-2-Field of Invention:
The present invention relates to Process for preparing instant hair pack for revitalizing hair and scalp.
Prior Art:
In the market various lotions/chemicals are available which claim revitalizing hair and scalp. However, such lotions/chemicals do not achieve the desired results in that same have side effects pertaining to skin problems. Furthermore, none of these available lotion/chemicals can be used instantly as a hair pack and therefore, commercially same are not viable.
It has therefore been a long-felt need to develop such a hair pack for revitalizing for hair and scalp which not only overcomes above disadvantages but is ecofriendly to skin and scalp and to hair and is cheaper to make and economically viable.
This and other objects of the present invention have been achieved by the instant hair pack for revitalizing hair and scalp of the present invention.
According to the present invention there is provided Process for preparing instant hair pack for revitalizing hair and scalp which comprises:
(i) preparing herbal extract as herein described;
(ii) preparing of Kera Herb mixture 11 as herein described;
(iii) autoclaving the mixture of Step (i) and Step (ii) on the same day;

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(iv) preparing a mixture of Multani matti which has been previously sieved to
80 to 120 mesh sieve mixed with DM water and incorporating the mixture in
autoclave mixture of Step (iii);
(v) adding balance of water, poly ethylene glycol 1500, cationic conditioner
such as herein described, Structure XL, D Panthenol, Methyl Paraben and Tulsi
paste and heating the above mixture while stirring 75 to 90°C;
(vi) taking Cetostearyl Alcohol, Emulsifying wax, Liquid paraffin,
Dimethicone, Bis(C13-15 Alkoxy) PG Amodimethicone, PEG/PPG-15/15
Dimethicone, Brij 721, Grape seed oil and Propyl paraben and melting the said
material at 75 to 90°C while slowly stirring the same, adding the obtained
material in a mixing kettle containing the hot water at 75 to 85°C to homogenize
the same;
(vii) adding Multani matti paste of step (iv) to said mixture of step (vi) at 65 to
85°C and homogenizing the same;
(viii) and if desired adding Almond oil, Jajoba oil to paste of Step (vii)
followed by addition of Cyclopentasiloxane, Dimethiconol(CMlOOO) at 50 to
70°C followed by autoclaving the obtained herbal extract while mixing;
(ix) adding DM water at 40 to 50°C followed by addition of known
preservative Menthol, perfume and Lemon oil at 25 to 35°C;
(x) and finally storing the obtained product in a place away from excessive
heat and moisture.
The said herbal extracts consists of following ingredients:

-4-

1 Methi Extract 2.0000 — 3.0000
2 Seweed Extract 2.0000 — 3.0000
3 Rita Extract 1.0000 — 2.0000
4 Mehndi Extract 0.0500 — 0.2000
5 Amla Extract 0.0500 — 0.2000
6 Shikakai Extract 0.0500 — 0.2000
7 Neem extract 0.0500 — 0.2000
8 Aloe vera Pwder 0.0050 — 0.0100
9 Tulsi Paste 0.1000 — 0.2000
10 Grapeseed Oil 0.1000 — 0.5000
11 Jajoba Oil 0.0100 — 0.0500
12 Almond Oil 0.0500 — 0.2000
13 Lemon Oil 0.1000 — 0.2000
14 Multani Matti 3.0000 — 6.0000
15 Methyl Paraben 0.1000 — 0.1500
16 Propyl Paraben 0.1000 — 0.1500
17 Poly ethelyn glycol 1500 1.5000 — 2.5000
18 Polymer / Thickener 1.0000 — 2.0000
19 Cationic Conditioner 1.0000 — 2.0000
20 Structure XL 1.0000 — 2.0000
21 D Panthenol 0.1000 — 0.5000
22 DM Water QS to 100 Ltrs. / Kgs
23 Liquid Paraffin Light 4.0000 — 6.0000
24 Cetostearyl Alcohol 1.0000 — 3.0000
25 Emulsifyng wax (Non ionic) 1.0000 — 3.0000
26 Dimethicone 0.5000 — 1.0000
27 Brij 721 1.0000 — 3.0000
28 Sodium Lactate 1.0000 — 2.0000
29 Soya Protein 0.1000 — 0.5000
30 Conditioner 1.0000 — 2.0000
31 Bis (C13-15 Alkoxy) PG Amodimethicone 0.5000 — 1.0000
32 PEG/PPG-25/15 Dimethicone 0.5000 — 1.0000
33 Glycine 0.1000 — 0.5000

~5~

34353637 38 39 DL Panthenol Panthenyl ethyl etherPreservative Menthol Citric acid Perfume (if desired) 0.1000 — 0.5000 0.0500 — 0.10000.0100— 0.0500 0.0100— 0.0500 QS. To adjust pH 0.3000— 0.6000
Likewise, Keraherb 11 is selected from :

12 3 3 4 5 6 7 8 9 10 Ushir Extract Brahmi Extract Gulab phool Extract Anantamool Extract Chamomile Extract Jatamansi Extract Behra Extract Keshut Extract Sailaja Extract Arnica Extract Japa Extract 0.0100— 0.0700 0.0100— 0.0700 0.0100— 0.0700 0.0100— 0.0700 0.0100— 0.0700 0.0100— 0.0700 0.0100— 0.0700 0.0100— 0.0700 0.0100— 0.0700 0.0100— 0.0700 0.0100 — 0.0700
We now give below various ingredients of instant hair pack in quantities (in Kgs for 100 Lts/Kgs.):

SL NO. INGREDIENTS QUANTITY (in KG) (for 100 Ltrs/Kgs.)
12 3 45 67 8 Methi Extract Seweed Extract Rita Extract Mehndi ExtractAmla Extract Shikakai Extract Neem extract Aloe vera Pwder 2.0000 — 3.0000 2.0000 — 3.0000 1.0000— 2.0000 0.0500— 0.20000.0500— 0.2000 0.0500— 0.2000 0.0500— 0.2000 0.0050— 0.0100

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9 Tulsi Paste 0.1000 — 0.2000
10 Grapeseed Oil 0.1000 — 0.5000
11 Jajoba Oil 0.0100 — 0.0500
12 Almond Oil 0.0500 — 0.2000
13 Lemon Oil 0.1000 — 0.2000
14 Multani Matti 3.0000 — 6.0000
15 Methyl Paraben 0.1000 — 0.1500
16 Propyl Paraben 0.1000 — 0.1500
17 Poly ethelyn glycol 1500 1.5000 — 2.5000
18 Polymer / Thickener 1.0000 — 2.0000
19 Cationic Conditioner 1.0000 — 2.0000
20 Structure XL 1.0000 — 2.0000
21 D Panthenol 0.1000 — 0.5000
22 DM Water QSto lOOLtrs./Kgs
23 Liquid Paraffin Light 4.0000 — 6.0000
24 Cetostearyl Alcohol 1.0000 — 3.0000
25 Emulsifyng wax (Non ionic) 1.0000 — 3.0000
26 Dimethicone 0.5000 — 1.0000
27 Brij 721 1.0000 — 3.0000
28 Sodium Lactate 1.0000 — 2.0000
29 Soya Protein 0.1000 — 0.5000
30 Conditioner 1.0000 — 2.0000
31 Bis (C13-15 Alkoxy) PG Amodimethicone 0.5000 — 1.0000
32 PEG/PPG-25/15 Dimethicone 0.5000 — 1.0000
33 Glycine 0.1000 — 0.5000
34 DL Panthenol 0.1000 — 0.5000
35 Panthenyl ethyl ether 0.0500 — 0.1000
36 Preservative 0.0100 — 0.0500
37 Menthol 0.0100 — 0.0500
38 Citric acid QS. To adjust pH
39 Perfume 0.3000 — 0.6000
KERAHERB 11
40 Ushir Extract 0.0100 — 0.0700
41 Brahmi Extract 0.0100 — 0.0700

_ *7 —

42 Gulab phool Extract 0.0100— 0.0700
43 Anantamool Extract 0.0100— 0.0700
44 Chamomile Extract 0.0100— 0.0700
45 Jatamansi Extract 0.0100— 0.0700
46 Behra Extract 0.0100— 0.0700
47 Keshut Extract 0.0100— 0.0700
48 Sailaja Extract 0.0100— 0.0700
49 Arnica Extract 0.0100— 0.0700
50 Japa Extract 0.0100— 0.0700
We shall now describe the present invention in detail, which is given in stage wise: Stage: 1 (Preparation of Aqueous herbal extract)
All the herbs are cleaned well and cut into small pieces before being used. Weighed as per the formula quantity and are immersed into hot boiling water and soaked well The required quantities of preservatives are to be added. The vessel to be left as such in loosely closed condition, for at least 8 to 14 hours, preferably overnight. Filtered through a 80 - 120 mesh nylon cloth and also through a sparkler filter or a suitable clean, dry, sterilized filter bag. The loss of water is made up by adding the required amount of previously boiled and cooled DM water. Add the required quantity of Aloe vera powder extract. This aqueous herbal mixture is stored in a clean well closed SS / HDPE container. This herbal mixture is to be used within 20 - 24 hours.
Stage: 2 (Preparation of Kera Herb mixture 11)
All the 11 herbs are cleaned well and cut into small pieces before being used. Weighed as per the formula quantity and are immersed into hot boiling water, the herbs are soaked well and preservatives added. The vessel to be left as such in loosely closed condition, for at least 8 to 14 hours, preferably

overnight. Filtered through a 80 - 120 mesh nylon cloth and also through a sparkler filter or a suitable clean, dry, sterilized filter bag. The loss of water is made up by adding the required amount of previously boiled and cooled DM water. This aqueous herbal mixture is stored in a clean well closed SS / HDPE container. This herbal mixture is to be used within20 - 24 hours.
Stage: 3
Both the filtered herbal mixtures of Stage 1 & Stage 2 are to be Autoclaved at 12 to 16 lbs pressure for 25-35 minutes. The Autoclaving to be done on the same day the batch being produced.
Stage: 4
Weigh the formula quantity of Multani matti which has been previously sieved through a sieving machine fitted with an SS 80 - 120 mesh sieve. Mix well with a portion of DM water and pass the total material through a suitable colloid mill until a homogeneous paste like material is obtained. This mixture is to be prepared a couple of hours before being incorporated in the batch. Stage: 5
The balance formula quantity of DM water, is taken in a suitable gel preparation kettle, along with the other water phase ingredients, Poly ethelyn glycol 1500, Cationic conditioner, Structure XL, D panthenol, Methyl paraben and Tulsi paste. Heat the total material with constant stirring up to 75 - 90° C, transfer the material into a suitable mixing SS kettle (fitted with an high speed homogenisor and an effective mixing system, SS jacket for heating and cooling) after straining the same through a 80 - 120 mesh nylon filter cloth. Start the homogenizer and the mixing. Add the formula quantity of polymer/thickener gradually in to the mixer.

-9-Stage: 6
Simultaneously weigh the formula quantities of materials consisting of Cetostearyl alcohol, Emulsifying wax (nonionic), Liquid paraffin, Dimethicone, Bis (C13-15 Alkoxy) PG Amodimethicone, PEG/PPG-15/15 Dimethicone, Brij 721, Grape seed oil and Propyl paraben. Melt the total material in a suitable melting kettle to around 75 - 90° C, with slow speed stirring. Add the heated oil phase of Stage 6, into the mixing kettle containing the hot water phase, after straining through a 80 - 120 mesh nylon filter cloth, ensure that the temperatures of both phases during addition is above 75 - 85° C. Continue homogenizing. At about 65-85° C, add the Multani matti paste and a formula quantity mixture of Dl panthenol, Panthenyl ethyl ether & Glycine gradually, Stop the homogenizer after about 10-20 minutes. Continue mixing and scrapping at 15-25 RPM speed. Start cool water circulation when the temp of the mass is about 55 - 70°C, add the formula quantities of Almond oil and Jajoba oil, continue mixing and scrapping. Add the formula quantities of Sodium lactate and Cyclopentasiloxane, dimethiconol (CM 1000), at about 50 - 70°C. followed by the autoclaved herbal extracts Continue mixing.
Add the formula quantities of materials of Soya protein and DM water, at about 50 - 60° C. Stop cool water circulation and run chilled water circulation Continue mixing. At around 40 - 50°C add the required formula quantities of Preservative and Menthol, Perfume and Lemon oil. Mix well. At about 25 -35°C, the total material is milled in a colloid mill until a smooth fine homogeneous glossy paste like material is obtained. Drop the batch into clean sanitized SS storage vessels or clean HDPE plastic vats properly closed.

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Stage: 7
The bulk storage vats / vessels containing product of present invention is stored in a place away from excessive heat and moisture.

-11-
WE CLAIM:
1. Process for preparing instant hair pack for revitalizing hair and scalp which comprises:
(i) preparing herbal extract such as herein described;
(ii) preparing of Kera Herb mixture 11 such as herein described;
(iii) autoclaving the mixture of Step (i) and Step (ii) on the same day;
(iv) preparing a mixture of Multani matti which has been previously sieved to
80 to 120 mesh sieve mixed with DM water and incorporating the mixture in
autoclave mixture of Step (iii);
(v) adding balance of water, poly ethylene glycol 1500, cationic conditioner
such as herein described, Structure XL, D Panthenol, Methyl Paraben and Tulsi
paste and heating the above mixture while stirring 75 to 90°C;
(vi) taking Cetostearyl Alcohol, Emulsifying wax, Liquid paraffin,
Dimethicone, Bis(C13-15 Alkoxy) PG Amodimethicone, PEG/PPG-15/15
Dimethicone, Brij 721, Grape seed oil and Propyl paraben and melting the said
material at 75 to 90°C while slowly stirring the same, adding the obtained
material in a mixing kettle containing the hot water at 75 to 85°C to homogenize
the same;
(vii) adding Multani matti paste of step (iv) to said mixture of step (vi) at 65 to
85°C and homogenizing the same;
(viii) and if desired adding Almond oil, Jajoba oil to paste of Step (vii) followed
by addition of Cyclopentasiloxane, Dimethiconol(CMlOOO) at 50 to 70°C
followed by autoclaving the obtained herbal extract while mixing;

- 12,-
(ix) adding DM water at 40 to 50°C followed by addition of known preservative Menthol, perfume and Lemon oil at 25 to 35°C;
(x) and finally storing the obtained product in a place away from excessive heat and moisture.
2. Process for preparing instant hair pack for revitalizing hair and scalp as claimed in claim 1, wherein the said herbal extract consists of following ingredients:

12 3 4 Methi Extract Seweed Extract Rita Extract Mehndi Extract 2.0000 — 3.0000 2.0000 — 3.0000 1.0000— 2.0000 0.0500— 0.2000
5 6 7 8 9 Amla Extract Shikakai Extract Neem extract Aloe vera Pwder Tulsi Paste 0.0500— 0.2000 0.0500— 0.2000 0.0500— 0.2000 0.0050— 0.0100 0.1000— 0.2000
10 11 12 13 14 Grapeseed Oil Jajoba Oil Almond Oil Lemon Oil Multani Matti 0.1000— 0.5000 0.0100— 0.0500 0.0500— 0.2000 0.1000— 0.2000 3.0000— 6.0000
15 16 17 18 19 20 Methyl Paraben Propyl Paraben Poly ethelyn glycol 1500 Polymer / Thickener Cationic Conditioner Structure XL 0.1000— 0.1500 0.1000— 0.1500 1.5000— 2.5000 1.0000— 2.0000 1.0000— 2.0000 1.0000— 2.0000
21 22 23 D Panthenol DM Water Liquid Paraffin Light 0.1000 — 0.5000 QSto lOOLtrs./Kgs. 4.0000— 6.0000

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24 Cetostearyl Alcohol 1.0000— 3.0000
25 Emulsifyng wax (Non ionic) 1.0000— 3.0000
26 Dimethicone 0.5000— 1.0000
27 Brij 721 1.0000— 3.0000
28 Sodium Lactate 1.0000— 2.0000
29 Soya Protein 0.1000— 0.5000
30 Conditioner 1.0000— 2.0000
31 Bis (C13-15 Alkoxy) PG Amodimethicone 0.5000— 1.0000
32 PEG/PPG-25/15 Dimethicone 0.5000— 1.0000
33 Glycine 0.1000 — 0.5000
34 DL Panthenol 0.1000 — 0.5000
35 Panthenyl ethyl ether 0.0500 — 0.1000
36 Preservative 0.0100— 0.0500
37 Menthol 0.0100— 0.0500
38 Citric acid QS. To adjust pH
39 Perfume (if desired) 0.3000— 0.6000
3. Process for preparing instant hair pack for revitalizing hair and scalp as claimed in claim 1 or 2, whrein Keraherb 11 is selected from:-

1 Ushir Extract 0.0100— 0.0700
2 Brahmi Extract 0.0100— 0.0700
3 Gulab phool Extract 0.0100— 0.0700
3 Anantamool Extract 0.0100— 0.0700
4 Chamomile Extract 0.0100— 0.0700
5 Jatamansi Extract 0.0100— 0.0700
6 Behra Extract 0.0100— 0.0700
7 Keshut Extract 0.0100— 0.0700
8 Sailaja Extract 0.0100— 0.0700
9 Arnica Extract 0.0100— 0.0700
10 Japa Extract 0.0100— 0.0700

Process for preparing instant hair pack for revitalizing hair and scalp which comprises: (i) preparing of herbal extract as herein described, (ii) preparing of Kera Herb mixture 11 as herein described, (iii) autoclaving the mixture of Step (i) and Step (ii) on the same day; (iv) preparing a mixture of Multani matti which has been previously sieved to 80 to 120 mesh sieve mixed with DM water and incorporating the mixture in autoclave mixture of Step (iii); (v) adding balance of water, poly ethylene glycol 1500, cationic conditioner such as herein described, Structure XL, D Panthenol, Methyl Paraben and Tulsi paste and heating the above mixture while stirring 75 to 90°C; (vi) taking Cetostearyl Alcohol, Emulsifying wax, Liquid paraffin, Dimethicone, Bis(C13-15 Alkoxy) PG Amodimethicone, PEG/PPG-15/15 Dimethicone, Brij 721, Grape seed oil and Propyl paraben and melting the said material at 75 to 90°C while slowly stirring the same, adding the obtained material in a mixing kettle containing the hot water at 75 to 85°C to homogenize the same; (vii) adding Multani matti paste of step (iv) to said mixture of step (vi) at 65 to 85°C and homogenizing the same; (viii) and if desired adding Almond oil, Jajoba oil to paste of Step (vii) followed by addition of Cyclopentasiloxane, Dimethiconol(CMlOOO) at 50 to 70°C followed by autoclaving the obtained herbal extract while mixing; (ix) adding DM water at 40 to 50°C followed by addition of known preservative Menthol, perfume and Lemon oil at 25 to 35°C; (x) and finally storing the obtained product in a place away from excessive heat and moisture.