Specification
OSP-6 1399 English Specification Draft
[Document Type] Specification
['ritle of the In\rention] METIIOD OF PRODUCING ROUGHLY SHAPED
MATERIAL FOR ROLLING BEARING
[Teclu~icaFl ield of the Invention]
[OOOI]
The present invention relates to a method of producing a roughly shaped
material for a rolling bearing.
Priority is claimed on Japanese Patent Application No. 2013-23 1292, filed on
November 7,201 3, the content of \vhich is incorporated herein by reference.
[Related Art]
[0002]
For exatnple~ash own in FIG. 11( A), a roughly shaped material forformation
of a bearing ring of a rolling bearing that is used in automobiles, industrial machinery,
and the like is produced by a method including a process (hot forging) of heating steel
composed of high-carbon clronle bearing steel to a forging temperature in a range of
1 100°C to 1200°C and perfornling plastic working with respect to the steel, a process
of cooling a forged article that is obtained, and a process of performing an annealing
treatment in u~hichth e forged article after cooling is heated to a soaking temperature in
a range of 780°C to 810°C, and the forged article that is heated is slowly cooled down.
In the method, after hot forging and cooling are performed to allow cementite to
precipitate (refer to FIG. 1 l(B)), it is necessary to spheroidize cementite by performing
an annealing treatment for 15 hours to 16 hours (refer to FIG. 11 (B)). Accordingly,
the method has a disadvantage in that a long period of time is taken for production of
the roughly shaped material.
[0003]
OSP-61399 English Specification Draft
Accordingl~: so as to shorten the tinle required for production of the roughly
shaped material, some of the present inventors have suggested a method of shorteni~lg
or onlitting the spheroidizing a~inealitigb y heating steel composed of high-carbon
clxome bearing steel to a temperature T in a range ofAel point to (Aem point+5O0C)
\vl~ilec ontrolling a heating rate so that the heating rate in a tempe~aturera nge of 600°C
or higher is set to 10 "C/s or greater, and forging the steel at a temperature in a range of
(Arl poi1lt+150~C)to Arl point in 10 minutes after reaching the tetnperatore T (for
exa~nplere fer to Patent Document 1).
[Prior Art Document]
[Patent Documcnt]
[0004]
[ ~ a G tD~otc utnetit 11 Japanese Unexamit~edP atent Application, First
Publication No. 2009-242 18
[Disclosure of the Irnretltion]
[Problems to be Solved by the Invention]
[0005]
According to the tnethod described in Patent Document 1, a spheroidal
cementite structure, which is fortned tl~~ougsphli eroidizing annealing in the related art,
can be formed by performing only forging without performing spheroidizing annealing.
Accordingly, it is possible to shorten or omit the annealing treatment for a long period
of time (15 hours to 16 hours). However, in the method described in Patent
Document 1, in a case where steel co~nposedo f high-carbon chsotiie bearing steel is
forged at a telnperature in a range of (Art point+l5O0C) to Art point, a desired
spheroidal cementite structure is obtained, but grains of ferrite, \vhich is a matrix
structure, are considerably refined depending on forging conditions or a portion of the
OSP-61399 English Specification Draft
roughly shaped matcrial that is obtained tllmngh forging. Along with the refi~lcment,
hardness may rise to approximately Hw.350 to 11~400. I11 this case, machinability map
decrease in accordance with the rising of the hardness, or additional processing may be
difficult.
[0006]
The invention has been made in consideration of the above-described
circumference, and an object thereof is to provide a method of producing a roughly
shaped material for a rolling bearing, which is capable of producing the roughly shaped
material capable of stably securing satisfactory machinabilit~: in a short period of time.
[Means for Solving the Problenii]
[0007]
Accordi~igto an aspect of the invention, there is przided a method of
producing a roughly shaped material for a rolling bearing by forging a steel composed
of a high-carbon chrome bearing steel containing 0.7 mass% to 1.2 mass% of a carbon,
and 0.8 mass% to 1.8 mass% of a chromium. The method includes (A) forging the
steel to a predetermined shape \vliile heating the steel to a forging temperature in a
range of (Ael point+25"C) to (Ael point+l05C), and cooling a forged article to a
temperature of Ael point or lower, and (B) performing an annealing in which the
forged article obtained in (A) is heated to a soaking temperature in a range of (Ael
point+2S0C) to (Ael poillt+85"C), the forged article is retained for 0.5 hours or longel;
and the forged article is cooled down to 700°C or lower at a coolitig rate of 0.30 "CIS or
slower.
[OOOS]
According to the method of producing a roughly shaped material for a rolliilg
bearing of the invention, it1 the process (A), the steel composed of high-carbon clu.oine
OSP-6 1399 Englisli Specification Drafl
bearing steel is forged (warn forged) at a forging temperatnre in a range of (Ael
point+25"C) to (Ael point+l05"C), al~dis cooled down to a temperature of Ael point or
loxvcr to form fine spheroidal cementite in a state of being dispersed in a structure of
steel. Then, in tlie process (B), the forged article that is obtained is retained at a
soaking temperature in a range of (Ael pointt25"C) to (Ael point+85OC) for 0.5 11ours
or longer and is cooled down to 700°C or lower at a cooling rate of 0.30 "CIS or slower
so as to grow the fine splleroidal cementite to a relatively large size. Accordingly, it
is possible to fu12lier sliorteti the production time in comparison to a production method
in the related art in which steel is subjected to plastic working (hot forging) by heating
the steel to a forging temperature of 1100°C to 1200°C. Furtlierniore, it is possible to
obtain a roughly shaped material capable of securing satisfactory machinability during
production of bearitig rings and the like.
In the method of the related art (method described in Patent Document l),
steel composed of high-carbon chrome bearing steel is forged at a temperature it1 a
range of (Arl point+l5O0C) to Arl point to form spheroidal cenientite. However, in
the method of the related art, even when the steel is forged under desired conditions, a
locally fine ferrite structnre is fornled due to heat extraction through contact with a die
or air, and the like. Therefore, a variatio~is likely to occur in a distribution of
hardness due toa fine structure, in a state of a microstmcture, and a distribution of the
a~nouuot f residual austenite after a quenching and te~nperingtr eatment (hereinafter,
also referred to as "QT" treatment) due to unevenness of the microstructure.
However, according to tlie method of producing a roughly shaped material for a rolling
bearing of tlie invention, after forging and cooling (the process A), the forged article
that is obtained is annealed by retaining the forged article at a soaking temperature in a
range of (Ael point+25'C) to (Ael point+85"C) for 0.5 honrs or longel; and by cooling
OSP-61399 English Specification Draft
the forged article to 700°C or lower at a cooling rate of 0.30 "CIS or slower.
Accordingly, it is possible to effectively suppress occulrence of a variation in the
distribution of hardness, the state of the microstructore, and the distribution of the
amount of residual anstenite after the QT treatment.
[0009]
In the method of producing a ronglily sliaped material for a rolling bearing of
the invention, it is preferable that the soaking tetnperatnre in the process (B) is set to
760°C to 820°C. In this case, it is possible to more efficiently grow the spheroidal
cementite.
In addition, iu the method of producing a mughly shaped material for a rolling
bearing of the invention, it is preferable that the cooling rate in the process (B) is set to
0.30 "CIS or slo\ver. In this case, formation of sheet-shaped or layered cenlentite is
suppressed. Accordingly, it is possible to more efficiently grow the spheroidal
cementite.
[Effects of the Invention]
[OOlO]
According to the method of producing a roughly shaped material for a rolling
bearing of the invention, it is possible to produce a roughly shaped material capable of
securing n~achinabilityin a sliol-t period of titne.
[Brief Description of the Drav.~ings]
[OOI 11
FIG. 1 is a cross-sectional view of a rolling bearing including bearing rings
\vI~icha re foinled by a rouglily shaped material for bearing rings which is produced by
a production method according to an e~nbodimetito f the invention.
FIG. 2 is a process diagram showing a sequence and heat treatment conditions
OSP-61399 English Specification Draft
of the prodoction method according to the ctllbodi~llento f the invention.
FIG. 3 is a process diagram showing a sequence of a warn1 forging process in
the production method according to the enlbodin~enot f the invention.
FIG. 4 is a drawing-substituting photograph showing results obtained by
observing a st~~lctusrtea te in each process of the production method according to the
embodinlent of the invention, (A) is a draxxring-substihlti~tillpg hotograph of a steel
structure before the warm forging process, (B) is a drawing-substituting photograph of
a structure of a forged article at the time of terminating the warm forging process, and
(C) is a drawing-substituting photogaph of a structure of a roughly shaped material for
bearing rings which is obtained after an annealing process.
FIG. 5 is a view showing results obtained by investigating a relationship
between a soaking temperature and hardness, and results obtained by observing a
structure of a roughly shaped material for bearing rings which is obtained after an
annealing process in Test Example 3. (a) is a graph showing the results obtained by
investigating the relationship between the soakiug temperature and the hardness, (b) is
a drawing-substituting photograph of the structure of the roughly shaped material for
bearing rings when the soaking tetnperature is set to 740C, (c) is a drawingsubstituting
photograph of tl~est ructure of the roughly shaped material for bearing
rings when the soaking temperature is set to 760°C, (d) is a drax41ing-substituti~lg
photograph of the strocture of the roughly shaped material for bearing rings ~vhenth e
soaking temperature is set to 820°C, and (e) is a drawing-substituti~lgp hotograph of the
structure of the roughly shaped material for bearing rings when the soaking
temperature is set to 840°C.
FIG. 6 is a view showitlg results obtained by investigating a relationship
between a cooling rate and hardness, and results obtained by observing a structure of a
OSP-61399 Englisli Specification Draft
roughly sliaped material for bearing rings \vI~icIi s obtained after an annealing process
in Test Example 5. (a) is a graph showing the results obtained by investigating the
relationship between the cooling rate and the hardness, (b) is a drawing-substituting
photograph of the sttxlcture of the ronglily shaped material for bearing rings when the
cooling rate is set to 7 "Clnli~(i 0.12 'Cis), (c) is a drawing-substituting photograpli of
the striicture of the roughly shaped material for bearing rings when the cooling rate is
set to 16 oC/ini~(l0 .27 "Cls), (d) is a drawing-substituting photograph of the structure
of the roughly sliaped material for bearing rings when the cooling rate is set to 26
"Clnlin (0.43 "Cis), and (e) is a drawing-substituting photograpli of the structure of the
roughly shaped material for bearing rings when the cooling rate is set to 93 OCImin
(I .55 'CIS).
FIG. 7 is a view showing results obtained by investigating a relationship
behveen a cooling temperature and hardness, atid results obtained by observing a
structure of a roughly shaped material for bearing rings which is obtained after an
annealing process it1 Test Example 6. (a) is a graph sho\ving the results obtained by
investigating the relationship between the cooling temperature and the hardtiess, (b) is
a drawing-substituting photograph of the structure of the roughly shaped material for
bearing rings when the cooling temperature is set to 650°C, (c) is a drawingsubstituting
photograpli of the structure of the rouglily shaped ~nateriafl or bearing
rings when the cooling temperature is set to 700°C, and (d) is a drawing-substituting
photograph of the structure of the roughly shaped material for bearing rings when the
cooling temperature is set to 730°C.
FIG. 8 is a diagram showing heat treatment conditio~isin Example 1.
FIG. 9 is a diagram showing heat treatment cotiditions in Exatnple 2.
FIG. 10 is a drawing-substituting photograph sho\ving results obtained by
OSP-61399 English Specification Draft
observing a stlx~ctureo f a forged article that is obtained after an annealing process in
Test Example 7. (a) is a drawing-substituting photogxaph sho~vinga result obtained
by observing a structure of a forged article in Exatnplc 1, and (b) is a drawingsubstituting
photograph showing a result obtained by observing a structure of a forged
article in Example 2.
FIG. 11 is a view showing heat treatrticnt conditions in a ~iletl~oodf p roducing
a roughly shaped material for bearing rings in the related art in which hot forging is
performed, and results obtained by observing a state of a structure in each process.
[Embodiments of the Lnvention]
[0012]
Hereinafter, a niethod (hereinafter, also simply referred to as "production
method") of a roughly shaped material for a rolling bearing i f the invention
will be described in detail with reference to the accot~~panyindgra wings.
FIG. 1 is a cross-sectional view of a rolling bearing includi~lgb earing rings
which are formed by a roughly shaped material for bearing rings wliich is produced by
a production method according to an ernbodimet~ot f the invetition. Furthermore, in
this embodiment, description will be given of a conical roller bearing as an example of
the rolling bearing, but the invention is not limited to the example. In addition, in this
embodiment, description will be given of a roughly shaped material for fornlation of
bearing rings (an inner ring and an outer ring) of the rolling bearing as at1 example of
the rougl~lys haped material. I-Iowever, the invention is not limited to the exatiiple,
and is also applicable to a roughly shaped material for formation of a rollitig body
(roller, ball).
A rolling bearing 1 sliown in FIG. 1 includes at1 i~lneri ng 11, an outer ring 12,
a plurality of rollers (rolling bodies) 13 \vhich are arranged between the inner and outer
OSP-61399 English Specification Draft
rings I I and 12, and a retainer 14 that retains the plttrality of rollers 13. The inner
ring 11 and the outer ring 12 of the rolling bearing 1 are fornled from a roughly shaped
material for bearing rings (a roughly shaped material for an inner ring and a roughly
shaped nlaterial for an outer ring) which is produced by the productioa method of the
invention.
[00 131
FIG. 2 is a process diagram showing a sequence and heat treatment cot~ditions
of the production tnethod according to the embodiment of the invention, FIG. 3 is a
process diagram showvitlg a sequence of a warm forging process in the production
tnethod according to the eelnbodinlent of the invention, and FIG. 4 is a drawingsubstituting
substituting photograph sl~owingre sults obtained by observing a structure in each
procession 6Oa that is formed at a lower side of the inner tubular portion
60 (refer to (b) in FIG. 3).
Then, in the separation and punching process, the inner tubular portion 60 of
the formed blank B2 is punched by using a punch (not shown), and the bottom portion
6Oa of the inner tubular pollion 60 is punched by using the punch, thereby separating a
forged article 51 for an outer ring and a forged article 61 for an inner ring from each
other, and separating the forged article 61 for an inner ring and the bottonl portion 6lb
from each other*to+fortn a prepared hole 61a in the forged article 61 for an inner ring
(refer to (c) in FIG. 3).
[00 191
After termination of forging, a forged article that is obtained is cooled down
to a temperature (cooling temperature) of Ael point or lower (refer to (a) in FIG. 2).
As described above, when the forged a~ticlteh at is obtained is cooled down to the
cooling temperature, it is possible to efficiently form fine spheroidal cementite. The
OSP-61399 Englisli Specilicatiot~ Draft
cooling temperature is Ael point or lowel; and is preferably 400°C or lowel; fro111 the
viewpoint of col~~pletecloyt npleting trat~sformnatiouo f an austenite strncture after
termination of forging so as to suppress for~~~atoifo an p earlite structure and forn~ation
of a martensite structure or a bainite structure which is an overcooled structure. In
addition, the cooling tenlperature is preferably room temperature (25°C) or higher from
the viewpoints of reducing a load on cooling facilities, improving production efficiency,
and reducing productio~c~os t.
A cooling rate when steel is cooled down to the cooling temperature can be
appropriately deter~ninedin accordance with a co~npositiono f steel, a forging shape,
and the like. Fut-thern~orei,n this specificatiot~t,h e "cooling temperature" represents
a cooling temperature at the central portion of steel.
-
[0020]
Tllrough the warm forging process, it is possible to form a structure (refer to
step (B) in FIG. 2, and FIG. 4(B)) in which fine spl~eroidacl ementite is dispersed afier
the \arm forging process (step (B) in FIG. 2) from a structure (refer to FIG. 4(A)) that
includes pearlite before the waml forging process (step (A) in FIG. 2).
[0021]
(Annealing Process)
In the at~nealit~pgro cess, first, the forged article, wvhich is obtained in the
war111 forging process, is heated until the temperature of the central portion of the
forged article reaches a soaking temperature in a range of (Ael point+2S0C) to (Aer
point+8S°C) (refer to (b) in FIG. 2).
[0022]
The soaking ten~peraturei s (Ael point+2S°C) or highel; and is preferably (Ael
point+3S°C) or highel; fsom the viewvpoint of obtaining a roughly shaped material
OSP-61399 English Specification Draft
capable of stably securing satisfactory macliinability. In addition, the soaking
temperature is (Ael point+8S0C) or lower, and is preferably (Ael point+7S0C) or lower,
fiom the vie\vpoitit of suppressirig fornlation of sheet-shaped or layered cementite.
Specifically, the soaking tetiperature is 760°C or higher, and is preferably 770°C or
highel; from the viewpoint of obtaining a roughly shaped material capable of securing
satisfactory machinability. The soaking temperature is 820°C or lowel; and is
preferably 810°C or lower, from the viewpoint of suppressing formation of sheetshaped
or layered cementite. Furthermore, in this specification, the "soaking
temperature" represents a soaking temperature at the central portion of steel.
A temperature rising rate ~vhenh eating steel to the soaking temperature can be
appropriately determined in accordance with a co~npositiono f steel, a forging shape,
and tlie like.
[0023 J
When a temperature at the central portion of the forged article reaches a
soaking tetnperature in a range of (Ael point+25"C) to (Ae, point+85'C), tlie forged
article is retained at the soaking temperature for 0.5 hours or longer (refer to (b) in FIG.
2).
The time (soaking time) for retention at the soaking temperature is preferably
1 .O hour or longer from the viewpoint of obtaining a roughly shaped material capable
of stably securing satisfactory macliinabilitj~. Fu~-thennoree, ven when the soaking
time is lengthened to be longer than 10 hours, an additional improvement in
characteristics of the roughly shaped material, which corresponds to a period of the
soaking time, is not exhibited. Therefore, it is preferable that the soaking time is as
shorter as possible from the viewpoiilt of sl~o~tenittihge production time. The tipper
limit of the soaking time is typically 5.0 lio~urso r shorten
OSP-61399 Etiglisli Specificatioti Draft
[0024]
After the forged article is retained at the soaking time for 0.5 hours or longer,
the forged article is cooled do\vti to a cooling temperature of 700°C or lower at a
cooling rate of 0.30 "Cls or slower (refer to (b) in FIG. 2).
The cooling rate is preferably 0.007 "CIS or fastel; and is Inore preferably
0.020 "CIS or faster, from the viewpoint of improving productivity (shortening of
prodnction time). I11 addition, the cooling rate is 0.30 "CIS or slowel; is preferably
0.27 "CIS or slower, and is more preferably 0.25 "CIS or slower, fio~nth e viewpoint of
suppressing formnatiotl of sheet-shaped or layered cernetitite.
The cooling temperature is 700°C or lowel; and is preferably 650°C or lower,
from the viewpoint of suppressing fornlation of sheet-shaped or layered cementite. In
addition, the cooling temperature is preferably ro& temperature (25OC) or higher fiotii
the viewpoints of reducing a load on eoolit~gfa cilities, improving production efficiency,
and of reducing the production cost.
[0025]
Through the annealing process, fine spheroidal cementite (refer to FIG. 4(B))
is allowed to eficiently grow in a structure after the warm forging process (step (B) in
FIG. 2). Accordingly, it is possible to fonn a structure (refer to FIG. 4(C)) in which
the spheroidal cementite is dispersed after the atnieali~igp rocess (step (C) in FIG. 2).
In this manner, it is possible to obtain a roughly shaped material for bearing
rings of a rollitig bearing.
Exatnples
[0026]
Next, the effect of a rolling Inember and a method of matiufacturitlg the
rolling member according to the en~bodimenot f the invention will be verified with
OSP-61399 English Specification Draft
reference to exatuples aud the like.
[0027]
(Experiment Example 1)
Steel (Ael=735"C) composed of high-carbon chrome bearing steel A
(composition: 0.98 mass% of carbon, 1.48 mass% of chomiurn, 0.25 mass% of silicon,
0.45 mass% of manganese, 0.012 mass% of phosphorous, 0.006 mass% of sulful; and a
remainder including iron and utlavoidable impurities) was forged and annealed under
conditions shown in Table 1, thereby obtaining test pieces (model number: 6208) of a
roughly shaped material for bearing rings in Experiment Nos. 1 to 17.
[0028]
[Table 11
OSP-61399 Englisli Specification Draft
[0029]
(Test Esamnple 1)
Vickers hardness at 55 sites aruong the test pieces of Experiment Nos. 1 to 17
was tneasured in accordance with JIS Z 2244, and an average value of the Vickers
hardness measured at the 55 sites was obtained. In addition, 5 mass% of picral etchant
was brought into cotitact wit11 the central portion of each of the test pieces of
Experiment Nos. 1 to 17 for 10 seconds to corrode the central portion, and then a
corroded surface was obsenled with a scanning electron niicroscope (product name:
EPMA-1600, manufactured by Shimadzu Corporation). Next, an evaluation of
hardness arid structure spheroidizing, and an overall evaluatioti were performed for the
respective test pieces. The results thereof are shown in Table 2. Fut-therrnore, the
evaluation standards for the hardness and the structure spheroidizing, and for the overall
evaluation of each of the respective test pieces are as follows.
[0030]
(Evaluation Standards for Hardness)
Good: Vickers hardness is Hv240 or less.
Poor: Vickers hardness is greater that1 Hv240.
[003 11
(Evaluation Standards for Structure Spheroidizing)
Good: Sheet-shaped or layered cementite is not sho~vna,n d spheroidal
cemelltite is unifornlly dispersed in a stt-ucture.
Poor: Sheet-shaped or layered cementite is sl~oun.
[0032]
(Evaluation Standards for Overall Evaluation)
Good: Evaluation of the hardness and tlie evaloation of the structure
OSP-61399 English Specification Draft
spheroidizing are good.
Poor: At least one of the evaluation of the hardness and of tic evaluation of the
structure spheroidizing is poor.
[0033]
[Table 21
[0034]
Fro111 results shown in Table 2, in a case where the follo\ving conditions were
satisfied (Experiment Nos. 1 to 3,6, 10, 11, and 13 to IS), that is, in a case where the
forging temperature was in a range of (Ael point+2S°C) to (Ael point+lOS°C), the
cooling temperature after forging was Ael point or lowel; the soaking temperature
during annealing was in a range of (Ael point+2S°C) to (Ae, point+8S°C), the soaking
time \vas 0.5 horns or longer, the cooling rate after soaking was 0.30 'CIS or sl%ver, and
the cooling temperatore \<'as 700°C or lower, it co~~bled s een that all of the test pieces
which were obtained had Vickers hardness of I-Iv240 or less (hardness capable of stably
obtaining satisfactory machinability), and had a structure in which sheet-shaped or
layered cementite was not shown and spheroidal cementite was oniformly dispersed,
and thus hardness and structure spheroidizing were suitable for the roughly shaped
material for bearing rings. In contrast, in a case where the above-described conditions
were not satisfied, that is, in a ease wvhere the soaking temperature was Ae, point+S0C
(Experiment No. 12), Ael point+l05"C (Experiment No. 16), or Ael poitt+l35"C
(Experiment No. 17), the soaking time was 0 hour (Experiment NO.'^), the cooling
temperature after soaking was 730°C (Experiment No. 4) or 780°C (Experiment No. 5),
the cooling rate after soaking was 0.50 "CIS (Experiment No. 7), and the cooling rate
after soaking was 1.50 'CIS (Experiment No. 8), it could be seen that at least one of
hardness and st~~~ctsuphrer oidizing of the test pieces was not suitable for the roughly
OSP-61399 English Specification Drart
shaped material for bearing rings.
[0035]
Even in a case using steel composed of high-carbon cl~ro~ibiea ring steel B
(Ael=735'C) containing 1.0 mass% of carbon, 1.5 mass% of chromium, 0.3 inass% of
silicon, 0.45 mass% of manganese, 0.01 mass% of phosphorous, 0.005 mass% of sulfur,
and a re~nainderin cluding iron and unavoidable impurities, high-carbon clwome bearing
steel C (Ael=735"C) containing 0.8 mass% of carbon, 1.4 mass% of chromium, 0.2
mass% of silicon, 0.4 mass% of manganese, 0.005 mass% of phosphorous, 0.004
mass% of sulful; and a remainder iticluding iron and unavoidable impurities, or highcarbon
chrome baring steel D (Ael=745OC) coritainitlg 0.9 mass% of carbon, 1.7 mass%
of chroniiom, 0.2 mass% of silicon, 0.45 mass% of tnanganese, 0.005 mass% of
phosphorous, 0:005 inass% of sulfur, and a remainder including iron aid unavoidable
impurities instead of steel cotnposed of the high-carbon chrome bearing steel A, it could
be seen that the same tendency as in steel composed of high-carbon chrome bearing
steel A was shown.
[0036]
(Experiment Example 2)
Steel (Ael=73S°C) conlposed of high-carbon chrome bearing steel
(coniposition: 0.98 mass% of carbon, 1.48 mass% of clwomium, 0.25 mass% of silicon,
0.45 mass% of manganese, 0.012 mass% of phosphorous, 0.006 mass% of solfin; and a
remainder including iron and unavoidable impurities) was forged and annealed under
conditions shown in Table 3, thereby obtaining test pieces (model number: 6208) of a
roughly shaped material for bearing rings in Experiment Nos. 18 to 41.
[0037]
[Table 31
OSP-61399 English Specification Draft
LO0381
(Test Example 2)
The Vickers hardness at 55 sites atnotig the test pieces of Experiment Nos. 18
to 19 \?'as tneasured in accordance \\it11 JIS Z 2244, and the average value of the Vickers
hardness nleasured at the 55 sites was obtained. In addition, 5 inass% of picral etcliant
was brought into contact with the central portion of each of the test pieces of
Experinlellt Nos. 18 and 19 for 10 seconds to corrode the ceutral portion, and then a
corroded surface was observed with a scanning electron microscope (product name:
EPMA- 1600, manufactured by Shimadzu Corporation). Furthermore, the test pieces
of Experinlent Nos. 18 and 19 were produced ur~detrh e same conditions except that the
tenlperature rising rates in the annealing process were different fiom each other.
-
[0039]
As a result, it could be seen that all of the test pieces in Experiment Nos. I8
and 19 had a Vickers hardness of I-Iv240 or less (a hardness capable of obtaining
satisfactor~mr achinability), and had a structure it1 which sheet-shaped or layered
cementite was not shown and spheroidal cementite \+.as uniformly dispersed, and thus
hardness and structure spheroidizing were suitable for the roughly shaped material for
bearing rings (not shown). Accordingly, it is implied that an effect of the tenlperature
rising rate in the annealing process on hardness and a structure state of the roughly
shaped material for bearing rings is small.
[0040]
(Test Example 3)
Vickers hardness at 55 sites anlong the test pieces of Experime~lNt os. 20 to 27
was measured in accordance with JIS Z 2244, and an average value of the Vickers
l~ardr~etsnse asured at tl~e5 5 sites was obtained. In addition, 5 mass% of picral etchant
OSP-61399 English Specification Draft
was brought into contact with the central portion of each of the test pieces of
Experiment Nos. 20 to 27 for 10 secollds to corrode the central portion, and then a
corroded surface was observed with a scanning electron nlicroscope (product name:
EPMA-1600, manufactured by Shimadzu Corporatio~i). Furtherniore, the test pieces
of Experi~ncnNt os. 20 and 27 were produced under the same conditions except that
soaking temperatures in the annealing process were different from each other. In Test
Exanlple 3, results obtained by investigating a relationship between the soaking
tenlperah~rea nd the hardness, and results obtained by observing the struch~reo f the
roughly shaped ~llateriafl or bearing rings which was obtained after the annealing
process are sl~ownin FIG. 5. In FIG. 5, (a) is a graph showing the results obtained by
investigating the relationship between the soaking temperature and the hardness, (b) is a
drawing-substituting photograph of the structure of the roughly shaped material for
bearing rings when the soaking temperature is set to 740°C, (c) is a drawing-substih~ting
photograph of the structure of the roughly shaped material for bearing rings hen the
soaking temperature is set to 760°C, (d) is a drawing-substituting photograph of the
structure of the roughly shaped material for bearing rings when the soaking temperature
is set to 820°C, and (e) is a dralving-substituting photograph of the structure of the
rouglily shaped material for bearing rings when the soaking temperature is set to 840°C.
In the drawing, the scale bar represents 5 pm.
[0041]
As shown in FIG. 5, in a case where the soaking temperature is 760°C to 820°C
((Ael point+25OC) to (Ael point+85"C)) (Experiment Nos. 22 to 25), it could be seen
that all of the test pieces which were obtained had a Vickers hardness of Hv240 or less
(a hardness capable of obtaining satisfactory n~achinability)a, nd tended to have a
structure in which sheet-shaped or layered cementite was not shown and spheroidal
OSP-61399 English Specification Draft
cementite \vas unifor~nlyd ispersed, and thos all of the hardness and structure
spheroidizing were suitable for the roughly shaped nlaterial for bearing ritlgs. In
contrast, in a case \vhere the soaking temperature was 740°C (Experimetlt No. 20),
750°C (Experiment No. 21), 840°C (Experiment No. 26), 850°C (Experiment No. 27),
and 870°C (Experitilent No. 28), Vickers hardness of the test pieces was greater than
Hv240 (the hard~~easts w hich machinability deteriorates), or the sheet-shaped or
layered ce~nentitew as shown. Accordinglj: from the res~~ltist ,i s implied that the
soaking temperature is preferably (Ael poi11t+25"C) to (Ael poil~t+XS~C).
[0042]
(Test Example 4)
Vickers hardness at 55 sites among the test pieces of Experiment Nos. 29 to 33
was measured in accordance with JIS Z 2244, and an average value of the Vickers
hardness measured at the 55 sites was obtained. In addition, 5 mass% of picral etchant
was brought into contact with the central portion of each of the test pieces of
Experiment Nos. 29 and 33 for 10 seconds to corrode the central portion, and then a
corroded surface was observed \\it11 a scanning electron microscope (product natne:
EPMA-1600, manufactured by Shimadzu Corporation). Furthermore, the test pieces
of Experiment Nos. 29 to 33 were produced under the same conditions except that the
soaking time in the annealing process is different fro111 each other.
[0043]
As a result, in a case where the soaking time was 0.5 hours (Experiment No.
30), 1 hour (Experiment No. 31), 1.5 hours (Experiment No. 32), and 2 hours
(Experinlent No. 33), it could be seen that all of the test pieces which were obtained had
a Vickers hardness of Wv240 or less (a hardness capable of obtaining satisfactory
machinability), and had a struchlre in which sheet-shaped or layered cementite was not
OSP-61399 English Specification Draft
shown and spheroidal cementite was uniforn~lyd ispersed, and thus hardness and
structure spl~eroidizing\I rere suitable for the ro~~ghslhya ped material for bearing rings
(not showvn). In contrast, in a case where the soaking time was 0 hour (Experiment No.
29), Vickers hardness of the test piece was greater than Hv240 (hardness at which
tnachinability deteriorates) (not showvn). Accordingly, from the results, it is implied
that the soaking time is preferably 0.5 hours or longer.
[0044]
(Test Example 5)
Vickers hardness at 55 sites atnong the test pieces of Experinlent Nos. 34 to 37
was rneasured in accordance wvith JIS Z 2244, and the average value of the Vickers
hardness measured at the 55 sites was obtained. In addition, 5 mass% of picral etchant
was brought into contact with the central portion of each of the test pieces of
Experiment Nos. 34 to 37 for 10 seconds to corrode the central portiot~a, nd then a
corroded surface was observed with a scanning electron microscope (product name:
EPMA-1600, manufactured by Shiniadzu Corporation). Furthermore, the tcst pieces
of Experiment Nos. 34 and 37 were produced under the same conditions except that the
cooling rates in the annealing process were different from each other. In Test Exa~nple
5, results obtained by investigating a relationship between the cooling rate and the
hardness, and results obtained by observing the structure of the roughly shaped material
for bearing rings which was obtained after the annealing process are shown in FIG. 6.
In the dra\ving, (a) is a graph showving the results obtained by investigating the
relationship betwveen the cooling rate and the hardness, (b) is a drawing-substituting
photograph of the structure of the roughly shaped material for bearing rings when the
cooling rate is set to 7 "Cln~in(0 .12 'CIS), (c) is a drawing-substituting photograph of
the structure of the roughly shaped material for bearing rings when the cooling rate is
OSP-61399 Englisll Specification Draft
set to 16 "Clmin (0.27 "CIS), (d) is a drawing-substitt~tingp hotograph of the structure of
the roughly shaped material for bearing rings when the cooling rate is set to 26 "Clnlin
(0.43 "CIS), and (e) is a dra\+ing-substituting pl~otograph of the structure of the roughly
shaped material for bearing rings \vllen the cooling rate is set to 93 'Cl~nin (1.55 "CIS).
In the drawing, the scale bar represents 5 pn1.
[0045]
From the results shown in FIG. 6, in a case where the cooling rate was 0.12
'CIS (Experiment No. 34) and 0.27 "CIS (Experiment No. 35), it could be seen that all of
the test pieces which were obtained had Vickers hardness of Hv240 or less (hardness
capable of stably obtaining satisfactory ~nachinability)a, nd had a structure in which
sheet-shaped or layered cementite was not shown and spheroidal cementite was
uniformly dispersed, and thus hardness and structure spheroidizing were suitable for the
roughly shaped material for bearing rings. In contrast, in a case where the cooling rate
was 1.55 "C/s (Experiment No. 37), it could be seen that the Vickers hardness of the test
piece wvas greater than Hv240 (the hardness at which nlachinability deteriorates), and
the sheet-shaped or layered cementite was seen. Accordingly, the results implies that
' the cooling sate in the annealing process is preferably 0.30 "C/s or lowel; and is more
preferably 0.27 "CIS or lower.
[0046]
(Test Example 6)
Vickers hardness at 55 sites among the test pieces of Experiment Nos. 38 to 43
was ~neasured in accordance with JIS Z 2244, and an average value of the Vickers
hardness nleasored at the 55 sites wvas obtained. In addition, 5 mass% of picral etchant
was brought into contact with the central portion of each of the test pieces of
Experiment Nos. 38 to 43 for 10 seconds to corrode the central portion, and then a
OSP-61399 English Specification Draft
corroded surface was obset~fedw ith a scart~titige lectron ~tticroscope( product name:
EPMA-1600, manufactured by Sliintadzn Corporation). Furthennore, the test pieces
of Experinlent Nos. 38 and 43 were produced under the same conditions except that the
cooling tentperaturc in the annealing process was different from each other. In Test
Exantple 6, results obtained by investigating a relationship between the cooling
temperature and the hardness, and results obtained by observing tlie structure of the
roughly shaped material for bearing rings which is obtained after the annealing process
are showvn in FIG. 7. In the drawing, (a) is a graph showing the results obtained by
investigating the relationship between the cooling temperature and the hardness, (b) is a
drawing-substituting pltotograplt of the structure of the roughly shaped material for
bearing rings when the cooling temperature is set to 650°C, (c) is a drawing-substituting
photograph of the structure of the roughly shaped material for bearing rings when the
cooling temperature is set to 700°C, and (d) is a drawing-substituting photograph of the
structure of the roughly shaped material for bearing rings when the cooling temperature
is set to 730°C. In the drawing, a scale bar represents 5 pm.
[0047]
From the results shown in FIG. 7, in a case where the cooling temperature \%as
600°C (Experiment No. 38), 650°C (Experitnent No. 39), and 700°C (Experiment No.
40), it could be seen that all of the test pieces which were obtained had Vickers hardness
of Hv240 or less (Itardness capable of obtaining satisfactory machinability), and tended
to have a s t ~ ~ ~ c tinu rweh ich sheet-shaped or layered cementite was not showv~ai nd
spheroidal cementite was uniformly dispersed, and thus tlie hardness and the structure
spheroidizing were suitable for the roughly shaped material for bearing rings. In
contrast, in a case where the cooling temperature was 750°C (Experiment No. 42) and
780°C (Experiment No.'43), it could be seen that there is a tendency where the Vickers
OSP-61399 English Specification Draft
hardness of the test pieces was greater than Hv240 (hardness at which machinability
deteriorates), and tlie slie'et-shaped or layered cementite was shoowii. Accordingly,
fio111 the results, it is i~iipliedth at the cooling temnperature in the atuiealing process is
preferably 700°C or lower.
[0048]
(Exaniple I and Example 2)
Steel (Ael=735"C) composed of high-carbon chronie bearing steel
(composition: 0.98 mass% of carbon, 1.48 inass% of clwomiuti~0, .25 inass% of silicon,
0.45 mass% of manganese, 0.012 mass% of phosphorous, 0.006 mass% of sulfiil; and a
remainder including iron and unavoidable impurities) was forged and annealed under
conditions show~iin Table 4. Then, the forged articles which were obtained were
subjected to a quenching treatment and a tempering treattilent urider conditions shown
in FIG. 8 (Example 1) and under co~iditions hown in FIG. 9 (Exaniple 2), thereby
obtaining test pieces (model tmmber: 6208) of a roughly shaped material for bearing
rings.
[0049]
[Table 41
[0050]
(Test Example 7)
5 mass% of picral etchant \wras brought into contact with the central portion of
each of forged a~ticleasf ter the annealing process in Exa~ilple1 and Example 2 for 10
seco~~tdos c or~odetl ie central portion, and then a corroded surface wwras observed with a
scamiing electron niicroscope (product name: EPMA-1600, nianufactured by Shimadzu
Corporation). In addition, the \Tickers hardness at 55 sites among tlie test pieces of
Exaniple 1 and Example 2 was measured in accordance with JIS Z 2244, and the
OSP-61399 Et~glislS~p ecification Draft
average value of the Vickers hardaess measured at the 55 sites was obtained. Ncxt,
evaluation of hardtless of the respective test pieces and stl.acture spheroidizing of the
forged articles after the annealing process was perforn~ed. In addition, the X-ray
diffraction intensity was measured at a surface layer portion and the center portion of
the test pieces of the roughly shapcd material for bearing rings ill Example 1 and
Example 2 by at1 X-ray diffraction method. The X-ray diffractiotl intensity Iy of fcc
that is a crystal structure of residual austenite, and the X-ray diffractio~in~t ensity Iu of
bcc that is a crystal st~ucttureo f a te~nperedm artensite were obtained. From the X-ray
difFractiot1 intensity ratio which was obtained, the amount of residual austenite at the
surface layer portion and the center portioll of the test pieces of the rooghlp shaped
material for bearing rings in Example 1 and 2 was obtained by using the followi~~g
theoretical Expression (I):
1 Ny-1 +(RylRa)x(IulIy) (1)
( h E~x pression, Vy represents the amount of residual austenite, Ry and Ru
represent coefticients depending on crystal orientatiotls that is measured, Iy and la
represent X-ray diffraction intensities).
In test Example 7, results, wvllich are obtained by obsel-ving a structure of the
forged article obtained after the annealing process, are sho\vn in FIG. 10. In the
drawing, (a) is a drawing-substituting pllotograph showing a result obtained by
obsei~ringth e structure of the forged article in Example 1, and (b) is a drawingsubstituting
photograp11 showiilg a result obtained by obsewing the structure of the
forged article in Example 2. Furthennore, a scale bar in the drawing represents 10 pm.
The amount of residual austei~itca t the surface layer portion and the center portion of
the test pieces of the roi~ghlys haped material for beariug rings in Exatnple 1 and
Example 2, and results obtained by perforlning evaluatio~ol f the hardness of the
OSP-61399 Englisli Specification Draft
respective tcst pieces and tlie structure splieroidizing of the forged articles afler the
annealing process are sliowvn in Table 5. In addition, tlie evaluation standards for the
evaluation of tlie hardness of the respective test pieces, and tlie structure spheroidizing
of the forged articles obtailicd after the annealing process are the same as the evaluation
standards used it1 Test Example 1. I11 addition, a case wvliere the amount of residual
austenite \\.as an amount (15 vol% or less), which is suitable for compatibility between
securement of rolling fatigue life and securement of dimensional stability in bearing
rings of a rolling bearing is regarded as "Good".
[0051]
[Table 51
[0052]
From results sliown in FIG. I0 and Table 5, in Example 1 and Example 2 which
satisfies conditions in which the forging temperature is in a range of (Ael poi11t+25~C)
to (Ael point+105"C), the coolit~gte mperature after forging was Ael point or lower, the
soaking temperature during annealing was in a range of (Ael point+25OC) to (Ael
point+85'C) and the soaking tenlperahre during annealing was in a range of preferably
(Ael point+35C) to (Ael point+75"C), the soakirig time was 0.5 hours or longel; the
cooling rate after soaking wvas 0.30 'CIS or slower, and the cooling temperature was
700°C or lower, it can be seen that all of the amount of residual austenite, tlie liardness,
and the structure spheroidizing are in ranges wvhich are suitable for manufacturing of
bearing rings.
[Brief Description of the Reference Symbols]
[0053]
1: CONICAL ROLLER BEARING (ROLLING BEARING)
11 : INNER RING (BEARING RING)
OSP-61399 English Specification Draft
12: OUTER RING (BEARING RING)
EXPERIMENT
No.
1
2
3
4
5
Ael
("C)
735
6
7
8
9
10
735
735
735
735
735
735
735
735
---7 35
WARM FORGING PROCESS
----- 830(Ae1+95)
830(Ae,+95)
830(Ae,+95)
830(Ae,+95)
FORGING
TEMPERATURE
("C)
830(Ae1 +95)
ANNEAL1 NG PROCESS
830(Ae,+95)
830(Ae7+95)
830(Ae,+95)
830(Ae,+95)
830(Ae1+95)
COOLING
TEMPERATURE
("C)
AIR COOLING
TEMPERATURE
RISING RATE
("C/s)
0.08
AIR COOLING
AIR COOLING
AIR COOLING
AIR COOLING
0.1 0
0.10
0.1 0
0.1 0
0.10
0.1 0
0.10
1.5
1 .O
1 .O
1 .O
1 .O
11 735 830(Ae1+95) AIR COOLING 0.40
AIR COOLING
AIR COOLING
AIR COOLING
AIR COOLING
AIR COOLING
700
700
700
700
700
pp
700
700
12
- 13
14
15
SOAKING
TEMPERATURE
("C)
I 780(Ae1+45)
0.40
0.40
0.40
0.40
16
0.40
0.40
0.40
0.40
0.40
735
735
735
735
SOAKING
TIME
(h)
1 .O
780(Ae1 +45)
780(Ae1 +45)
780(Ae, 4-45)
735
780(Ae1 +45)
780(Ae, 4-45)
780(Ae1 4-45)
780(Ae, 4-45)
780(Ae1 +45)
17 735
830(Ae1 +95)
830(Ae1+95)
830(Ae,+95)
---- 830(Ae1+95)
COOLING
RATE
("C/s)
0.1 0
1 .O
1 .O
1 .O
1 .O
830(Ae,+95)
COOLING
TEMPERATURE
("C)
600
1 .O
1 .O
1 .O
0.0
0.5
830(Ae1+95)
AIR COOLING
AIR COOLING
AIR COOLING
AIR COOLING
0.1 0
ppp
0.10
0.1 0
0.1 0
AIR COOLING
600
700
730
780
0.25
0.50
1.50
0.1 0
0.1 0 ppp
AIR COOLING
0.40
0.40
0.40
0.40
600
600
600
700
700
740(Ae1+5)
760(Ae, 4-25]
800(Ae1 +65)
820(Ae, +85)
0.40 1 .O
0.40 870(Ae1+1 35) 1 .O
[table 2 1
I EVALUATION
EXPER l hlENT
No.
1
2
3
4
5
6
7
8
HARDNESS
(Hv240 or less)
-
9
10
11
12
13
14
15
16
17
GOOD
GOOD
GOOD
GOOD
POOR
GOOD
POOR
POOR
STRUCTURE
SPHEROlDlZlNG
POOR
GOOD
GOOD
POOR
GOOD
GOOD
GOOD
GOOD
POOR
OVERALL
GOOD
GOOD
GOOD
POOR
POOR
GOOD
POOR
POOR
GOOD
GOOD
GOOD
POOR
POOR
GOOD
POOR
POOR
GOOD
GOOD
GOOD
GOOD
GOOD
GOOD
GOOD
POOR
POOR
-
POOR
GOOD
GOOD
POOR
GOOD
GOOD
GOOD
POOR
POOR
[table 3 1
OSP-61399 English Specification Draft
[Document T>lpe] CLAIMS
What is claimed is:
1. A method of producing a roughly shaped material for a rolling bearing by
forging a steel composed of a high-carbon chrome bearing steel containing 0.7 mass%
to 1.2 mass% of a carbon, and 0.8 mass% to 1.8 mass% of a chroniium, the method
comprising:
(A) forging the steel to a predetermined shape while heating the steel to a
forging temperature in a range of (Ael point+25OC) to (Ael point+l05"C), and cooling a
forged article to a temperature of Ael point or lower; and
(B) performing an annealing in which the forged article obtained in (A) is
heated to a soaking temperature in a range of (Ael point+25"C) to (Ae, point+85"C), the
forged article is retained for 0.5 hours or longer, and the forged article is cooled down to
700°C or lo\ver at a cooling rate of 0.30 "CIS or slower.
2. The method of producing a roughly shaped material for a rolling bearing according
to Claim 1,
\\~liereitit he soaking temperature is set to 760°C to 820°C.
3. The method.oPproducing a roughly shaped material for a rolling bearing according
to Claim 1 or 2,
\vlierein the cooling rate is set to 0.27 "CIS or slo\vel: