Dimethyl ether as a propellant and the paint component with water as a solvent. Limitations: The invention has not pointed out the odor levels in the formulation and substrate suitability and durability levels. The invention, also, doesn’t address the non-oxidizable glitter particles and the process in detail.
[0010] There is a continuing need for development of eco-friendly, odourless, water-based glitter paint compositions that provide an improved cling property on surfaces like metal, glass, paper, plastic, and the like.

OBJECTIVE OF THE INVENTION
[0011] An object of the present invention is to provide a glitter paint composition that is free of odor-producing organic solvents.
[0012] An object of the present invention is to provide a water-based glitter paint composition.
[0013] An object of the present invention is to provide a water-based aerosol glitter spray paint composition.
[0014] An object of the present invention is to provide an eco-friendly water-based aerosol glitter spray paint composition.
[0015] An object of the present invention is to provide an eco-friendly water-based aerosol glitter spray paint composition comprising non-oxidizable glitter with fine particle size, variation in colours and having a good mechanical stability; and Dimethyl ether as propellant.
[0016] An object of the present invention is to provide an eco-friendly water-based aerosol glitter spray paint composition comprising water as a base solvent, solid components such as glitter, a resin system to hold the pigment and/or glitter, a rheology modifier to maintain the right rheology of the suspension, film forming polymers, anti-foaming and other ingredients.
[0017] Another object of the present invention is to provide an eco-friendly water-based aerosol glitter spray paint composition comprising,
a. water ranging from about 40% w/w to about 50% w/w;
b. acrylic styrene copolymer ranging from about 10% w/w to about 30% w/w;
c. polyurethane dispersion ranging from about 10% w/w to about 20% w/w;
d. coated alumina powder ranging from about 5% w/w to about 20% w/w;
e. modified silane ranging from about 0.2% w/w to about 1% w/w;
f. synthetic thickener ranging from about 0.1% w/w to about 2% w/w;
g. propylene glycol ranging from about 0.01% w/w to about 2% w/w;
h. glycerine ranging from about 0.05% w/w to about 2% w/w; and
i. dimethyl ether ranging from about 10% w/w to about 50% w/w.
[0018] Yet another object of the invention was to provide an aerosol spray container comprising the eco-friendly water-based aerosol glitter spray paint composition.
SUMMARY OF THE INVENTION
[0019] This summary is provided to introduce a selection of concepts in a simplified form that are further described below in Detailed Description section. This summary is not intended to identify key features or essential features of the claimed subject matter, nor is it intended to be used as an aid in determining the scope of the claimed subject matter.
[0020] In an aspect, the present disclosure relates to a glitter spray paint composition.
[0021] In an aspect, the present disclosure relates to a water-based glitter spray paint composition.
[0022] In an aspect, the present disclosure relates to a water-based aerosol glitter spray paint composition.
[0023] In an aspect, the present disclosure relates to an eco-friendly water-based aerosol glitter spray paint composition.
[0024] In an aspect, the present disclosure relates to an eco-friendly water-based aerosol glitter spray paint composition comprising non-oxidizable glitter with fine particle size, variation in colours and having a good mechanical stability; and Dimethyl ether as propellant.
[0025] In another aspect, the present disclosure relates to an eco-friendly water-based aerosol glitter spray paint composition that is odorless or produces negligible odor.
[0026] In another aspect, the present disclosure relates to a water-soluble paint composition comprising water as a base solvent, solid components such as pigment and/or glitter, a resin system to hold the pigment and/or glitter, a rheology modifier to maintain the right rheology of the suspension, film forming polymers, anti-foaming and other ingredients.
[0027] Other aspects of the invention will be set forth in the description which follows, and in part will be apparent from the description, or may be learnt by the practice of the invention.

DETAILED DESCRIPTION
[0028] The following is a detailed description of embodiments of the disclosure. The embodiments are in such detail as to clearly communicate the disclosure. However, the amount of detail offered is not intended to limit the anticipated variations of embodiments; on the contrary, the intention is to cover all modifications, equivalents, and alternatives falling within the spirit and scope of the present disclosure as defined by the appended claims.
[0029] All publications herein are incorporated by reference to the same extent as if each individual publication or patent application were specifically and individually indicated to be incorporated by reference. Where a definition or use of a term in an incorporated reference is inconsistent or contrary to the definition of that term provided herein, the definition of that term provided herein applies and the definition of that term in the reference does not apply.
[0030] Reference throughout this specification to “one embodiment” or “an embodiment” means that a particular feature, structure or characteristic described in connection with the embodiment is included in at least one embodiment. Thus, the appearances of the phrases “in one embodiment” or “in an embodiment” in various places throughout this specification are not necessarily all referring to the same embodiment. Furthermore, the particular features, structures, or characteristics may be combined in any suitable manner in one or more embodiments.
[0031] In some embodiments, numbers have been used for quantifying weight percentages, angles, and so forth, to describe and claim certain embodiments of the invention and are to be understood as being modified in some instances by the term “about.” Accordingly, in some embodiments, the numerical parameters set forth in the written description and attached claims are approximations that can vary depending upon the desired properties sought to be obtained by a particular embodiment. In some embodiments, the numerical parameters should be construed in light of the number of reported significant digits and by applying ordinary rounding techniques. Notwithstanding that the numerical ranges and parameters setting forth the broad scope of some embodiments of the invention are approximations, the numerical values set forth in the specific examples are reported as precisely as practicable. The numerical values presented in some embodiments of the invention may contain certain errors necessarily resulting from the standard deviation found in their respective testing measurements.
[0032] Various terms as used herein are shown below. To the extent a term used in a claim is not defined below, it should be given the broadest definition persons in the pertinent art have given that term as reflected in printed publications and issued patents at the time of filing.
[0033] As used in the description herein and throughout the claims that follow, the meaning of “a,” “an,” and “the” includes plural reference unless the context clearly dictates otherwise. Also, as used in the description herein, the meaning of “in” includes “in” and “on” unless the context clearly dictates otherwise.
[0034] Unless the context requires otherwise, throughout the specification which follow, the word “comprise” and variations thereof, such as, “comprises” and “comprising” are to be construed in an open, inclusive sense that is as “including, but not limited to.”
[0035] The recitation of ranges of values herein is merely intended to serve as a shorthand method of referring individually to each separate value falling within the range. Unless otherwise indicated herein, each individual value is incorporated into the specification as if it were individually recited herein.
[0036] All methods described herein can be performed in any suitable order unless otherwise indicated herein or otherwise clearly contradicted by context. The use of any and all examples, or exemplary language (e.g. “such as”) provided with respect to certain embodiments herein is intended merely to better illuminate the invention and does not pose a limitation on the scope of the invention otherwise claimed. No language in the specification should be construed as indicating any non-claimed element essential to the practice of the invention.
[0037] Groupings of alternative elements or embodiments of the invention disclosed herein are not to be construed as limitations. Each group member can be referred to and claimed individually or in any combination with other members of the group or other elements found herein. One or more members of a group can be included in, or deleted from, a group for reasons of convenience and/or patentability. When any such inclusion or deletion occurs, the specification is herein deemed to contain the group as modified.
[0038] The description that follows, and the embodiments described therein, is provided by way of illustration of an example, or examples, of particular embodiments of the principles and aspects of the present disclosure. These examples are provided for the purposes of explanation, and not of limitation, of those principles and of the disclosure.
[0039] The headings and abstract of the invention provided herein are for convenience only and do not interpret the scope or meaning of the embodiments.
[0040] The following discussion provides many example embodiments of the inventive subject matter. Although each embodiment represents a single combination of inventive elements, the inventive subject matter is considered to include all possible combinations of the disclosed elements. Thus if one embodiment comprises elements A, B, and C, and a second embodiment comprises elements B and D, then the inventive subject matter is also considered to include other remaining combinations of A, B, C, or D, even if not explicitly disclosed.
[0041] While a particular form of the invention has been illustrated and described, it will be apparent that various modifications can be made without departing from the spirit and scope of the invention.
[0042] The present disclosure generally relates to an eco-friendly water-based aerosol glitter spray paint composition.
[0043] In an embodiment of the present invention, the glitter paint composition comprises water as a base solvent, solid components such as glitter, a resin system to hold the pigment and/or glitter, a rheology modifier to maintain the right rheology of the suspension, film forming polymers, anti-foaming and other ingredients.
[0044] In an embodiment of the present invention, the resin system is selected from but not limited to water-soluble resin selected from but not limiting to polyester resins, alkyd resins such as those formed by combining polybasic acids or their anhydrides with a polyhydric alcohol, modified alkyd resins such as those formed by substituting acrylic acid for a portion of the polybasic acid, vinyl resins, vinyl-modified polyester resins and vinyl-modified alkyd resins, polyurethane with a polymerizable unsaturated monomer in water, acrylic latexes which may be a water soluble interpolymer of units from at least one neutral free radical polymerizable ester having a vinylidene group attached to the functional group, melamine, polyethylene, and the like. A blend of multiple resin systems depending on the functionality and the end use on the substrate may also be used.
[0045] In an embodiment of the present invention, the film former is selected from but not limited to acrylic, styrene, acrylic styrene copolymers, butyl ethyl acrylic copolymer, and the like. Preferably film former is acrylic copolymer and more preferably an acrylic styrene copolymer.
[0046] In an embodiment of the present invention, the rheology / viscosity modifier is selected from but not limited to polymeric thickeners, xanthan gum, alginates, guar gum, modified guar gum, and the like. More preferably a carboxyvinyl polymer.
[0047] In an embodiment of the present invention, the glitter is selected from but not limited to metallic or non-metallic particles including aluminum flake, mica, tin flake, gold flake, metallic titanium flake, nickel flake, titanium dioxide, mica, oxides of iron, bismuth oxychlorides, bronze, copper or alloy, coated polyester, coated alumina, gold, silver, and the like. More preferably alumina or pigment coated alumina or polyester or pigment coated polyester.
[0048] In a preferred embodiment of the present invention, the glitter is non-oxidizable glitter, selected from but not limited to coated polyester particles, coated aluminum particles, and the like.
[0049] In an embodiment of the present invention, the glitter may be used as microparticles that have wider ranges of sizes. In some embodiments, the microparticles may have a diameter of at least about 1 µm, 2 µm, 3 µm, 4 µm, 5 µm, 6 µm, 7 µm, 8 µm, 9 µm, 10 µm, 11 µm, 12 µm, 13 µm, 14 µm, 15 µm, 16 µm, 17 µm, 18 µm, 19 µm, 20 µm, 25 µm, 30 µm, 35 µm, 40 µm, 45 µm, 50 µm, 55 µm, 60 µm, 65 µm, or at least 70 µm. Preferably between 5 to 40 µm and more preferably between 10 to 30 µm.
[0050] In an embodiment of the present invention, the anti-foaming agent is selected from but not limited to silicones, modified silanes, silicone-modified mineral oils, acrylic agents and the like. More preferably a modified silane.
[0051] In an embodiment of the present invention, water is present in at least 5% w/w, at least 10% w/w, least 15% w/w, at least 20% w/w, at least 25% w/w, at least 30% w/w, at least 35% w/w, at least 40% w/w, at least 15% w/w, at least 50% w/w, at least 55% w/w, at least 60% w/w, at least 65% w/w, at least 70% w/w, at least 75% w/w, at least 80% w/w, at least 85% w/w, or at least 90% w/w. Most preferably 40 to 50% w/w.
[0052] In an embodiment of the present invention, the resin system is present in at least 5% w/w, at least 10% w/w, at least 11% w/w, at least 12% w/w, at least 13% w/w, at least 14% w/w, at least 15% w/w, at least 16% w/w, at least 17% w/w, at least 18% w/w, at least 19% w/w, at least 20% w/w, or at least 25% w/w. Most preferably 11 to 15% w/w.
[0053] In an embodiment of the present invention, the film former is present in at least 5% w/w, at least 10% w/w, at least 11% w/w, at least 12% w/w, at least 13% w/w, at least 14% w/w, at least 15% w/w, at least 16% w/w, at least 17% w/w, at least 18% w/w, at least 19% w/w, at least 20% w/w, at least 25% w/w, or at least 30% w/w. Most preferably 10 to 15% w/w.
[0054] In an embodiment of the present invention, the rheology / viscosity modifier is present in at least 0.1% w/w, at least 0.2% w/w, least 0.3% w/w, at least 0.5% w/w, at least 0.6% w/w, at least 0.7% w/w, at least 0.8% w/w, at least 0.9% w/w, at least 1% w/w, at least 1.1% w/w, at least 1.2% w/w, at least 1.3% w/w, at least 1.4% w/w, at least 1.5% w/w, at least 1.6% w/w, at least 1.7% w/w, at least 1.8% w/w, or at least 2% w/w. Most preferably 0.5 to 1.5% w/w.
[0055] In an embodiment of the present invention, the glitter is present in at least 5% w/w, at least 6% w/w, at least 7% w/w, at least 8% w/w, at least 9% w/w, at least 10% w/w, at least 11% w/w, at least 12% w/w, at least 13% w/w, at least 14% w/w, at least 15% w/w, at least 16% w/w, at least 17% w/w, at least 18% w/w, at least 19% w/w, at least 20% w/w, or at least 25% w/w. Most preferably 7 to 15% w/w.
[0056] In an embodiment of the present invention, the anti-foaming agent is present in at least 0.1% w/w, at least 0.2% w/w, least 0.3% w/w, at least 0.5% w/w, at least 0.6% w/w, at least 0.7% w/w, at least 0.8% w/w, at least 0.9% w/w, at least 1% w/w, at least 1.1% w/w, at least 1.2% w/w, at least 1.3% w/w, at least 1.4% w/w, at least 1.5% w/w, at least 1.6% w/w, at least 1.7% w/w, at least 1.8% w/w, or at least 2% w/w. Most preferably 0.3 to 0.6% w/w.
[0057] In an embodiment of the present invention, the paint composition may further comprise pigment selected from but not limited to color pigments such as graphite, chromium oxide, iron oxide, carbon black, phthalocyanine pigments, quinacridone pigments, and the like; and extender pigments such as calcium carbonate, magnesium carbonate, barium sulfate, silicate salts, alumina hydrate, calcium sulfate, and the like.
[0058] In an embodiment of the present invention, the glitter paint composition may further comprise anti-freeze agents, curing catalysts, surface modifiers, dispersing agents, and the like.
[0059] In an embodiment of the present invention, the anti-freeze agent is polyol. Preferably diol and more preferably glycerol.
[0060] In an embodiment of the present invention, the glitter paint composition may be applied on a variety of surfaces like textile, paper, metal, plastic, glass, and the like.
[0061] In an embodiment of the present invention, the glitter paint composition can be stored in an aerosol spray container.
[0062] In an embodiment of the present invention, the aerosol spray container is made of tin or aluminum. More preferably a coated aluminum container.
[0063] In an embodiment of the present invention, the aerosol spray container comprises an actuator orifice of diameter above 0.15 mm, more preferably above 0.25 mm.
[0064] In an embodiment of the present invention, the glitter paint composition is an eco-friendly glitter paint composition.
[0065] In an embodiment of the present invention, the glitter paint composition is an eco-friendly paint composition that is odorless or produces negligible odor.
[0066] In an embodiment of the present invention, the glitter paint composition comprises a propellant, preferably dimethyl ether.
[0067] In an embodiment, the present disclosure provides a method for producing eco-friendly water-based aerosol glitter spray paint composition, said method comprising the steps of:
Film former is slowly added in water in the reactor. The components are mixed until a homogenous mixture is achieved. The anti-foaming and de-aerating agent is then added slowly to remove all the foam and bubbles generated in the homogenous mix. The resin is then added in the mixture and stirred until homogenous.
The particle size of the glitter powder was grounded well in a grinder and particles below 60 microns were filtered out. The process of grinding of the glitter particles was repeated and continued until the particle size achieved was below 50 microns, preferably between 5 to 40 microns and further preferable between 10 to 30 microns.
Glitter powders are then added slowly in recirculation followed by addition of rheology modifier. The composition then undergoes the homogenization process to give a perfectly dispersed glitter formulation which is the glitter part.
The glitter part composition is then filled in the can. A steel ball is added which is required to maintain good dispersion before spraying and the propellent is pumped to give pressure of 5 bar. This aerosol can which contains the composition with glitter part and the Dimethyl ether as propellent is now the water-based glitter aerosol spray.
The aerosol can is then shaken well to maintain the proper dispersion of glitter powder and sprayed on different surfaces like textile, paper, metal, glass and plastic to check the efficiency, the effect yield, the durability and odour after spraying.
[0068] While the foregoing describes various embodiments of the disclosure, other and further embodiments of the disclosure may be devised without departing from the basic scope thereof. The scope of the invention is determined by the claims that follow. The invention is not limited to the described embodiments, versions or examples, which are included to enable a person having ordinary skill in the art to make and use the invention when combined with information and knowledge available to the person having ordinary skill in the art.
[0069] In an embodiment, the eco-friendly water-based aerosol glitter spray paint composition of the present invention maybe used in any manner known to a person skilled in the art.
EXAMPLES
[0070] The present disclosure is further explained in the form of following examples. However, it is to be understood that the foregoing examples are merely illustrative and are not to be taken as limitations upon the scope of the invention. Various changes and modifications to the disclosed embodiments will be apparent to those skilled in the art. Such changes and modifications may be made without departing from the scope of the invention.
[0071] Example 1: Aerosol spray paint composition 1
Water : 43.5 g
Acrylic Styrene Copolymer : 11.18 g
Polyethylene dispersion : 13.09 g
Gold Bronze Alloy powder : 8.25 g
Anti-foam : 0.48 g
Synthetic Thickener : 0.9 g
Glycerine : 0.4 g
Propylene glycol : 0.5 g
Dimethyl ether : 22.6 g
The composition is evenly dispersed and homogenous.
The composition of aerosol glitter spray is found to be odourless when sprayed on textile, metal, glass, plastic and paper.
The composition when sprayed on textile and then air-dried gives washing durability of 2 home laundering cycles. However, when the composition is sprayed on textile and then dried at 80 deg C in a dryer or when dried using a hot gun with temperature up to 90 deg C for 5 minutes, the durability to washing goes up to 5 home laundering cycles with a rating of 3 as per ISO standards.
The composition when sprayed on textile, metal, glass and paper and baked at a temperature of 1200C for 4 min or when the composition is sprayed on textile and washed with water, blackening of gold powder was observed which is a result of oxidation, and the gold particles became dark yellow in colour.
The composition when sprayed on textile, metal, glass, plastic and paper and then air dried, a good soft touch was felt.
The composition when sprayed was soft and uniform effect was seen on the surface.
[0072] Example 2: Aerosol spray paint composition 2
Water : 41.5 g
Acrylic Styrene Copolymer : 13.09 g
Polyurethane dispersion : 12.09 g
Gold Coated Alumina powder : 7.54 g
Anti-foam : 0.38 g
Synthetic Thickener : 0.8 g
Propylene glycol : 0.25 g
Glycerine : 0.5 g
Dimethyl ether : 24.6 g

The composition is evenly dispersed and homogenous.
The composition of aerosol glitter spray is found to be odourless when sprayed on textile, metal, glass, plastic and paper.
The composition when sprayed on textile and then air-dried gives washing durability of 2 home laundering cycles. However, when the composition is sprayed on textile and then dried at 80 deg C in a dryer or when dried using a hot gun with temperature upto 90 deg C for a time of 5 minutes, the durability to washing goes up to 5 home laundering cycles with a rating of 3 as per ISO standards
The composition when sprayed on textile, metal, glass and paper and baked at a temperature of 120 deg C for 4 min or when the composition is sprayed on textile and washed with water, no oxidation was observed, and the gold particles remained yellow gold in colour.
The composition when sprayed on textile, metal, glass, plastic and paper and then air dried, a good soft touch was felt.
The composition when sprayed was soft and uniform effect was seen on the surface.
[0073] Example 3: Aerosol spray paint composition 3
Water : 45.1 g
Acrylic copolymer : 10.09 g
Polyvinyl alcohol : 15.09 g
Gold Coated Polyester powder : 8.04 g
Anti-foam : 0.35 g
Synthetic Thickener : 0.83 g
Propylene glycol : 0.25 g
Glycerine : 0.5 g
Dimethyl ether : 21.5 g

The composition is evenly dispersed and homogenous.
The composition of aerosol glitter spray is found to have odour when sprayed on textile, metal, glass, plastic and paper.
The composition when sprayed on textile and then air-dried gives washing durability of 3 home laundering cycles. However, when the composition is sprayed on textile and then dried at 80 deg C in a dryer or when dried using a hot gun with temperature upto 90 deg C for a time of 5 minutes, the durability to washing goes up to 7 home laundering cycles with a rating of 3 as per ISO standard.
The composition when sprayed on textile, metal, glass and paper and baked at a temperature of 120 deg C for 4 min or when the composition is sprayed on textile and washed with water, no oxidation was observed, and the gold particles remained yellow gold in colour.
The composition when sprayed on textile and paper and then air dried, a harsh touch was felt. The composition when sprayed on metal, glass and plastic and then air dried, soft touch was felt.
The composition when sprayed was soft and uniform effect was seen on the surface.

[0074] Example 4: Aerosol spray paint composition 4
Water : 46.5 g
Acrylic Styrene Copolymer : 14 g
Melamine : 4 g
Coloured Alumina powder : 7 g
Anti-foam : 0.3 g
Synthetic Thickener : 1 g
Propylene Glycol : 0.25 g
Dimethyl ether : 27.2 g

The composition is evenly dispersed and homogenous.
The composition of aerosol glitter spray is found to have no odour when sprayed on textile, metal, glass, plastic and paper.
The composition when sprayed on textile and then air-dried gives washing durability of 3 home laundering cycles. However, when the composition is sprayed on textile and then dried at 80 deg C in a dryer or when dried using a hot gun with temperature upto 90 deg C for a time of 5 minutes, the durability to washing goes up to 9 home laundering cycles with a rating of 4 as per ISO standard.
The composition when sprayed on textile, metal, glass and paper and baked at a temperature of 120 deg C for 4 min or when the composition is sprayed on textile and washed with water, no oxidation was observed, and the original colour of the coated glitter particles remained the same in appearance.
The composition when sprayed on textile and paper and then air dried, the substrate felt mildly harsh. The composition when sprayed on metal, glass and plastic and then air dried, soft touch was felt.
The composition when sprayed was not very smooth and uniformity during spraying was hampered.

Documents

Application Documents

# Name Date
1 202121033217-FORM 4 [23-01-2025(online)].pdf 2025-01-23
1 202121033217-IntimationOfGrant18-02-2022.pdf 2022-02-18
1 202121033217-STATEMENT OF UNDERTAKING (FORM 3) [23-07-2021(online)].pdf 2021-07-23
2 202121033217-REQUEST FOR EARLY PUBLICATION(FORM-9) [23-07-2021(online)].pdf 2021-07-23
2 202121033217-PatentCertificate18-02-2022.pdf 2022-02-18
2 202121033217-IntimationOfGrant18-02-2022.pdf 2022-02-18
3 202121033217-CLAIMS [09-11-2021(online)].pdf 2021-11-09
3 202121033217-PatentCertificate18-02-2022.pdf 2022-02-18
3 202121033217-POWER OF AUTHORITY [23-07-2021(online)].pdf 2021-07-23
4 202121033217-CLAIMS [09-11-2021(online)].pdf 2021-11-09
4 202121033217-CORRESPONDENCE [09-11-2021(online)].pdf 2021-11-09
4 202121033217-FORM-9 [23-07-2021(online)].pdf 2021-07-23
5 202121033217-FORM FOR STARTUP [23-07-2021(online)].pdf 2021-07-23
5 202121033217-FER_SER_REPLY [09-11-2021(online)].pdf 2021-11-09
5 202121033217-CORRESPONDENCE [09-11-2021(online)].pdf 2021-11-09
6 202121033217-FORM FOR SMALL ENTITY(FORM-28) [23-07-2021(online)].pdf 2021-07-23
6 202121033217-FER_SER_REPLY [09-11-2021(online)].pdf 2021-11-09
6 202121033217-FER.pdf 2021-10-19
7 202121033217-FORM-26 [17-09-2021(online)].pdf 2021-09-17
7 202121033217-FORM 1 [23-07-2021(online)].pdf 2021-07-23
7 202121033217-FER.pdf 2021-10-19
8 202121033217-EVIDENCE FOR REGISTRATION UNDER SSI(FORM-28) [23-07-2021(online)].pdf 2021-07-23
8 202121033217-FORM 18A [26-07-2021(online)].pdf 2021-07-26
8 202121033217-FORM-26 [17-09-2021(online)].pdf 2021-09-17
9 202121033217-EVIDENCE FOR REGISTRATION UNDER SSI [23-07-2021(online)].pdf 2021-07-23
9 202121033217-FORM 18A [26-07-2021(online)].pdf 2021-07-26
9 202121033217-FORM28 [26-07-2021(online)].pdf 2021-07-26
10 202121033217-DECLARATION OF INVENTORSHIP (FORM 5) [23-07-2021(online)].pdf 2021-07-23
10 202121033217-FORM28 [26-07-2021(online)].pdf 2021-07-26
10 202121033217-STARTUP [26-07-2021(online)].pdf 2021-07-26
11 202121033217-COMPLETE SPECIFICATION [23-07-2021(online)].pdf 2021-07-23
11 202121033217-STARTUP [26-07-2021(online)].pdf 2021-07-26
12 202121033217-COMPLETE SPECIFICATION [23-07-2021(online)].pdf 2021-07-23
12 202121033217-DECLARATION OF INVENTORSHIP (FORM 5) [23-07-2021(online)].pdf 2021-07-23
12 202121033217-STARTUP [26-07-2021(online)].pdf 2021-07-26
13 202121033217-DECLARATION OF INVENTORSHIP (FORM 5) [23-07-2021(online)].pdf 2021-07-23
13 202121033217-EVIDENCE FOR REGISTRATION UNDER SSI [23-07-2021(online)].pdf 2021-07-23
13 202121033217-FORM28 [26-07-2021(online)].pdf 2021-07-26
14 202121033217-FORM 18A [26-07-2021(online)].pdf 2021-07-26
14 202121033217-EVIDENCE FOR REGISTRATION UNDER SSI(FORM-28) [23-07-2021(online)].pdf 2021-07-23
14 202121033217-EVIDENCE FOR REGISTRATION UNDER SSI [23-07-2021(online)].pdf 2021-07-23
15 202121033217-EVIDENCE FOR REGISTRATION UNDER SSI(FORM-28) [23-07-2021(online)].pdf 2021-07-23
15 202121033217-FORM 1 [23-07-2021(online)].pdf 2021-07-23
15 202121033217-FORM-26 [17-09-2021(online)].pdf 2021-09-17
16 202121033217-FER.pdf 2021-10-19
16 202121033217-FORM 1 [23-07-2021(online)].pdf 2021-07-23
16 202121033217-FORM FOR SMALL ENTITY(FORM-28) [23-07-2021(online)].pdf 2021-07-23
17 202121033217-FER_SER_REPLY [09-11-2021(online)].pdf 2021-11-09
17 202121033217-FORM FOR SMALL ENTITY(FORM-28) [23-07-2021(online)].pdf 2021-07-23
17 202121033217-FORM FOR STARTUP [23-07-2021(online)].pdf 2021-07-23
18 202121033217-CORRESPONDENCE [09-11-2021(online)].pdf 2021-11-09
18 202121033217-FORM-9 [23-07-2021(online)].pdf 2021-07-23
18 202121033217-FORM FOR STARTUP [23-07-2021(online)].pdf 2021-07-23
19 202121033217-FORM-9 [23-07-2021(online)].pdf 2021-07-23
19 202121033217-POWER OF AUTHORITY [23-07-2021(online)].pdf 2021-07-23
19 202121033217-CLAIMS [09-11-2021(online)].pdf 2021-11-09
20 202121033217-REQUEST FOR EARLY PUBLICATION(FORM-9) [23-07-2021(online)].pdf 2021-07-23
20 202121033217-POWER OF AUTHORITY [23-07-2021(online)].pdf 2021-07-23
20 202121033217-PatentCertificate18-02-2022.pdf 2022-02-18
21 202121033217-IntimationOfGrant18-02-2022.pdf 2022-02-18
21 202121033217-REQUEST FOR EARLY PUBLICATION(FORM-9) [23-07-2021(online)].pdf 2021-07-23
21 202121033217-STATEMENT OF UNDERTAKING (FORM 3) [23-07-2021(online)].pdf 2021-07-23
22 202121033217-FORM 4 [23-01-2025(online)].pdf 2025-01-23
22 202121033217-STATEMENT OF UNDERTAKING (FORM 3) [23-07-2021(online)].pdf 2021-07-23

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