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Method Of Manufacturing A Ceramic Core For A Blade Ceramic Core And Blade

Abstract: The method of manufacturing a ceramic core for a blade comprising a lower part forming a core body an upper part forming a squealer tip recess and a set of rods for holding the upper part and the lower part together comprises: · a step of coating the rods with a material that has a flash point below 1000°C; · a step of positioning the rods in a mould; · a step of moulding the upper and lower parts by injecting ceramic; · a step of firing the ceramic core.

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Patent Information

Application #
Filing Date
30 June 2014
Publication Number
13/2015
Publication Type
INA
Invention Field
METALLURGY
Status
Email
remfry-sagar@remfry.com
Parent Application
Patent Number
Legal Status
Grant Date
2020-07-17
Renewal Date

Applicants

SNECMA
2 Boulevard du Général Martial Valin F 75015 Paris

Inventors

1. TRUELLE Franck Edmond Maurice
Snecma PI (AJI) Rond Point René Ravaud Réau F 77550 Moissy cramayel Cedex
2. GRANDIN Alain
Snecma PI (AJI) Rond Point René Ravaud Réau F 77550 Moissy cramayel Cedex
3. MOUGAMADOU ABOUDALCADAR Maidin
Snecma PI (AJI) Rond Point René Ravaud Réau F 77550 Moissy cramayel Cedex

Specification

METHOD OF MANUFACTURING A CERAMIC CORE
FOR MOBILE BLADE, CERAMIC CORE AND MOBILE BLADE
5 FIELD
The field of the invention relates to methods of manufacturing
ceramic cores used in lost wax moulding for manufacturing complex hollow
blading for circulation of mobile blades. The invention is particularly
applicable to the aeronautical field in which such blades can be used in
lo aircraft engines.
STATE OF THE ART
The ceramic core is a discardable part that is used particularly to
obtain the metal blading cooling circuit.
15
Firstly, cores are fabricated by injection of a polymer-ceramic mix
into an injection tool. Secondly, the cores are subsequently fired to eliminate
the polymer and to sinter the ceramic. Thirdly, the cores are deburred and
impregnated with resin which gives them mechanical strength.
20
Figure 1 shows a ceramic core body 10 comprising an upper part
2 forming a squealer tip recess and a lower part 1 forming a core body. The
ceramic core is used for the blades, particularly turbine blades for an aircraft
engine. In general, this type of blade is coupled to circular blading
25 surrounding the blades. The part forming a recess forms an open cavity at
the end of the blade. Functionally, the recess reduces centrifugal forces at
the root of the blade and reduces heat transfer at the tip of the blade. It is
fixed to the core body by the use of rods 3 that connect the core body to the
recess. The rods may also be made of ceramic. In general, any material with
30 a coefficient higher than the coefficient of expansion of the cores is suitable
for making the rods.
One problem that arises with the manufacture of such cores is
encountered during the firing step of said cores. The firing step follows the
35 ceramic moulding step in a mould in which the rods are pre-positioned before
injection of the material.
Once the rods 3 have been moulded connecting the core body to
the recess, they are fixed to the moulded ceramic that has taken the shape of
a recess and a core body. As the temperature rises during firing, the rods
expand. Figure 2 shows the result of expansion of a rod in the ceramic after
s firing, particularly due to the generation of a crack 20 forming open cracking
20 of the recess 2.
One solution consists of applying a local overthickness on the core
facing the alumina rod.
10 Figure 3 shows an overthickness 30 introduced so as to
consolidate the part forming a crack after the ceramic has been fired along
the recess at the level of the rods located inside the ceramic. The extra
thickness is subsequently removed. Before the local overthickness has been
cut flush, there were no visible cracks along the rod.
15 One disadvantage of this solution is that this overthickness has to
be removed after firing, for example by manual grinding. It is found that the
crack can once again appear on the recess during this operation. It then
forms an open crack on the surface of the recess.
One major disadvantage is that the core is then unusable and
20 potentially has to be scrapped.
SUMMARY OF THE INVENTION
The invention solves the above-mentioned disadvantages.
The purpose of the invention applies to a method of manufacturing
25 a ceramic core for a blade comprising a lower part forming a core body, an
upper part forming a squealer tip recess and a set of rods contributing to
holding the upper part with the lower part. The method according to the
invention comprises:
a coating step, in which the rods are coated with a material with
30 a flash point below a temperature threshold above which the
expansion of the rod is greater than a predefined proportion;
a step in which the rods are positioned in a mould;
r a step in which the upper and lower parts are moulded by a
ceramic injection, the moulded parts thus forming a single part
in the mould and defining a core shape;
a step to fire the ceramic core.
According to one embodiment, the temperature threshold is
1000°C.
5 According to one embodiment, the expansion of the rod as a
percent is 1 %.
The ceramic core manufacturing method prevents cracking of the
ceramic caused by the presence of rods during firing.
10 The method according to the invention particularly includes a
preliminary step such as varnishing to coat at least one rod. Varnishing the
rod can prevent cracking of the recess.
Each rod may be made of alumina or it may be made from a
ceramic material with a coefficient higher than the coefficient of expansion of
15 the cores.
Cracking is avoided by inflammation of the varnish during firing
which releases a space between the fired ceramic and the expanded rod.
The inflammation temperature of the varnish or an equivalent material
covering the rods releases a space around the rod that expands at a
20 temperature higher than the inflammation temperature of the varnish.
Advantageously, the steps are carried out in sequence.
Advantageously, a mould removal step (DEM) of the core
precedes the core firing step (CUI).
Advantageously, each rod is coated on the surface thal might be
2s surrounded by the recess.
Advantageously, coating of part of the rods consists of a coat of
varnish.
Advantageously, the coating of the rods consists of either:
- a deposit of a coat of wax on a part of the surface of each rod;
- a deposit of a coat of resin on a part of the surface of each rod;
- a deposit of a coat of graphite on a part of the surface of each
rod.
The purpose of the invention also relates to a ceramic core for a
35 turbine blade comprising a lower part forming a core body, an upper part
forming a recess and a set of rods that contribute to holding the upper and
lower parts together, characterised in that the core is made using a method
according to the invention.
The invention also relates to a blade for a turbine made using a
s foundry method that used a core made by the method according to the
invention.
BRIEF DESCRIPTION OF TI-IE FIGURES
Other characteristics and advantages of the invention will become
10 clear after reading the following detailed description with reference to the
appended figures that show:
figure 1: a view of a ceramic core for mobile blades;
figure 2: a view of a ceramic core after firing and formation of a
crack. on the recess in the core;
1s figure 3: a view of a ceramic core comprising an overthickness to
compensate for the formation of a crack;
figure 4: a diagram showing the main steps in the method
according to the invention.
20 DESCRIPTION
In this description, the "flash point" or "inflammability point" refers
to the lowest temperature at which a body or a combustible material emits
sufficient vapour to form a gaseous mix with ambient air that inflames under
the effect of a heat energy source.
25
Throughout the remainder of the description, the term "coating"
step will be used to refer to the coating applied according to this patent
application.
A ceramic core for a turbine blade comprises a lower part forming
30 a core body, an upper part forming a recess and a set of rods contributing to
holding the upper and lower parts to each other. The upper and lower parts
are fixed to each other. In one simplified embodiment of the invention, at
least one rod contributes to holding the two parts of the core in place.
Depending on the embodiment, the upper and lower parts may
35 comprise a common zone that also contributes to holding the two parts
together. Figure 1 shows such an embodiment in which the parts 1 ,and 2 are
also held together by a common zone 4 located on the side of the core.
The method of manufacturing a ceramic core according to the
5 invention comprises a coating step denoted END in figure 4, of the rods
before they are inserted into a mould for moulding the ceramic parts. The
varnish is deposited on the part of the rod that will be surrounded by the
recess in the core. In one embodiment, the part of the rod that is surrounded
by the core body is not covered with varnish.
10 In one particular embodiment of the invention, the rods may be
coated after they have been positioned in the mould. But preferably the rods
are coated before they are inserted in the mould so that the entire surface of
the rod is covered uniformly.
Rods may be coated in different ways, depending on the type of
is material applied, the thickness of the required coat andlor the part of the rod
or rods to be covered.
In one embodiment of the invention, the entire rod is coated with a
material with a flash point of less than 1000°C.
In another embodiment, only the part of each rod surrounded by
20 the recess is covered with a rendering. The part of the rod surrounded by the
core body is not coated with varnish. One advantage is that the quantity of
varnish is adapted to the part of the structure weakened by expansion of the
rod.
The temperature limit of 1000°C corresponds to the temperature at
25 which transformation of ceramic materials forming the core begins. This limit
is thus a particularly interesting temperature so that the material applied on
the rod will inflame before the firing temperature reaches this limit. It is also
possible to choose lower limits that will function at least as well as long as the
temperature of the flash point of the material is below this limit.
30 In general, a temperature threshold is chosen such that the
coating material such as a varnish inflames before the rod expands.
Expansion is assumed to be effectively zero below a certain limit. In one
embodiment, this limit is fixed at 1% which corresponds to 1% expansion of
the rod dimensions. According to other embodiments, the predefined
35 proportion defining the so-called "consequent" expansion limit may be more
than 1% and up to 2% or even more depending on the materials used and
their dimensions.
In different embodiments, the material may be applied either by
5 dipping the rods or by application of the material on the rods, for example
with a brush.
In one preferred embodiment, the applied material is a varnish.
This varnish may for example be a "nail varnish" type. The varnish
10 application method may then be applied on the rod using a brush in a
conventional manner like a woman would apply varnish to her finger
nail.
An appropriate varnish includes solvents, resin, nitrocellulose and
plastifiers. For example, a varnish like a "Thixotropic base" varnish marketed
15 under the trade name "Peggy Sage nail varnish all formulas" may be used in
the method according to this invention.
Once the varnish has been applied on the rod, the rod is placed in
a mould. Preferably, the rod is positioned according to a step of the method
denoted POS, after the varnish has dried. The position of each rod in the
20 mould is such that when the material is injected, it will surround each rod.
The method includes a moulding step denoted MOU in figure 4,
comprising an injection of ceramic in the mould. Injection of the ceramic
forms the core in the housing provided for it, thus forming the body and the
recess depending on the shape of the mould.
25 The ceramic moulding step comprises moulding of the lower part
forming the core body and moulding of an upper part forming a recess. The
two parts are preferably moulded at the same time. The rods are positioned
such that part of the rod is in the upper part of the core and part of the rod is
in the lower part of the core. The ceramic material injected into the part of the
30 mould forming the recess surrounds the part of the rod present in the recess
and the ceramic material injected into the part of the mould forming the core
body surrounds the part of the rod positioned in this part of the mould.
After moulding, the rod holds the two parts of the core together.
In another step in the manufacturing method according to the
35 invention, the core is then removed from the mould, this step is denoted DEM
in figure 4. The rod or rods fixed to the two parts of the core is (are) thus also
taken out of the mould.
A firing step of the core thus removed from the mould, denoted
CUI in figure 4, can then be initiated.
s While the core is being fired, the varnish covering the rods
reaches its flash point before expansion of the rod reaches consequent
proportions. Thus, the coefficient of expansion of alumina at 1200°C is
1.03%. Consequently, burning or inflammation of the varnish occurring at the
flash point of the varnish takes place at a temperature lower than the firing
lo temperature that causes expansion of the alumina rod.
Inflammation of the varnish releases a space all around the rod
before it expands. The rod moulded in the lower and upper part of the core
then expands under the effect of firing with increasing temperature. One
advantage of the varnish coat applied on the rod and that burned is that it
is leaves a space around the rod, said space providing the additional space
required by its expansion. Therefore the quantity of varnish applied on each
rod can be chosen so as to adapt the space created around the rod to match
the additional volume occupied by expansion of the rod.
Depending on the embodiment, tests can be used to choose the
20 type of material used to cover the rods and to choose the appropriate
thickness of said coats when they are applied on the rods. These tests can
determine the ideal space released by the material that burned to correspond
to the space required for expansion of the rod during firing.
Consequently, during and after firing, expansion of the rod no
2s longer Imposes a mechanical stress on the ceramic material surrounding it
that could cause a crack.
In previous solutions, it was found that cracking often occurred in
the recess. Since the recess is thinner than the core body, cracks caused by
resistance to internal expansion of the rods occurred principally in the recess.
30
The crack that might form shown particularly in figure 2, no longer
appears when the rod is impregnated with a material such as varnish. Due to
this preliminary step in which the rods are coated by an inflammable material,
there is no longer any need to apply an overthickness on the surface of core
35 recess.
The steps in the method according to the invention are preferably
executed in sequence. But in one embodiment, it could be envisaged that the
coating step of each rod is performed after the rods have been put into the
s mould. On the other hand, it appears inevitable that moulding and firing
should be done sequentially if the invention is to function satisfactorily.
Other products with approximately equivalent properties as the
varnish may be used for replacement during the coating step according to the
invention.
10 All products that can be used in this invention enable a deposition
of a thin coat, for example a few hundredths of a millimetre. The products
applied to the rods must be eliminated by firing before expansion of the
alumina rod. In preferred embodiments of the invention, it is also important
that these products used as coatings for the rods should not leave any
is undesirable chemical residues.
Each of the products listed below has its own advantages, so that
it may be preferred to others depending on required operational choices.
Apart from varnish, products that might be envisaged to bond to
the rod by making a thin coat and to burn before 1000°C without leaving any
20 residues include wax, resin, paint and/or graphite.
These products have the following advantages:
- they bond to the rod when they are applied to its surface;
- it is easy to apply a deposit in a thin coat;
- a uniform deposit can be made over the entire surFace of the
rod;
- finally, they are all eliminated by firing at a temperature below
1000°C.
Resin is preferably chosen so that it does not contain any material
30 that could pollute the furnaces when firing the cores.
For graphite, combustion may advantageously be controlled so as
to avoid or limit emissions of carbon monoxide. Finally, combustion may be
controlled so as to provide a sufficiently oxidising atmosphere during firing.
One advantage of wax is its plasticity and malleability at ambient
35 temperature that makes it particularly useful for coating a rod. Its melting
point of 45°C releases a space around the rod before expansion of the rod.
Another advantage lies in its low viscosity when it is molten so that it releases
a uniform space around the rod.
The method according to the invention may include ceramic
s sintering and resin coverage steps after the core has been fired.
The invention also relates to a ceramic core obtained by the
method according to the invention. The ceramic core according to the
invention has the special feature that it can be made by the use of rods
10 coated with a material with a flash point lower than the expansion
temperature of alumina.
The invention also relates to a mobile turbine blade comprising a
ceramic core obtained by the method according to the invention.
CLAIMS
5 1. Method of manufacturing a ceramic core (10) for a blade comprising a
lower part (I) forming a core body, an upper part (2) forming a recess
and a set of rods (3) contributing to holding the upper part with the
lower part, characterised in that it comprises:
* a coating step (END) in which the rods are coated with a
10 material with a flash point below a temperature threshold above
which the expansion of the rod is greater than a predefined
proportion;
r a step in which the rods are positioned (POS) in a mould;
* a step in which the upper and lower parts are moulded (MOU)
by a ceramic injection, the moulded parts thus forming a single
part in the mould and defining a core shape;
a step to fire (CUI) the ceramic core.
2. Method of manufacturing a ceramic core according to claim 1,
20 characterised in that the steps are made in sequence.
3. Method of manufacturing a ceramic core according to either of claims
1 to 2, characterised in that the temperature threshold is 1000°C.
25 4. Method of manufacturing a ceramic core according to any one of
claims 1 to 3, characterised in that the predefined expansion as a
percent is 1 %.
5. Method of manufacturing a ceramic core according to any one of
30 claims 1 to 4, characterised in that a mould removal (DEM) of the core
precedes the firing step (CUI) of this core.
6. Method of manufacturing a ceramic core according to any one of
claims 1 to 5, characterised in that each rod is coated on the surface
35 that might be surrounded by the recess.
7. Method of manufacturing a ceramic core according to any one of
claims 1 to 6, characterised in that the coating on part of the rods is
varnishing with a varnish coat.
5 8. Method of manufacturing a ceramic core according to any one of
claims 1 to 7, characterised in that coating of rods comprises
deposition of a coat of wax on a part of the surface of each rod.
9. Method of manufacturing a ceramic core according to any one of
10 claims 1 to 7, characterised in that coating of rods comprises
deposition of a coat of resin on a part of the surface of each rod.
10.Method of manufacturing a ceramic core according to any one of
claims 1 to 7, characterised in that coating of rods comprises
IS depositior~o f a graphite coat on a part of the surface of each rod.
11.Ceramic core (10) for a turbine blade comprising a lower part (1)
forming a core body, an upper part (2) forming a recess and a set of
rods (3) contributing to holding the upper and lower part to each other,
20 characterised in that the core (10) is manufactured using a method
according to any one of the previous claims .
12. Blade for a turbine, characterised in that it was made using a foundry
method that used a core according to claim 11.

Documents

Application Documents

# Name Date
1 OTHER DOCUMENT.pdf 2014-07-03
2 FORM 5.pdf 2014-07-03
3 FORM 3.pdf 2014-07-03
4 FORM 2 + SPECIFICATION.pdf 2014-07-03
5 DRAWINGS.pdf 2014-07-03
6 Copy of General Power of Authority-SNECMA.pdf 2014-07-03
7 5365-delnp-2014-Correspondence-Others-(04-07-2014).pdf 2014-07-04
8 5365-DELNP-2014.pdf 2014-07-11
9 5365-delnp-2014-Others-(04-12-2014).pdf 2014-12-04
10 5365-delnp-2014-Correspondence Others-(04-12-2014).pdf 2014-12-04
11 5365-DELNP-2014-FER.pdf 2019-05-01
12 5365-DELNP-2014-Proof of Right (MANDATORY) [01-11-2019(online)].pdf 2019-11-01
13 5365-DELNP-2014-PETITION UNDER RULE 137 [01-11-2019(online)].pdf 2019-11-01
14 5365-DELNP-2014-PETITION UNDER RULE 137 [01-11-2019(online)]-1.pdf 2019-11-01
15 5365-DELNP-2014-OTHERS [01-11-2019(online)].pdf 2019-11-01
16 5365-DELNP-2014-FORM 3 [01-11-2019(online)].pdf 2019-11-01
17 5365-DELNP-2014-FER_SER_REPLY [01-11-2019(online)].pdf 2019-11-01
18 5365-DELNP-2014-DRAWING [01-11-2019(online)].pdf 2019-11-01
19 5365-DELNP-2014-COMPLETE SPECIFICATION [01-11-2019(online)].pdf 2019-11-01
20 5365-DELNP-2014-CLAIMS [01-11-2019(online)].pdf 2019-11-01
21 5365-DELNP-2014-ABSTRACT [01-11-2019(online)].pdf 2019-11-01
22 5365-DELNP-2014-OTHERS-041119.pdf 2019-11-06
23 5365-DELNP-2014-Correspondence-041119.pdf 2019-11-06
24 5365-DELNP-2014-PETITION UNDER RULE 137 [13-07-2020(online)].pdf 2020-07-13
25 5365-DELNP-2014-PETITION UNDER RULE 137 [13-07-2020(online)]-1.pdf 2020-07-13
26 5365-DELNP-2014-FORM-26 [13-07-2020(online)].pdf 2020-07-13
27 5365-DELNP-2014-Written submissions and relevant documents [15-07-2020(online)].pdf 2020-07-15
28 5365-DELNP-2014-PatentCertificate17-07-2020.pdf 2020-07-17
29 5365-DELNP-2014-IntimationOfGrant17-07-2020.pdf 2020-07-17
30 5365-DELNP-2014-US(14)-HearingNotice-(HearingDate-15-07-2020).pdf 2021-10-17

Search Strategy

1 5365delnp2014_SS_29-04-2019.pdf

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