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Organic Potash Composition And A Process For The Preparation Thereof

Abstract: An organic potash composition comprises 75 to 96% by weight incineration ash, and 4 to 25% by weight mixture of natural minerals. Further, a process for the preparation of an organic potash composition comprises incineration ash, is passed through a sieve to obtain sieved ash. 75 - 96% by weight sheaved ash is taken into a granulation drum. 4-25 % by weight mixture of natural minerals are added into the said granulation drum and mixing with sieved ash. Water is added in the granulation drum to obtain moisture in the range of about 15 - 18% and obtain rough granules of different sizes. The rough granules are passed so obtained through dry drum at a temperature of about 500 to 600° C to obtain dry granules having moisture in the range of about 5-8 %. The dry granules are passed through a cooling drum reduces the temperature of the granules and also provides strength to the granules. The granules are passed so obtained through a mesh of the size of about 4-6 mm so as separate undersized and oversized granules and to obtain granules of the size of 4 - 6 mm having moisture in the range of about 5 - 8 % and K 20 in the range of about 15.5 - 28 % to be used as fertilizer.

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Patent Information

Application #
Filing Date
20 January 2022
Publication Number
29/2023
Publication Type
INA
Invention Field
CHEMICAL
Status
Email
Parent Application
Patent Number
Legal Status
Grant Date
2025-01-21
Renewal Date

Applicants

Bharuwa Agri Science Private Limited
Room No. 7, Divya Yog Mandir, Dadubagh, Kankhal,Haridwar , Uttarakhand-249408, India.

Inventors

1. Acharya Balkrishna
Kripalu Bagh Ashram, Kankhal, Haridwar, Uttarakhand-249404, India.

Specification

This invention relates to an organic potash composition and a process for the preparation thereof. Particularly this invention relates to a composition organic potash composition for use as a fertilizer.
Background of the Invention
Roots are the building blocks of a plant, and the growth of roots is an important factor of a plant and crop as a whole. It is found that healthy and web-like roots are needed to maintain the overall health of a plant. In fact, roots are responsible to supply the required amount of nutrients and water are needed for the growth of the plants. The required amount of the nutrients, nowadays, is not found in the soil and therefore different kinds of fertilizers are mixed with the soil to supply nutrients to the plants as and when required. Conventional fertilizers provide nutrients but do not nourish the roots of the plants as such. Therefore, it is required to ensure that the ingredients are mixed precisely and measured to be applied in the fields. Overuse of the known fertilizers can kill the plants and thus the crop.
Japan patent application (JP2006001819A) discloses a method and apparatus for manufacturing phosphorus fertilizer using incineration ash. The method comprises in adding sewage sludge incineration ash as a raw material and add additives such as magnesium and calcium, heat in a melting furnace, separate into molten metal and molten slag, let out molten slag, and then rapidly cool to phosphorus fertilizer, total phosphoric acid

concentration of the raw incineration ash is measured, and when the total phosphoric acid concentration is lower than a predetermined target product concentration, the addition ratio of the high phosphorus-containing waste is obtained before the melting treatment. A method for producing a phosphorus fertilizer, which is added to raw material to increase the concentration of soluble phosphonic acid in the product to a predetermined value to produce a product having a stable soluble phosphonic acid concentration.
WIPO patent application (WO2005123629A1) discloses a method and apparatus for producing phosphate fertilizer utilizing sludge incineration ash containing phosphorus component as the main raw material, auxiliary materials containing magnesium, calcium, and Z or potassium components and a reducing agent are added, and heated and melted at 1350 to 1450 ° C in a melting furnace. A method of producing a phosphate fertilizer by separating the molten slag into two layers of molten metal and a molten slag in the melting furnace and allowing the molten slag to flow out, and then quenching the molten slag to produce phosphate fertilizer. Before adding the reducing agent, measure the total phosphoric acid concentration of the incinerated ash of the main raw material, and if the total phosphoric acid concentration is lower than the target product concentration, add the high phosphorus content before melting. A method for producing a phosphate fertilizer comprises determining a ratio and adding the mixture into a melting

furnace to produce a product having 6 to 25% of soluble phosphate in product.
WP patent application (WO2005123629A1) discloses a sludge incineration ash containing phosphorus component as the main raw material, auxiliary materials containing magnesium, calcium, and Z or potassium components, and a reducing agent are added, and heated and melted at 1350 to 1450 ° C in a melting furnace. A method of producing a phosphate fertilizer by separating the molten slag into two layers of molten metal and a molten slag in the melting furnace and allowing the molten slag to flow out, and then quenching the molten slag to produce phosphate fertilizer. Before adding the reducing agent, measure the total phosphoric acid concentration of the incinerated ash of the main raw material, and if the total phosphoric acid concentration is lower than the target product concentration, add the high phosphorus content before melting. A method for producing a phosphate fertilizer comprises determining a ratio and adding the mixture into a melting furnace to produce a product having 6 to 25% of soluble phosphate in product.
Indian patent no. 230555 (211/DEL/2002) discloses a process for the manufacture of fly ash based soil conditioner cum fertilizer which comprises mixing fly ash in the range of 80 to 95 wt % with grounded phosphatic rock in the range of 3 to 10 wt % and potassium chloride in the range of 0.5 to 4.0 wt% with water under constant shaking to form a workable mixture;

adding to the said workable mixture urea in the range of 0.5 to 5.0 wt % and humic acid in the range of 0.3 to 1.0 wt % to obtain urea- humic acid slow-release type formulation; subjecting the resulting mixture to room temperature and adding bio-fertilizer in the range of 0.15 to 0.35 wt %, under constant stirring for around 10 minutes after each addition and discharging the resulting mixture at room temperature to obtain fly ash based soil conditioner cum fertilizer.
Chinese patent no. (CN102219564B) discloses about organic potassic fertilizer, makes: make apple residue fermenting raw materials, potassium hydroxide aqueous solution heating hydrolysis, make biogenic organic acid potassium water-soluble organic matter by the following method; For excessive potassium hydroxide, biogenic organic acid neutralization, filtration, obtain organic potassic fertilizer.
Chinese patent no. (CN102219564B) discloses about an organic phosphatic fertilizer (potash fertilizer) fertilizer is described, comprises animal organic materials (deglued bone meal bone piece, degelatinized bone dust bone piece, bone black, bone ash, sclerotin secondary calcium phosphate, fishbone powder).
There are disadvantages associated with the known fertilizer compositions. One of the disadvantages is that known fertilizer compositions are more expensive than natural fertilizers as the known fertilizers contain more synthetic/chemical ingredients.

Another disadvantage associated with the known fertilizer compositions is that conventional fertilizers have chemicals which are potentially harmful to the skin and respiratory system of human beings.
Yet another disadvantage associated with the known fertilizer compositions is that conventional fertilizers have such chemicals which are harmful to the microorganisms that live in the soil.
Still another disadvantage associated with the known fertilizer compositions is that conventional fertilizers are highly soluble in water, and as a result, they leach into groundwater, and thus do not provide a full benefit to the plant as it has fewer nutrients available to it.
A further disadvantage associated with the known fertilizer compositions is that conventional fertilizers cause pollution of water as the chemicals used in the fertilizer are leaching away from chemical fertilizer and into the soil.
Another disadvantage associated with the known fertilizer compositions is that the chemicals used in the conventional fertilizers seep into the subsoil and interact with clay resulting in the formation of impermeable layers known as hardpan and as a result the soil becomes compacted.
Yet another disadvantage associated with the known fertilizer compositions is that conventional fertilizers have such chemicals which pollute the natural quality of the soil is have been diminished.

Still another disadvantage associated with the known fertilizer compositions is that known fertilizers are accumulated in soil over time, resulting in long-term imbalances in the soil's pH and fertility.
OBJECTIVE OF THE INVENTION
Therefore, an object of the present invention is to provide an organic potash composition and a process for the preparation thereof which obviates the disadvantages associated with the known chemical fertilizer.
Another object of the present invention is to provide an organic potash composition and a process for the preparation thereof to provide a cheap natural fertilizer having non-chemical ingredients.
Yet another object of the present invention is to provide an organic potash composition capable to increase the creation of flowers and the production of seeds.
Still another object of the present invention is to provide an organic potash composition which increases plant resistance to disease and aids in the preparation of the plant for winter.
A further object of the present invention is to provide an organic potash composition having natural ingredients which are not potentially harmful to the skin and respiratory system of human beings.

Another object of the present invention is to provide an organic potash composition having natural ingredients which are not harmful to the microorganisms present in the soil.
Yet another object of the present invention is to provide an organic potash composition having natural chemicals with enough nutrients which are non-soluble in water and therefore do not leach into groundwater and also provide full benefit to the plant.
Still another object of the present invention is to provide an organic potash composition which does not cause pollution in water and thus does not leach away into the soil.
A further object of the present invention is to provide an organic potash composition having natural ingredients which do not seep into the subsoil and also do not interact with clay therefore impermeable layers are not formed and thus soil does not become compacted.
Another object of the present invention is to provide an organic potash composition having natural ingredients which do not pollute the natural quality of the soil and thus do not diminish the soil.
Yet another object of the present invention is to provide an organic potash composition which does not accumulate in the soil over time and therefore soil's pH and fertility are not affected and thus no imbalance of pH and fertility is caused.

STATEMENT OF THE INVENTION
According to this invention, there is provided an organic potash composition comprising 75 - 96 % by weight sugar cane incineration ash. The mixture of natural minerals comprises, for example, Dolomite 10-30% and Bentonite 70-90%.
Further, according to this invention, there is provided a process to prepare organic potash composition comprising:
i) Passing the incineration ash through a sieve to obtain sieved ash,
ii) Taking 75 - 96% by weight sheaved ash into a granulation drum, iii) Adding 4-25 % by weight mixture of natural minerals into the
said granulation drum and mixing with sieved ash, iv) Added water in the granulation drum to obtain moisture in the
range of about 15 - 18% and obtain rough granules of different
sizes, v) Passing rough granules so obtained through dry drum at a
temperature of about 500 to 600° C to obtain dry granules having
moisture in the range of about 5-8 %, vi) Passing dry granules through a cooling drum at a temperature of
about 20 to 25° C to reduce the temperature of the granules and
also to provide strength to the granules, vii) Passing the granules so obtained through a mesh of the size of
about 4 - 6 mm so as separate undersized and oversized
granules and to obtain granules of the size of 4 - 6 mm having

moisture in the range of about 5 - 8 % and K 20 in the range of about 15.5 - 28 % to be used as fertilizer.
BRIEF DESCRIPTION OF THE ACCOMPANYING DRAWINGS
An organic potash composition and a process for the preparation thereof, according to a preferred embodiment of the present invention, is herein described and illustrated in the accompanying examples.
DETAILED DESCRIPTION OF THE INVENTION
An organic potash composition and a process for the preparation thereof is herein described with numerous specific details so as to provide a complete understanding of the invention. However, these specific details are exemplary details and should not be treated as a limitation to the scope of the invention. Throughout this specification the word "comprise" or variations such as "comprises or comprising", will be understood to imply the inclusions of a stated element, integer or step, or group of elements, integers or steps, but not the exclusions of any other element, integer or step or group of elements, integers or steps.
An organic potash composition / organic fertilizer composition, according to an embodiment of the present invention comprises 75 - 96 % by weight sugar cane incineration ash. The mixture of natural minerals comprises, for example, Dolomite 10-30% and Bentonite 70-90%.
The incineration ash, according to an embodiment, is derived from molasses. The ash derived from molasses comprises, for example, 75 - 96

% by weight sugar cane incineration ash. The mixture of natural minerals comprises, for example, Dolomite 10-30% and Bentonite 70-90%.
The organic potash composition / organic fertilizer, according to the process of the present invention, is prepared by passing the incineration ash through a sieve to obtain sieved ash. Then 75 - 96% by weight sheaved ash is taken into a granulation drum. Subsequently, 4-25 % by weight mixture of natural minerals is added into the said granulation drum and is mixed properly with sieved ash. The water is then added in the granulation drum to obtain moisture in the range of about 15 - 18% and to obtain rough granules of different sizes. The rough granules so obtained are then passed through dry drum at a temperature of about 500 to 600° C to obtain dry granules having moisture in the range of about 5-8 %. The dry granules are then passed through a cooling drum at a temperature of about 20 to 25° C to reduce the temperature of the granules and also to provide strength to the granules. The granules so obtained are passed through a mesh of the size of about 4 - 6 mm so as separate undersized and oversized granules and to obtain granules of the size of 4 - 6 mm having moisture in the range of about 5 -8 % and K 20 (what is K20, please elaborate it) in the range of about 15.5 -28 %. The granules so obtained are packed for use as a fertilizer.
In one embodiment the steps of passing dry granules through the cooling drum at a temperature of about 20 to 25° C is repeated to obtain the required shape of the granules and have proper strength.

The organic potash composition is also useful to grow healthy flowers in order to prepare a landscape. Also, the invented organic potash composition has the following advantages;
1. The organic potash composition / organic fertilizer of the present invention has a balanced amount of the nutrients needed to grow the crops,
2. improve the retention power of the soil for water and nutrients,
3. in improving the accretion rate for nutrients and micro-organisms in the soil,
4. organic fertilizer composition that contains 14.5% to 28% potash,
5. calcium, magnesium, zinc, ferrous, and sulfur that is helpful in maintaining good soil structure and nutrient supplements.
The organic potash composition and a process for the preparation thereof are herein described and illustrated with the help of the following examples;
EXAMPLE-1:
96 kg Ash (derived from molasses) was taken in a granulation drum. 4 kg mixture of natural minerals was subsequently added into the granulation drum. The required amount of water was then added into the granulation drum such that to obtain moisture of 18% and rough granules. The granules so obtained were passed through a dry drum at a temperature of 600° C. The mixture so obtained was then passed through a cooling drum at a temperature of 25° C to reduce the temperature of granules. This procedure

provides strength to granules and also to provide strength to the granules. The granules so obtained were then passed through a mesh of the size of about 4-6 mm so as separate undersized and oversized granules and to obtain granules of the size of 4 - 6 mm having moisture in the range of about 8 % and K 20 in the range of about 28 % to be used as fertilizer.
Example - 2:
90 kg ash (derived from molasses) was taken in a granulation drum. 10 kg mixture of natural minerals was subsequently added into the granulation drum. The required amount of water was then added into the granulation drum such that to obtain moisture of 15% and rough granules. The granules so obtained were passed through a dry drum at a temperature of 500° C. The mixture so obtained was then passed through a cooling drum at a temperature of 20° C to reduce the temperature of granules. This procedure provides strength to granules and also to provide strength to the granules. The granules so obtained were then passed through a mesh of the size of about 4-6 mm so as separate undersized and oversized granules and to obtain granules of the size of 4 - 6 mm having moisture in the range of about 5 % and K 20 in the range of about 15.5 % to be used as fertilizer.
The organic fertilizer so obtained was then analyzed for its quality and the following nutrients were found in the final products of examples 1 and 2;
• Carbon 2-8%,
• Magnesium 0.25-1%

• Potassium 14.5-30%
• Calcium 6-8%
• Iron 0.6-1 %
• Zinc .5-1.2%
• Sulphur 2-5%
• Manganese 0.01-0.05%
• Boron 0.01-0.2%, and
• Chlorine 0.10-1.0%
Certain features of the invention have been described with reference to the example embodiments. However, the description is not intended to be construed in a limiting sense. Various modifications of the example embodiments as well as other embodiments of the invention, which are apparent to the persons skilled in the art to which the invention pertains, are deemed to lie within the spirit and scope of the invention.

We Claim:
1. An organic potash composition comprising 75 to 96% by weight
incineration ash and 4 to 25% by weight mixture of natural minerals.
2. The organic potash composition as claimed in claim 1, wherein the incineration ash comprises, for example, ash obtained from molasses having 4-25 % by weight farm sugar cane incineration ash, 75 - 96% by weight organic wastage base ash, etc.
3. The organic potash composition as claimed in claim 1, wherein the mixture of natural minerals comprises, for example, Dolomite 10-30 %, bentonite70-90%.
4. A process for the preparation of an organic potash composition comprising:
i) Passing the incineration ash through a sieve to obtain sieved
ash, ii) Taking 75 - 96% by weight sheaved ash into a granulation
drum, iii) Adding 4-25 % by weight mixture of natural minerals into the
said granulation drum and mixing with sieved ash, iv) Added water in the granulation drum to obtain moisture in the
range of about 15 - 18% and obtain rough granules of different
sizes, v) Passing rough granules so obtained through dry drum at a
temperature of about 500 to 600° C to obtain dry granules
having moisture in the range of about 5-8 %,

vi) Passing dry granules through a cooling drum reduces the temperature of the granules and also provides strength to the granules, vii) Passing the granules so obtained through a mesh of the size of about 4 - 6 mm so as separate undersized and oversized granules and to obtain granules of the size of 4 - 6 mm having moisture in the range of about 5 - 8 % and K 20 in the range of about 15.5 - 28 % to be used as fertilizer. 5. A process for the preparation of an organic potash composition as claimed in claim 4, where dry granules are passed through the cooling drum at a temperature of about 20 to 25° C.

Documents

Application Documents

# Name Date
1 202211003301-STATEMENT OF UNDERTAKING (FORM 3) [20-01-2022(online)].pdf 2022-01-20
2 202211003301-POWER OF AUTHORITY [20-01-2022(online)].pdf 2022-01-20
3 202211003301-FORM FOR SMALL ENTITY(FORM-28) [20-01-2022(online)].pdf 2022-01-20
4 202211003301-FORM FOR SMALL ENTITY [20-01-2022(online)].pdf 2022-01-20
5 202211003301-FORM 1 [20-01-2022(online)].pdf 2022-01-20
6 202211003301-EVIDENCE FOR REGISTRATION UNDER SSI(FORM-28) [20-01-2022(online)].pdf 2022-01-20
7 202211003301-EVIDENCE FOR REGISTRATION UNDER SSI [20-01-2022(online)].pdf 2022-01-20
8 202211003301-COMPLETE SPECIFICATION [20-01-2022(online)].pdf 2022-01-20
9 202211003301-MSME CERTIFICATE [29-04-2024(online)].pdf 2024-04-29
10 202211003301-FORM28 [29-04-2024(online)].pdf 2024-04-29
11 202211003301-FORM 18A [29-04-2024(online)].pdf 2024-04-29
12 202211003301-FER.pdf 2024-06-07
13 202211003301-OTHERS [18-10-2024(online)].pdf 2024-10-18
14 202211003301-FER_SER_REPLY [18-10-2024(online)].pdf 2024-10-18
15 202211003301-COMPLETE SPECIFICATION [18-10-2024(online)].pdf 2024-10-18
16 202211003301-US(14)-HearingNotice-(HearingDate-30-12-2024).pdf 2024-12-02
17 202211003301-Correspondence to notify the Controller [26-12-2024(online)].pdf 2024-12-26
18 202211003301-Written submissions and relevant documents [11-01-2025(online)].pdf 2025-01-11
19 202211003301-Annexure [11-01-2025(online)].pdf 2025-01-11
20 202211003301-PatentCertificate21-01-2025.pdf 2025-01-21
21 202211003301-IntimationOfGrant21-01-2025.pdf 2025-01-21

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