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Organic Fertilizer And Process For Preparation Of The Same

Abstract: The present invention relates to novel organic fertilizer and process for preparation of the same. More particularly, the present invention relates novel fertilizer act as Organic Soil enhancer and plant nutrition and process for production of the same. The present invention also provides process for production of novel organic fertilizer comprising steps of mechanical mixing of a portion of different Organic compounds, Micro Nutrients, Macro Nutrients, Organic Carbon, Micro-flora and Bio-char in specific % to get desired organic fertilizer to fulfill the current need of the soil for better fertility.

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Patent Information

Application #
Filing Date
28 March 2012
Publication Number
47/2013
Publication Type
INA
Invention Field
CHEMICAL
Status
Email
Parent Application

Applicants

ABELLON CLEANENERGY LTD
ABELLON CLEAN-ENERGY LIMITED., 10TH FLOOR,SANGEETA COMPLEX, NR. PARIMAL RAILWAY CROSSING, ELLISBRIDGE, AHMEDABAD-380006, GUJARAT, INDIA

Inventors

1. PATEL PANKAJ
ABELLON CLEAN-ENERGY LIMITED., 10TH FLOOR,SANGEETA COMPLEX, NR. PARIMAL RAILWAY CROSSING, ELLISBRIDGE, AHMEDABAD-380006, GUJARAT, INDIA
2. PATEL BEENA
ABELLON CLEAN-ENERGY LIMITED., 10TH FLOOR,SANGEETA COMPLEX, NR. PARIMAL RAILWAY CROSSING, ELLISBRIDGE, AHMEDABAD-380006, GUJARAT, INDIA
3. DUBEY ANIL
ABELLON CLEAN-ENERGY LIMITED., 10TH FLOOR,SANGEETA COMPLEX, NR. PARIMAL RAILWAY CROSSING, ELLISBRIDGE, AHMEDABAD-380006, GUJARAT, INDIA

Specification

FORM-2
THE PATENTS ACT,1970 (39 OF 1970)
COMPLETE SPECIFICATION
(SEC-10, RULE 13)
TITLE OF THE INVENTION;
" ORGANIC FERTILIZER AND PROCESS FOR PREPARATION OF THE SAME"
APPLICANT:
Name: Abellon CleanEnergy Limited
Nationality: Indian
Address: 10th Floor, Sangeeta Complex, Nr. Parimal Railway Crossing, Ellisbridge, Ahmedabad - 380004, Gujarat, INDIA
The following Specification describes the invention

The following specification particularly describes the invention: The Field of Invention
The present invention relates to novel organic fertilizer and process for preparation of the same. More particularly, the present invention relates to novel organic fertilizer act as Organic Soil enhancer and plant nutrition. The present invention also provides process for preparation of novel organic fertilizer comprising steps of mechanical mixing of a portion of different Organic compounds, Micro Nutrients, Macro Nutrients, Organic Carbon, Micro-flora and Bio-char in specific % to get desired organic fertilizer to fulfill the current need of the soil for better fertility.
Background of the invention
Fertilizer is any organic or inorganic material of natural or synthetic origin (other than liming materials) that is added to a soil to supply one or more plant nutrients essential to the growth of plants. A recent assessment found that about 40 to 60% of crop yields are attributable to commercial fertilizer use.
Mined inorganic fertilizers have been used for many centuries, whereas chemically synthesized inorganic fertilizers were only widely developed during the industrial revolution.
Inorganic fertilizer use has also significantly supported global population growth - it has been estimated that almost half the people on the Earth are currently fed as a result of synthetic nitrogen fertilizer use.
Fertilizers typically provide, in varying proportions: Six macronutrients: Nitrogen (N), Phosphorous (P), Potassium (K), Calcium (Ca), Magnesium (Mg)
and Sulfur (S); Seven micronutrients: Boron (B), Chlorine (CI), Copper (Cu), Iron (Fe), Manganese (Mn),
Molybdenum (Mo) and Zinc (Zn). The macronutrients are consumed in larger quantities and are present in plant tissue in quantities from 0.15% to 6.0% on a dry matter (0% moisture) basis (DM). Micronutrients are consumed in smaller quantities and are present in plant tissue on the order of parts per million (ppm), ranging from 0.15 to 400 ppm DM, or less than 0.04% DM.
Only three other macronutrients are required by all plants: Carbon, Hydrogen and Oxygen. These nutrients are supplied by water and carbon dioxide.

Across the world, intense use of synthetic fertilizers in cultivating agricultural produces are causing the soil to lose natural fertility and as days passes, more and more quantity of fertilizers is required for obtaining the same output, as the soil becomes addicted to chemical fertilizers. Thus, it becomes a compulsion for farmers to use the same in ever increasing quantities. Soil fertility is diminishing gradually due to soil erosions, loss of nutrient, accumulation of salts and other toxic elements, water logging and un-balanced nutrient compensation. Organic wastes and bio-fertilizers are the alternate sources to meet the nutrient requirement of crops and to bridge the future gaps. Farming regions that emphasizing heavy chemical application led to adverse environmental, agricultural and health consequences. Many efforts are being exercised to combat the adverse consequences of chemical farming. Bio-fertilizer, organic manuring and bio-control have emerged as a promising component of integrating nutrient supply system in agriculture.
During our study, we found that use of heavy dose of synthetic fertilizers causes leaching out of Nitrous Oxide (N20) in soil, water as well as in the air. Nitrous Oxide in gaseous form, is 321 times more dangerous than Carbon Dioxide (C02) in terms of green house effect. Yet, this is an area not focused upon in the fight against global warming.
The practice of using more and more chemical fertilizers further increases leaching out of N2O. It also creates pressure on the world to develop infrastructure for production of more quantity of synthetic fertilizer to fulfill increasing requirements. In an era of scarcity of international resources in crude oil, price volatility is becoming a panic issue for the world.
It is also a fact that intensive use of synthetic fertilizer causes carcinogenic impact on agricultural produce. This is one of the major threats to mankind. Thus, it is most important for the world to minimize dependency on synthetic fertilizers and migrate to organic fertilizers. Organic fanning is one of the widely used methods, which is thought of as the best alternative to avoid the ill effects of chemical farming. There are several definitions of organic farming and the one given by the US Department of Agriculture (USDA) is considered the most coherent and stringent. It is defined as 'a system that is designed and maintained to produce agricultural products by the use of methods and substances that maintain the integrity of organic agricultural products until they reach the consumer.
Concept of organic farming is known in prior art as reflect in patents like US 6325837 Bl, US 6425933B1, US7662206 B2, US20100139345A1, WO0113706A1, US 20100251790A1, EP2 159 210 A2, WO 2007/035513, WO 00/44688, WO 00/44688, US 6517600 Bl. Patent WO 2009/144679 describe the process for preparing the soil additive product by aerobically processing carbon source

material at elevated temperature and for sufficient duration to decompose substantially to carbon source material aerobically and allowing beneficial activity to take place in the carbon source material and granulating the carbon source material.
The patent WO 00/44688 describe the methods of making organic compost from bovine manure by incubating the manure under aerobic condition followed by drying and pasteurizing of dried material and grinding of such pasteurized material in to powder. Fine powder enriched with nitrogen and humic acid source and use as organic compost. In U.S patent No 5597399 describe the method for soil enhancing compound production from mechanically mixing of composted agricultural waste like; bagasse rice hulls, corn husks and cotton gin waste.
Patent WO 2007/035513 describe process of fertilizer from biosolids like municipal biosolids and sludges, manures and animal residues, lagoon sludges, organic -containing sludges produced from food fermentation, sludge waste products, pharmaceutical fermentation waste, industrial fermention products, mixture/combinations thereof and adding of alkaline agent to such paste to make pH higher followed by adding of acid make pH neutral. Similary EP 2 159 210 A2 describe the methods for production of granulated organic fertilizer from sludge obtained from methane fermentation and admixture of glauconite to sludge. In US7662206 B2 describe the system devices and methods for treating organic sludges and converting in to organic fertilizer. Similarly US 6425933 Bl also provide the method of organic fertilizer production methods from manure.
U.S. Patent application no 6517600 BI describe the process for pure organic fertilize pellets from a compostable waste material or materials complying with organic standards comprising. In which first convert the waste material by composting in to fine particulate mass. Mix it with an agronomically acceptable source of nutrients to enhance compost fertilizer and blended mixture having a known nitrogen:phosphorus:potassium ration like 1-15:1-15:1-15. Such blend material pelletized at pressure 2000 - 6000 psi. In patent US 6325837 Bl is also describe the organic fertilizer from dehydrate forage plant and pelletizing of the same and its application to soil.
The US6174472 describe the process for formation of soil enhancing pellets from organic material including primary sewer sludge consisting of 60 % composted sewer sludge, 0 to 40 %

cellulosic plant material and 0 to 15 % soil and plant beneficiating chemicals. US 20100251790A1 describe methods for producing granular dry organic fertilizer from peat material mixture of 4 mm size. In contrast to that in patent WO 0113706Al describe method for preparing the chemically enhanced organic fertilizer pellets from a compostable waste material.
The present invention provides novel organic fertilizer in pelleted form and provide process for the preparation of novel organic fertilizer.
Object of the Invention
The main object of the present invention is to provide novel organic fertilizer.
Another object of the present invention is to provide process for the preparation of novel organic fertilizer.
Yet another objection of the present invention is to provide novel organic fertilizer containing organic compounds, micro nutrients, macro nutrients, organic carbon, micro-flora and bio-char in specific % value.
Detail Description of invention
The present invention relates to novel organic fertilizer and process for preparation of the same. More particularly, the present invention relates novel fertilizer act as Organic Soil enhancer and plant nutrition, The present invention also provides process for preparation of novel carbon neutral organic fertilizer comprising steps of mechanical mixing of a portion of different Organic compounds, Micro Nutrients, Macro Nutrients, Organic Carbon, Micro-flora and Bio-char in specific % value to get desired organic fertilizer to fulfill the current need of the soil for better fertility.
'Organic compounds' in accordance with the present invention is meant as any member of a large class of gaseous, liquid, or solid chemical compounds whose molecules contain carbon.
'Micro Nutrients' in accordance with the present invention is meant as elements essential for plant growth which are needed in only very small (micro) quantities . These elements are sometimes called minor elements or trace elements, but use of the term micronutrient is encouraged by the American Society of Agronomy and the Soil Science Society of America.
'Macro Nutrients' in accordance with the present invention is meant as element, such

as carbon, hydrogen, oxygen or nitrogen required in large proportion for the normal growth and development of a plant.
'Micro Flora' in accordance with the present invention is meant as living microorganisms that are so small that they can be seen only with a microscope and that maintain a more or less constant presence in a particular area, e.g. the pharynx or the rumen. Includes bacteria, viruses, protozoa, fungi.
'Bio-Char' in accordance with the present invention is meant as a charcoal-type material produced by cooking organic matter in a low-oxygen environment (pyrolysing) -holds great potential for carbon mitigation
The Organic compounds used in the present invention are selected from Tissues from dead plant and animals, Semi Microbial biomass like Bacteria, Fungi and microbes.
The selected organic compounds in proper % amounts improves soil aeration, soil texture, water holding capacity, increases nutrient exchanges between soil and plant, Balances soil pH, increases microbial biomass and nutrient buffer capacity. The organic compounds as per the present invention are in the range of 50% to 80%.
The Micro Nutrients are selected from Copper (Cu), Iron (Fe), Zinc (Zn), Manganese (Mn), Boron (Bo), Molybdenum (Mo).
The Macro Nutrients are selected from Nitrogen (N), Phosphorus (P), Potassium (K), Sulphur (S), Magnesium (Mg), Calcium (Ca).
The organic carbon refers as soil organic carbon (SOC) occurs in soil organic matter (SOM) which provides carbon and energy sources to soil microbes and increases microbial activity. SOC is 50-60% part of the SOM. SOC influences the physical structure of the soil, the soil's ability to store water ability, and ability to supply nutrients to plants through ion exchange. Increased amount of SOC increases carbon sequestration which turns to GHG mitigation.
The micro flora used in the present invention are collective bacteria and other micro-organisms in an ecosystem. The bacteria are selected from Pseudomonas sp., Bacillus sp., Azotobacter sp., Rhizobium sp., Calcium Solubilizer, Zinc Solubilizer, Silica Solubilizer and like. Micro Flora provides plant protection and/or nutrients. The micro flora are selected from Pseudomonas sp., Baccillus sp., Trichoderma sp., Azotobacter sp., Rhizobium sp., and like.
Bio-Char as per the present invention is biomass that is converted to a char-like material and has high soil stable carbon. It increases soil aeration in fine textured soils, improves soil aggregation, increases the retention of water in the rooting zone, acts as adsorption sites for microbial. Bio-char does not directly provide nutrients to the soil and/or plants but provides an environment for soil beneficial micro flora that benefit to the plant.
We have also observed that the ratio of organic carbon to nitrogen C:N ratio is also important for the plant growth. C:N ratio of the organic material influences the rate of decomposition of organic compounds as the decomposition either releases (mineralization) or immobilizes soil nitrogen. Carbon is used for energy and Nitrogen is used for building tissues. An Optimal C:N Ratio of organic matter added to soil should be < 20:1. Microbes need

1 kg of Nitrogen for every 8 kg of Carbon. The C:N ratio as per the present invention ranges from 7-15:1, The preferable C:N Ratio is from 8-12:1.
The pH of the fertilizer as per the present invention is maintained between 7 to 7.5.
There are various kinds of minerals and organic matter lying in the soil. In the early growth stage, plant may not be able to fully absorb nutrients from the soil. Considering this fact, to achieve the immediate effect, we have added the following naturally available acids and hormones to catalyze the growth.
1. Humic Acid - naturally available acid, which provides immediate carbon to the plant in early stage as well as causes mobilization of other mineral elements. It also enhances the soil's physical, chemical and biological property.
2. Gibberellic acid (GA3) - It is a group of naturally occurring plant hormones, which induces the root surface growth in the early stage, and enhances capacity of nutrient intake.
3. Indol-3 Acetic Acid (IAA) - It is a group of auxins, which are naturally occurring plant hormones synthesized in the apical portion of the plant. It catalyzes vegetative growth and trans-location of photosynthetic sink from upper portion to downward.
To provide total plant nutrition and presence of minerals around the root zone, we have added certain bacteria for the following reasons:
1. Nitrogen Fixation: Azotobacter sp., Rhizobium sp.
2. Phosphorus Solubilizer: Bacillus sp.
3. Potash Solubilizer : Pseudonmnas sp.
4. Calcium Solubilizer: Bacillus sp.
5. For Zinc Solubilizer bacteria
6. For Silica Solubilizer bacteria
7. Organic Matter Decomposer: Pseudomonas sp.
In order to maintain the adequate quantity and quality of bacteria in plant around the root zone and soil, we have added more fixed carbon, which is a house for various bacteria, to maintain natural fertility of soil.
plants may infestation of various kinds of pathogens including soil borne fungus, insects, and nematodes. To take preventive action from these pathogens, we have developed the following biological agents:
Trichoderma sp: To prevent pathogenic soil borne fungal attack Baeveria sp: To protect the root zone from termite attack
Pacilomyceas sp: To protect the root zone from nematodes (Meloydogyne javanica) attack Further, the present invention provides a process for the production of novel organic fertilizer as described in the present invention.

The process for the production of novel organic fertilizer as per the present invention comprises steps:
A. Mixing of fertilizer raw materials and feeding to Apron feeder,
B. Passing the well mixed material of step A to rotary screen followed by vibro screen
C. Passing the well screened material of step B to raw material silo
D. From silo equal sized mixed material passing to hammer mill,
E. Powdered material from Step D passing through filter cyclone and filtered material
(less than 2 mm) move to ripening mixture,
F. Well prepared material of step E fortified with different bacterial and fungal culture
followed by molasses addition from molasses tank
G. Passing of well mixed material of step F to pellet mill
H. Cutting the extruded pellets of step - G by adjustable cutter assembly to prepare
pellets of about 4 mm to 10 mm of diameter and 6 mm to 20 mm of length followed by
cooling through counter flow cooler,
I. Screening the pellets of step - r through screen 13 for removal of any fine particles to
give pure product
J. Screened pellets from step I pass to finish good silo followed by selling in form of
loose pellet or in bagging by bagging machine.
Further the fertilizers raw material means a mixture of all Organic Compounds, Micro Nutrients, Macro Nutrients and Bio-char. Compositional analysis of fertilizer pellets by method outlined above is mention in below table;

Sr.No Parameter Values
1 1 Nitrogen % Phosphorous % 2.8-3.0 2.2 - 2.5
3 Potassium % 2.2-2.5
4 Calcium % 2.0-2.5
5 Magnesium % 0.45-0.48.
6 Sulfur % 4.0-5.0
7 Organic Matter % 70-80
8 Organic Carbon % 40-45
9 pH 7.0 -7.2
10 Zinc % 0.003 - 0.005
11 Manganese % 0.04 - 0.05
12 Copper % 0.001 -0.0015

13 Iron % 0.060 - 0.065
14 Molybdenum % 0.00015-0.0002
15 Boron % 0.22-0.23
16 Cadmium % 0
17 Cobalt % 0
18 Moisture % 6 to 7
19 C:N ratio 15-17: 1
The detailed process of the present invention can be defined as below:
A. Premixing of fertilizer organic & inorganic Compounds:
Organic compounds of fertilizer like, Castor DOC (1 to 60 %), biochar (0% to 20%), castor shell (1 to 20 %), zinc sulphate (0% to 1%) and biomass ash (0% to 15%) mixed well in desired proportion at clean mixing area by rotating all compounds up and down. Mixing was done by manual or mechanically. Well mixed material feed to apron feeder
B. Screening of mixed material
Well mixed material feed to apron feeder followed by rotary screen, well mixed raw material screened in rotary drum screen and rejected material recovered through destoner. All passed materiel from rotary screen to vibro screen and rejected material recovered through destoner.
C. Storage of well mixed material
Well mixed and well screen material stored in raw material silo, Silo could be cylinder or rectangular.
D. Size reduction of raw material
Well mixed and well screened material from silo feed to hammer mill and final size is reduced to less than 2 mm. Dust particles are filtered through cyclone filter and dust free material pass to ripening mixer
E. Fortification of raw material
Aseptically grown respective bacterial culture with density 1 X 1011 (80-100 ml/ton) and fungal spore powder with density 3 X 109 to 5 X 109 (28 to 35 g/ton) were apply to premixed raw material. The bacteria specifically Azotobacter sp., Rhizobium sp., Bacillus sp., Pseudomonas sp., Zinc Solubilizer bacteria, Silica Solubilizer bacteria and Pseudomonas sp. and fungus specifically; Trichoderma sp., Baeveria sp. and Pacilomyceas sp. were used. Liquid bacterial

culture spray evenly on premixed material by mechanical spraying pump at rate of 25 ml to 90 ml /minute. Fungi powder also spread evenly by mechanical way to 1 gram to 14 grams/minute. Castor oil (0% to 5%) also spray mechanically at dosing rate of 100 liters/hour. Similarly molasses (1% to 8%) was also sprayed evenly by mixing them with water by mechanical way.
F. Application of PGR & organic acids
The PGR specifically GA (0% to 0.01%), IAA (0% to 0.01% ), Cytokinin (0% to 0.01%) and organic acids specifically Humic acid (0% to 2 %) were used. Desired concentration of PGR and organic acids were spray on premixed material fortified with bacterial culture, fungal spore and molasses. Again after spraying PGR and organic acids mix all material properly.
G. Final mixing
After application of PGR & organic acids, vigorously all materials were mixed by manual/mechanical so all material become even with respect to composition. Well mixed material conveyed to pellet mill.
H. Pelletization:
Material conveyed to the pellet mill containing die with holes of 6 mm diameter. The extruded pellets are cut by adjustable cutter assembly to produced pellets of 6 mm to 20 mm length. The temperature of extruded pallets is 50 to 80 °C, pellets are air cooled and temperature reduced to ambient temperature by counter flow cooler. Cooled pellets are pass through screen to remove dust particle if produced during processing.
G. Storage & Packaging
Cooled pellets were conveyed to finish good silo, from silo pellets can transferred to direct truck in loose pelletes or bagging in suitable size (1 -25 kg ) in plastic bag by automatic machine.
ADVANTAGES:
The advantages of the novel organic fertilizer prepared as per the present invention are:
■ Slow and sustained release of nutrients " Easy to store
■ More Durability
■ No Bad Odour
■ Better aeration in the soil
■ Targeted delivery system turns into better efficiency
■ No synthetic chemicals
■ Easy handling and application

■ Improves nutrient efficiency & reduces leaching The present invention is further described by the following non-limiting examples:
Example 1: Preparation of organic fertilizer and pelletization of the same Organic fertilizer pellets were prepared from component mention below:

Sr.No Name of Component % of component in fertilizer pellets Amount of component
added for 1000 kg fertilizer
pellet production
1 Castor DOC 55 550 kg
2 Biochar 10 100 kg
3 Castor shell 15 150 kg
4 Biomass ash 10.2 102 kg
5 Castor oil 1.6 16 kg
6 Molasses 6.7 67 kg
7 Zinc sulphate 0.1 1kg
8 Gibberellic acid (GA) 0.00250 0.03 kg
9 Indole acetic acid (IAA) 0.00250 0.03 kg
10 Cytokinin 0.00250 0.03 kg
11 Humic Acid 1.1 11kg
12 Total Bacterial culture - 700 ml
13 Total Fungal powder - 1kg
Procedure:
Castor DOC (550 kg), biochar (100 kg), biomass ash (102 kg), castor shell (150 kg) and Zinc sulphate (1.0 kg) were placed one above the other and form a pile. Mix all component by mechanical loader. Mixed material pass through rotary screen and vibro screen to remove any foreign particle like stone, metal etc. Screened material stored in silo and feeding to pellet mill for uniform sizing (size > 2mm), small particles/dust particle are collected by cyclone filter

and filtered material stored in ripening mixture. In ripening mixture liquid bacterial culture spray evenly on premixed material by mechanical spraying pump at rate of 30 ml /minute. 100 ml of each bacterial culture (Azotobacter sp., Rhizobium sp., Bacillus sp., Pseudomonas sp., Zinc Solubilizer bacteria, Silica Solubilizer bacteria and Pseudomonas sp.) with cell density of 1 X 10n were mixed just prior to spraying. Three fungal powder (Trichoderma sp., Baeveria sp. and Pacilomyceas sp.) with spore density 5 X 109 were sprayed evenly by mechanical way at rate of 5 grams/minute. Further castor oil (16 kg) and molasses ( 67 kg) were added mechanically at dosing rate of 100 liters/hour. Finally the PGR [GA (0.03 kg, IAA (0.03 kg), Cytokinin (0.03 kg)] and organic acid [Humic acid (11 kg) ] were added and mixed all material mechanically to form a homogenize mixture. Well mixed material conveyed to the pellet mill (Inovo 52-14, R.K. Machines) containing die with holes of 4 mm diameter. The extruded pellets are cut by adjustable cutter assembly to produced pellets of 6 mm to 20 mm length. The temperature of extruded pallets is 50 to 80 °C, pellets are air cooled and temperature reduced to ambient temperature by counter flow cooler (RKM 18 X 18, R. K. machines). Cooled pellets are pass through screen to remove dust particle if produced during processing. Results of produced pellets:

Sr. No Parameter Values
1 Nitrogen % 2.83
2 Phosphorous % 2.19
3 Potassium % 1.46
4 Calcium % 2.8
5 Magnesium % 0.33
6 Sulfur % 3.5
7 Organic Matter % 70.1
8 Organic Carbon % 40.1
9 PH 7.03
10 Zinc % 0.01

11
Manganese % 0.04
12 Copper % 0.001
13 Iron % 0.068
14 Molybdenum % 0.00014
15 Boron % 0.23
16 Cadmium % 0
17 Cobalt % 0
18 Moisture % 6.5
19 C:N ratio 14.17
Example 2: Preparation of organic fertilizer and peptization of the same
Organic fertilizer pellets were prepared from component mention below:

Sr. No Name of Component % of component in fertilizer pellets Amount of component
added for 1000 kg fertilizer
pellet production
1 Castor DOC 60 600
2 Biochar 10 100
3 Castor shell 10 100
4 Biomass ash 10.8 108
5 Castor oil 1 10
6 Molasses 6.5 65
7 Zinc sulphate 0.2 2
8 Gibberellic acid (GA) 0.00012 0.0012 kg
9 Indole acetic acid (IAA) 0.00012 0.0012kg 0.0012 kg
10 Cytokinin 0.00012

13 Humic Acid 1.5 15 kg
14 Total Bacterial culture 700 ml
15 Total Fungal powder
1kg
Procedure:

Castor DOC (600 kg), biochar (100 kg), biomass ash (108 kg), castor shell (100 kg) and Zinc sulphate (2.0 kg) were placed one above the other and form a pile. Mix all component by mechanical loader. Mixed material pass through rotary screen and vibro screen to remove any foreign particle like stone, metal etc. Screened material stored in silo and feeding to pellet mill for uniform sizing (size > 2mm), small particles/dust particle are collected by cyclone filter and filtered material stored in ripening mixture. In ripening mixture liquid bacterial culture spray evenly on premixed material by mechanical spraying pump at rate of 30 ml /minute. 100 ml of each bacterial culture (Azotobacter sp., Rhizobium sp., Bacillus sp., Pseudomonas sp., Zinc Solubilizer bacteria, Silica Solubilizer bacteria and Pseudomonas sp.) with cell density of 2 X 1011 were mixed just prior to spraying. Three fungal powder (Trichoderma sp., Baeveria sp. and Pacuomyceas sp.) with spore density 5 X 109 were sprayed evenly by mechanical way at rate of 5 grams/minute. Further castor oil (10 kg) and molasses (65 kg) were added mechanically at dosing rate of 100 liters/hour. Finally the PGR [GA (0.0012 kg, IAA (0.0012 kg), Cytokinin (0.0012 kg)] and organic acid [Humic acid (15 kg) ] were added and mixed all material mechanically to form a homogenize mixture. Well mixed material conveyed to the pellet mill (Inovo 52-14, R.K. Machines) containing die with holes of 4 mm diameter. The extruded pellets are cut by adjustable cutter assembly to produced pellets of 6 mm to 20 mm length. The temperature of extruded pallets is 50 to 80°C, pellets are air cooled and temperature reduced to ambient temperature by counter flow cooler (RKM 18 X 18, R. K. machines). Cooled pellets are pass through screen to remove dust particle if produced during processing. Results of fertilizer pellets:

Sr. No Parameter Values
] Nitrogen % 2.86
2 Phosphorous % 2.26
3 Potassium % 2.3
4 Calcium % 2.51

5
Magnesium % 0.42
6 Sulfur % 4.2
7 Organic Matter % 72
8 Organic Carbon % 41.5
9 pH 7.1
10 Zinc % 0.008
11 Manganese % 0.04
12 Copper % 0.001
13 Iron % 0.07
14 Molybdenum % 0.00017
15 Boron % 0.22
16 Cadmium % 0
17 Cobalt % 0
18 Moisture % 7.8
19 C:N ratio 14.51
Example 3: Preparation of organic fertilizer and pelletization of the same
Organic fertilizer pellets were prepared from component mention below:

Sr. No Name of Component % of component in fertilizer pellets Amount of component
added for 1000 kg fertilizer
pellet production
1
2 Castor DOC 65 8 650 80

Biochar

3 4 Castor shell Biomass ash 8 10.7 80 107
5 Castor oil 2 20
6 Molasses 4.5 45
7 Zinc sulphate 0.3 3
8 Gibberellic acid (GA) 0.00018 0.0018 kg
9 Indole acetic acid (IAA) 0.00018 0.0018 kg
10 Cytokinin 0.00018 0.0018 kg

11 Humic Acid 1.5 15 kg
12 Total Bacterial culture - 700 ml
13 Total Fungal powder - 1kg
Procedure:
Castor DOC (650 kg), biochar (100 kg), biomass ash (107 kg), castor shell (80 kg) and Zinc sulphate (3.0 kg) were placed one above the other and form a pile. Mix all component by mechanical loader. Mixed material pass through rotary screen and vibro screen to remove any foreign particle like stone, metal etc. Screened material stored in silo and feeding to pellet mill for uniform sizing (size > 2mm), small particles/dust particle are collected by cyclone filter and filtered material stored in ripening mixture. In ripening mixture liquid bacterial culture spray evenly on premixed material by mechanical spraying pump at rate of 30 ml /minute. 100 ml of each bacterial culture (Azotobacter sp., Rhizobium spv Bacillus sp., Pseudomonas sp., Zinc Solubilizer bacteria, Silica Solubilizer bacteria and Pseudomonas sp) with cell density of 1 X 1011 were mixed just prior to spraying. Three fungal powder (Trichoderma sp., Baeveria sp. and Pacilomyceas sp.) with spore density 5 X 109 were sprayed evenly by mechanical way at rate of 5 grams/minute. Further castor oil (20 kg) and molasses (45 kg) were added mechanically at dosing rate of 100 liters/hour. Finally the PGR [GA (0.0018 kg, IAA ( 0.0018 kg), Cytokinin (0.0018 kg)] and organic acids [Humic acid (15 kg)] were added and mixed all material mechanically to form a homogenize mixture. Well mixed material conveyed to the pellet mill (Inovo 52-14, R.K. Machines) containing die with holes of 4 mm diameter. The extruded pellets are cut by adjustable cutter assembly to produced pellets of 6 mm to 20 mm length. The temperature of extruded pallets is 50 to 80°C pellets are air cooled and temperature reduced to ambient temperature by counter flow cooler (RKM 18 X 18, R. K. machines). Cooled pellets are pass through screen to remove dust particle if produced during processing. Results of fertilizer pellets:

Sr. No
Parameter Values
1 Nitrogen % 2.94
2 Phosphorous % 2.26
3 Potassium % 1.49
4 Calcium % 2.12
5 Magnesium % 0.44
6 Sulfur % 4.6
7 Organic Matter % 75.24
8 Organic Carbon % 43
9 pH 7
10 Zinc % 0.012
11 Manganese % 0.03
12 Copper % 0.002
13 Iron % 0.07
14 Molybdenum % 0.00014
15 Boron % 0.26
16
17 Cadmium % Cobalt % 0 0
18 Moisture % 7.5
19 C:N ratio 14.63
Example 4: Preparation of organic fertilizer and peptization of the same
Organic fertilizer pellets were prepared from component mention below:

Sr. No Name of Component % of component in fertilizer pellets Amount of component
added for 1000 kg fertilizer
pellet production
1 Castor DOC 70 700
2 Biochar 6 60
3 Castor shell 6 60

4 Biomass ash 10.5 105
5 Castor oil 2 20
6 Molasses 3.5 35
7 Zinc sulphate 0.5 5
8 Gibberellic acid (GA) 0.00100 0.0100 kg
9 Indole acetic acid (IAA) 0.00100 0.0100 kg
10 Cytokinin 0.00100 0.0100 kg
11 Humic Acid 1.5 15 kg
12 Total Bacterial culture - 700 ml
13 Total Fungal powder - 1kg
Procedure:
Castor DOC (700 kg), biochar (60 kg), biomass ash (105 kg), castor shell (60 kg) and Zinc sulphate (5.0 kg) were placed one above the other and form a pile. Mix all component by mechanical loader. Mixed material pass through rotary screen and vibro screen to remove any foreign particle like stone, metal etc. Screened material stored in silo and feeding to pellet mill for uniform sizing (size > 2mm), small particles/dust particle are collected by cyclone filter and filtered material stored in ripening mixture. In ripening mixture liquid bacterial culture spray evenly on premixed material by mechanical spraying pump at rate of 30 ml /minute. 100 ml of each bacterial culture (Azotobacter sp., Rhizobium sp., Bacillus sp., Pseudomonas sp., Zinc Solubilizer bacteria, Silica Solubilizer bacteria and Pseudomonas sp.) with cell density of 1 X 1011 were mixed just prior to spraying. Three fungal powder (Trichoderma sp., Baeveria sp. and Pacilomyceas sp.) with spore density 5 X 109 were sprayed evenly by mechanical way at rate of 5 grams/minute. Further castor oil (20 kg) and molasses (35 kg) were added mechanically at dosing rate of 100 liters/hour. Finally the PGR [GA (0.010 kg, IAA ( 0.010 kg), Cytokinin ( 0.010 kg)] and organic acid [Humic acid (15 kg)] were added and mixed all material mechanically to form a homogenize mixture. Well mixed material conveyed to the pellet mill (Inovo 52-14, R.K. Machines) containing die with holes of 4 mm diameter. The

extruded pellets are cut by adjustable cutter assembly to produced pellets of 6 mm to 20 mm
length. The temperature of extruded pallets is 50 to 80 °C, pellets are air cooled and
temperature reduced to ambient temperature by counter flow cooler (RKM 18 X 18, R. K.
machines). Cooled pellets are pass through screen to remove dust particle if produced during
processing.
Results of fertilizer pellets:

Sr. No Parameter Values
1 Nitrogen % 2.86
2 Phosphorous % 2.26
3 Potassium % 1.98
4 Calcium % 1.89
5 Magnesium % 0.45
6 Sulfur % 4.86
7 Organic Matter % 76.4
8 Organic Carbon % 42.51
9 PH 7.12
10 Zinc % 0.008
11 12 13 14
15 Manganese % Copper % Iron %
Molybdenum % Boron % 0.040 0.001 0.06 0.00020
0.21
16 Cadmium % 0
17 Cobalt % 0
18 Moisture % 6.8
19 C:N ratio 14.86
Example 5: Preparation of organic fertilizer and pelletization of the same

Organic fertilizer pellets were prepared from component mention below:

ST. No Name of Component % of component in fertilizer pellets Amount of component
added for 1000 kg fertilizer
pellet production,
1 Castor DOC 40 400
2 Biochar 20 200
3 Castor shell 20 200
4 Biomass ash 8.51 85.1
5 Castor oil 4 40
6 Molasses 6 60
7 Zinc sulphate 0.01 0.1
8 Gibberellic acid (GA) 0.01000 0.1000 kg
9
10
11
12
13 Indole acetic acid (IAA)
Cytokinin
Humic Acid
Total Bacterial culture
Total Fungal powder 0.01000
0.01000
1.5 0.1000 kg
0.1000 kg
15kg
700 ml 1kg
Procedure:
Castor DOC (400 kg), biochar (200 kg), biomass ash (85.1 kg), castor shell (200 kg) and Zinc sulphate (0.10 kg) were placed one above the other and form a pile. Mix all component by mechanical loader. Mixed material pass through rotary screen and vibro screen to remove any foreign particle like stone, metal etc. Screened material stored in silo and feeding to pellet mill for uniform sizing (size > 2mm), small particles/dust particle are collected by cyclone filter and filtered material stored in ripening mixture. In ripening mixture liquid bacterial culture spray evenly on premixed material by mechanical spraying pump at rate of 30 ml /minute. 100 ml of each bacterial culture {Azotobacter sp., Rhizobium sp., Bacillus sp., Pseudomonas sp., Zinc Solubilizer bacteria, Silica Solubilizer bacteria and Pseudomonas sp.) with cell density of 1 X 1011 were mixed just prior to spraying. Three fungal powder (Trichoderma sp., Baeveria sp.

and Pacilomyceas sp.) with spore density 5 X 109 were sprayed evenly by mechanical way at rate of 5 grams/minute. Further castor oil (40 kg) and molasses (60 kg) were added mechanically at dosing rate of 100 liters/hour. Finally the PGR [GA (0.100 kg, IAA (0.100 kg), Cytokinin ( 0.100 kg)] and organic acid [Humic acrd (15 kg)] were added and' mixed all material mechanically to form a homogenize mixture. Well mixed material conveyed to the pellet mill (Inovo 52-14, R.K. Machines) containing die with holes of 4 mm diameter. The extruded pellets are cut by adjustable cutter assembly to produced pellets of 6 mm to 20 mm length. The temperature of extruded pallets is 50 to 80°C, pellets are air cooled and temperature reduced to ambient temperature by counter flow cooler (RKM 18 X 18, R. K. machines). Cooled pellets are pass through screen to remove dust particle if produced during processing. Results of fertilizer pellets:

Sr. No Parameter
Values
1 Nitrogen % 2.81
2 Phosphorous % 2.15
3 Potassium % 2.08
4 Calcium % 2.1
5 6 Magnesium % Sulfur % 0.4
4.77
7
8 9 Organic Matter % Organic Carbon % pH 76.8 43.1 7.2
10 Zinc % 0.001
11 Manganese % 0.05
12 Copper % 0.002
13 Iron % 0.06
14 Molybdenum % 0.00018
15 Boron % 0.22

16
Cadmium % 0
17 Cobalt % 0
18 Moisture % 6.8
19 C:N ratio 15.34
Example 6: Preparation of organic fertilizer and pelletization of the same
Organic fertilizer pellets were prepared from component mention below:

Sr. No Name of Component % of component in fertilizer pellets Amount of component
added for 1000 kg fertilizer
pellet production
1 Castor DOC 59 590
2 Biochar 12 120
3 Castor shell 17 170
4 Biomass ash 4 40
5 Castor oil 1 10
6 Molasses 5.49 54.9
7 Zinc sulphate 0.01 0.1
8 Gibberellic acid (GA) 0.00005 0.0005 kg
9 Indole acetic acid (IAA) 0.00005 0.0005 kg
10 Cytokinin 0.00005 0.0005kg
11 Humic Acid 2 20 kg
12 Total Bacterial culture - 700 ml
13 Total Fungal powder - 1kg
Procedure:
Castor DOC (590 kg), biochar (120 kg), biomass ash (102 kg), castor shell (170 kg) and Zinc sulphate (0.10 kg) were placed one above the other and form a pile. Mix all component by mechanical loader. Mixed material pass through rotary screen and vibro screen to remove any foreign particle like stone, metal etc. Screened material stored in silo and feeding to pellet mill

for uniform sizing (size > 2mm), small particles/dust particle are collected by cyclone filter and filtered material stored in ripening mixture. In ripening mixture liquid bacterial culture spray evenly on premixed material by mechanical spraying pump at rate of 30 ml /minute. 100 ml of each bacterial culture (Azotobacter sp., Rhizobium sp., Bacillus sp., Pseudomonas sp., Zinc Solubilizer bacteria, Silica Solubilizer bacteria and Pseudomonas sp.) with cell density of 1 X 1011 were mixed just prior to spraying. Three fungal powder (Trichoderma sp., Bneveria sp. and Pacilomyceas sp.) with spore density 5 X 109 were sprayed evenly by mechanical way at rate of 5 grams/minute. Further castor oil (10 kg) and molasses (54.9 kg) were added mechanically at dosing rate of 100 liters/hour. Finally the PGR [GA (0.0005 kg, IAA (0.0005 kg), Cytokinin (0.0005 kg)] and organic acid [Humic acid (20 kg)] were added and mixed all material mechanically to form a homogenize mixture. Well mixed material conveyed to the pellet mill (Inovo 52-14, R.K. Machines) containing die with holes of 4 mm diameter. The extruded pellets are cut by adjustable cutter assembly to produced pellets of 6 mm to 20 mm length. The temperature of extruded pallets is 50 to 80°C, pellets are air cooled and temperature reduced to ambient temperature by counter flow cooler (RKM 18 X 18, R. K. machines). Cooled pellets are pass through screen to remove dust particle if produced during processing. Results of fertilizer pellets:

Sr. No Parameter Values
1 Nitrogen % 2.83
2 Phosphorous % 2.5
3 Potassium % 2.22
4 ' Calcium % 2.05
5 Magnesium % 0.42
6 Sulfur % 4.2
7 Organic Matter % 76.9

8
Organic Carbon % 42.1
9 pH 7.1
10 Zinc % 0.007
11 Manganese % 0.04
12 Copper % 0.002
13 Iron % 0.07
14 Molybdenum % 0.00020
15 Boron % 0.23
\6 Cadmium % 0
17 Cobalt % 0
18 Moisture % 6.7
19 C:N ratio 14.88

Example 7: Preparation of organic fertilizer and pelletization of the same
Organic fertilizer pellets were prepared from component mention below:

Sr. No Name of Component % of component in fertilizer pellets Amount of component
added for 1000 kg fertilizer
pellet production
1 Castor DOC 50 500
2 Biochar 15 150
3 Castor shell 20 200
4 Biomass ash 4.5 45
5 Castor oil 1 10
6 Molasses 8 80
7 Zinc sulphate 0.02 0.2
8 9 Gibberellic acid (GA) Indole acetic acid (IAA) 0.00009 0.00009 0.0009 kg 0.0009 kg
10 11 Cytokinin Humic Acid 0.00009 1.8 0.0009 kg 18 kg
12 Total Bacterial culture 700 mli
13 Total Fungal powder - 1kg
Procedure:
Castor DOC (500 kg), biochar (150 kg), biomass ash (45 kg), castor shell (200 kg) and Zinc sulphate (0.20 kg) were placed one above the other and form a pile. Mix all component by mechanical loader. Mixed material pass through rotary screen and vibro screen to remove any foreign particle like stone, metal etc. Screened material stored in silo and feeding to pellet mill for uniform sizing (size > 2mm), small particles/dust particle are collected by cyclone filter and filtered material stored in ripening mixture. In ripening mixture liquid bacterial culture spray evenly on premixed material by mechanical spraying pump at rate of 30 ml /minute. 100 ml of each bacterial culture (Azotobacter sp., Rhizobium sp., Bacillus sp., Pseudomonas sp.,

Zinc Solubilizer bacteria, Silica Solubilizer bacteria and Pseudomonas sp.) with cell density of 2 X 1011 were mixed just prior to spraying. Three fungal powder (Trichoderma sp., Baeveria sp. and Pacilomyceas sp.) with spore density 5 X 109 were sprayed evenly by mechanical way at rate of 5 grams/minute. Further castor oil (10 kg) and molasses (80 kg) were added mechanically at dosing rate of 100 liters/hour. Finally the PGR [GA (0.0009 kg, IAA (0.0009 kg), Cytokinin (0.0009 kg)] and organic acid [Humic acid (18 kg)] were added and mixed all material mechanically to form a homogenize mixture. Well mixed material conveyed to the pellet mill (Inovo 52-14, R.K. Machines) containing die with holes of 4 mm diameter. The extruded pellets are cut by adjustable cutter assembly to produced pellets of 6 mm to 20 mm length. The temperature of extruded pallets is 50 to 80°C, pellets are air cooled and temperature reduced to ambient temperature by counter flow cooler (RKM 18 X 18, R. K. machines). Cooled pellets are pass through screen to remove dust particle if produced during processing. Results of fertilizer pellets:

Sr. No Parameter Values
1 Nitrogen % 2.88
2 Phosphorous % 1.98
3 Potassium % 2.34
4 Calcium % 2.1
5 Magnesium % 0.43
6 Sulfur % 4.27
7 Organic Matter % 71
8 Organic Carbon % 43.87
9
i pH 7
10 Zinc % 0.008
11 Manganese % 0.04
12 Copper % 0.001
13 Iron % 0.06

14
Molybdenum % 0.00020
15 Boron % 0.23
16 Cadmium % 0
17 Cobalt % 0
18 Moisture % 6.8
19 C:N ratio 15.22

Claims:
1. A novel organic fertilizer containing various processing waste material, PGRs, beneficial
micro organisms, suitable lubricant & binder. Method to produce the said organic fertilizer comprising the following steps,
Step -1. Mixing of raw material
Step - II. Physical cleaning of mixed material
Step - III. Size reduction {less than 2 mm)
Step - IV. Fortification with beneficial bacterial culture, fungal culture, PGRs, organic acid,
lubricants and binders Step - V. Pelletization of well mixed fortified material Step - VI. Cooling of fertilized pellets and packaging
2. The organic fertilizer produced by methods as claimed in claim 1 has Moisture % 6 -7, pH 7.0 - 7.2, Nitrogen % 2.8 -3.0, Phosphorus % 2.2 -2.5, Potassium % 2.2 -2.5, Calcium % 2.0-2.5, Magnesium % 0.45 -0.48, Sulfur % 4.0 -5.0, Organic matter % 70 -80, Organic carbon % 40 -45, Zinc % 0.003-0.005, Manganese % 0.04-0.05, Copper % 0.001-0.0015, Iron % 0.060 -0.065, Molybdenum % 0.00015-0.0002, Boron % 0.22 - 0.23 and C:N ratio 15-17:1.
3. A method as claimed in claim 1, where in raw material are castor DOC, castor shell, biomass ash, and zinc sulphate.
4. Raw material as claimed in claim 3, where in castor DOC in range of 1 to 60 %, Biochar 0 to 20 %, castor shell 1 to 20 %, biomass ash 0 to 15 % and zinc sulphate 0 to 1 %.
5. A method as claimed in claim 1, where in physical cleaning is done by mechanical way using various screens and magnetic belt and size reduction is done through hemmer mill to particle size less than 2 mm.
6. A method as claimed in claim 1, where in bacterial culture are Azotobacter sp., Rhizobium sp., Bacillus sp, Pseudomonas sp., Zinc solubilizer bacteria, Silica solubilizer bacteria and Pseudomonas sp., with cell density 1 X 1011 per ml and amount of mechanically addition of each culture is in range of 80 to 100 ml per ton.
7. A method as claimed in claim 1, where in fungal culture are Trichoderma sp., Baeveria sp., and Pacilomyceas sp., with spore density 5 X 109 per gram and mechanically addition of each fungal powder is in range of 28 g to 35 g per ton.

8. A method as claimed in claim 1, where in PGRs are Gibberellic acid, Indole acetic acid, Cytokinin at concentration of 0 to 0.1 % and organic acid as humic acid at concentration of 0.5 to 2%.
9. A method as claimed in claim 1, where in as lubricant is castor oil at concentration of 0 to 5 % and as binder molasses at concentration of 1 to 8 %.
10. The organic fertilizer containing component as claimed in any of the claim above is in the form of compounds or composites or aggregates or agglomerates or granulates or powder or briquettes or pellets of different size, different shapes, odor and color.

Documents

Application Documents

# Name Date
1 881- MUM -2012 - AFR - 31-8-2012.pdf 2023-10-26
1 881-MUM-2012-Other Patent Document-220216.pdf 2018-08-11
2 881-MUM-2012-AbandonedLetter.pdf 2019-12-09
2 881-MUM-2012-FORM 3.pdf 2018-08-11
3 881-MUM-2012-FORM 2.pdf 2018-08-11
3 881-MUM-2012-FER.pdf 2019-02-01
4 881-MUM-2012-FORM 2(TITLE PAGE).pdf 2018-08-11
4 881-MUM-2012-ABSTRACT(25-3-2013).pdf 2018-08-11
5 881-MUM-2012-FORM 2(TITLE PAGE)-(25-3-2013).pdf 2018-08-11
5 881-MUM-2012-ABSTRACT.pdf 2018-08-11
6 881-MUM-2012-FORM 2(25-3-2013).pdf 2018-08-11
6 881-MUM-2012-CLAIMS(25-3-2013).pdf 2018-08-11
7 881-MUM-2012-Form 18-220216.pdf 2018-08-11
7 881-MUM-2012-CORRESPONDENCE(25-3-2013).pdf 2018-08-11
8 881-MUM-2012-FORM 1.pdf 2018-08-11
8 881-MUM-2012-CORRESPONDENCE.pdf 2018-08-11
9 881-MUM-2012-DESCRIPTION(COMPLETE)-(25-3-2013).pdf 2018-08-11
9 881-MUM-2012-DESCRIPTION(PROVISIONAL).pdf 2018-08-11
10 881-MUM-2012-DESCRIPTION(COMPLETE)-(25-3-2013).pdf 2018-08-11
10 881-MUM-2012-DESCRIPTION(PROVISIONAL).pdf 2018-08-11
11 881-MUM-2012-CORRESPONDENCE.pdf 2018-08-11
11 881-MUM-2012-FORM 1.pdf 2018-08-11
12 881-MUM-2012-CORRESPONDENCE(25-3-2013).pdf 2018-08-11
12 881-MUM-2012-Form 18-220216.pdf 2018-08-11
13 881-MUM-2012-CLAIMS(25-3-2013).pdf 2018-08-11
13 881-MUM-2012-FORM 2(25-3-2013).pdf 2018-08-11
14 881-MUM-2012-ABSTRACT.pdf 2018-08-11
14 881-MUM-2012-FORM 2(TITLE PAGE)-(25-3-2013).pdf 2018-08-11
15 881-MUM-2012-ABSTRACT(25-3-2013).pdf 2018-08-11
15 881-MUM-2012-FORM 2(TITLE PAGE).pdf 2018-08-11
16 881-MUM-2012-FER.pdf 2019-02-01
16 881-MUM-2012-FORM 2.pdf 2018-08-11
17 881-MUM-2012-AbandonedLetter.pdf 2019-12-09
17 881-MUM-2012-FORM 3.pdf 2018-08-11
18 881-MUM-2012-Other Patent Document-220216.pdf 2018-08-11
18 881- MUM -2012 - AFR - 31-8-2012.pdf 2023-10-26

Search Strategy

1 searchstartegy881_30-01-2019.pdf