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Tannic Acid Exfoliated Tungsten Disulphide Reinforced Natural Rubber Nanocomposite And Method Of Preparation Thereof

Abstract: The invention discloses a biopolymer nanocomposite (100) with improved mechanical, thermal, antibacterial and biocompatibility properties and method (200) of fabrication thereof, are disclosed. The nanocomposite comprises tannic acid (TA) (102) exfoliated tungsten disulphide (WS2) (103) as nanofiller (WT) sheets (104), incorporated into a natural rubber (NR) (101) matrix, wherein the ratio of WS2: TA is 1:4. Amount of nanofiller in the nanocomposites varies from 0.5 to 5 phr of the matrix.. The incorporation of WT nanosheets enhances the mechanical, thermal, antibacterial and biocompatibility properties of rubber latex. Therefore, the obtained NWT green-synthesized nanocomposites hold great potential for diverse biomedical applications.

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Notices, Deadlines & Correspondence

Patent Information

Application #
Filing Date
07 October 2024
Publication Number
45/2024
Publication Type
INA
Invention Field
POLYMER TECHNOLOGY
Status
Email
Parent Application

Applicants

AMRITA VISHWA VIDYAPEETHAM
Amritapuri Campus, Amritapuri, Clappana P O, Kollam – 690525, Kerala, India

Inventors

1. ANANDAVALLY SABARISADANAM, Sethulekshmi
Sabarisadanam, Puthenchantha P.O., Vallikunnam Alappuzha, Kerala 690501
2. APPUKUTTAN, Saritha
Daffodils, Thiruvalla RSPO Thiruvalla Pathanamthitta Dist. – 689111, Kerala

Specification

Description:TANNIC ACID EXFOLIATED TUNGSTEN DISULPHIDE REINFORCED NATURAL RUBBER NANOCOMPOSITE AND METHOD OF PREPARATION THEREOF
CROSS-REFERENCES TO RELATED APPLICATIONS
None.
FIELD OF THE INVENTION
The present invention generally relates to polymer nanocomposites, and in particular to a rubber nanocomposite incorporating nanosheets exfoliated using a bio material to improve mechanical, thermal, antibacterial, and biocompatibility properties of polymer and its method of fabrication.
BACKGROUND OF THE RELATED ART
Transition metal dichalcogenides (TMD) represent a novel category of inorganic layered materials exhibiting metallic, semiconducting, and superconducting nature. Tungsten is a more abundant, cheaper, and less toxic metal in the Earth crust and is one of the heavier transition metals in the TMD group. Thus, tungsten disulfide (WS2) is gaining more research interest today. Bulk WS2 consists of robustly covalently bonded S-W-S sandwiches, here W atoms are situated between two atomic layers of sulfur. Weak van de , Claims:We claim:
1. A biopolymer nanocomposite (100) with improved mechanical, thermal, antibacterial and biocompatibility properties, comprising:
tannic acid (TA) (102) exfoliated tungsten disulphide (WS2) (103) as nanofiller (WT) sheets (104), incorporated into a natural rubber latex (NRL) (101) matrix, wherein the ratio of WS2:TA of 1:4 and amount of nanofiller in the nanocomposites varies from 0.5 to 5 phr of the matrix.

2. The nanocomposite (100) as claimed in claim 1, wherein the XRD analysis gives reduction in the intensity of peak at 14.3° indicating the exfoliation of tungsten disulphide with tannic acid in the NR nanocomposite.

3. The nanocomposite (100) as claimed in claim 1, wherein the optimum phr loading of WT nanosheets in NR is 1.5.

4. The nanocomposite (100) as claimed in claim 1, wherein the tannic acid exfoliated tungsten disulphide/ 1.5 phr loaded NR nanocomposite shows at least one of
23% increase in cross linking density,
32% increase in tensile strength,
7% increase in elongation a

Documents

Application Documents

# Name Date
1 202441075669-STATEMENT OF UNDERTAKING (FORM 3) [07-10-2024(online)].pdf 2024-10-07
2 202441075669-FORM FOR SMALL ENTITY(FORM-28) [07-10-2024(online)].pdf 2024-10-07
3 202441075669-FORM 1 [07-10-2024(online)].pdf 2024-10-07
4 202441075669-EVIDENCE FOR REGISTRATION UNDER SSI(FORM-28) [07-10-2024(online)].pdf 2024-10-07
5 202441075669-EVIDENCE FOR REGISTRATION UNDER SSI [07-10-2024(online)].pdf 2024-10-07
6 202441075669-EDUCATIONAL INSTITUTION(S) [07-10-2024(online)].pdf 2024-10-07
7 202441075669-DRAWINGS [07-10-2024(online)].pdf 2024-10-07
8 202441075669-COMPLETE SPECIFICATION [07-10-2024(online)].pdf 2024-10-07
9 202441075669-Proof of Right [09-10-2024(online)].pdf 2024-10-09
10 202441075669-FORM-9 [06-11-2024(online)].pdf 2024-11-06
11 202441075669-FORM-8 [06-11-2024(online)].pdf 2024-11-06
12 202441075669-FORM 18 [06-11-2024(online)].pdf 2024-11-06
13 202441075669-RELEVANT DOCUMENTS [19-03-2025(online)].pdf 2025-03-19
14 202441075669-POA [19-03-2025(online)].pdf 2025-03-19
15 202441075669-FORM 13 [19-03-2025(online)].pdf 2025-03-19
16 202441075669-OTHERS [06-05-2025(online)].pdf 2025-05-06
17 202441075669-EDUCATIONAL INSTITUTION(S) [06-05-2025(online)].pdf 2025-05-06