Abstract: The present invention relates to the process for the preparation of sodium 2-mercaptoethanesulfonate of formula (I). More particularly the present invention relates to a process for the preparation of pure sodium 2-mercaptoethanesulfonate salt from 2-thiouronium ethanesulfonate of formula (e) using aqueous ammonia and gaseous ammonia at below room temperature. The pure sodium 2-mercapotethanesulfonate is obtained by purification with alcohol or the mixture of alcohol: water. The HPLC purity of the final product of formula (I) obtained after the purification is more than 99.0% along with less than 1% of impurity-D in the final product of formula (I).
| # | Name | Date |
|---|---|---|
| 1 | 116-MUM-2009-FORM 3(29-11-2010).pdf | 2010-11-29 |
| 1 | 116-MUM-2009-RELEVANT DOCUMENTS [30-09-2021(online)].pdf | 2021-09-30 |
| 2 | 116-mum-2009-abstract.doc | 2018-08-10 |
| 2 | 116-MUM-2009-FORM 18(29-11-2010).pdf | 2010-11-29 |
| 3 | 116-MUM-2009-CORRESPONDENCE(29-11-2010).pdf | 2010-11-29 |
| 3 | 116-mum-2009-abstract.pdf | 2018-08-10 |
| 4 | 116-MUM-2009_EXAMREPORT.pdf | 2018-08-10 |
| 4 | 116-mum-2009-assignment.pdf | 2018-08-10 |
| 5 | 116-MUM-2009-REPLY TO EXAMINATION REPORT(2-7-2013).pdf | 2018-08-10 |
| 5 | 116-MUM-2009-CLAIMS(AMENDED)-(2-7-2013).pdf | 2018-08-10 |
| 6 | 116-MUM-2009-POWER OF ATTORNEY(2-7-2013).pdf | 2018-08-10 |
| 6 | 116-MUM-2009-CLAIMS(GRANTED)-(6-8-2014).pdf | 2018-08-10 |
| 7 | 116-MUM-2009-POWER OF ATTORNEY (2-7-2013).pdf | 2018-08-10 |
| 8 | 116-MUM-2009-MARKED COPY(2-7-2013).pdf | 2018-08-10 |
| 8 | 116-mum-2009-claims.pdf | 2018-08-10 |
| 9 | 116-MUM-2009-CORRESPONDENCE (2-7-2013).pdf | 2018-08-10 |
| 9 | 116-mum-2009-form 26.pdf | 2018-08-10 |
| 10 | 116-MUM-2009-CORRESPONDENCE(2-7-2013).pdf | 2018-08-10 |
| 10 | 116-mum-2009-form 2.pdf | 2018-08-10 |
| 11 | 116-MUM-2009-CORRESPONDENCE(IPO)-(6-8-2014).pdf | 2018-08-10 |
| 12 | 116-mum-2009-correspondence.pdf | 2018-08-10 |
| 12 | 116-mum-2009-form 2(title page).pdf | 2018-08-10 |
| 13 | 116-MUM-2009-FORM 2(TITLE PAGE)-(GRANTED)-(6-8-2014).pdf | 2018-08-10 |
| 14 | 116-mum-2009-description(complete).pdf | 2018-08-10 |
| 14 | 116-MUM-2009-FORM 2(GRANTED)-(6-8-2014).pdf | 2018-08-10 |
| 15 | 116-MUM-2009-DESCRIPTION(GRANTED)-(6-8-2014).pdf | 2018-08-10 |
| 15 | 116-MUM-2009-FORM 13(2-7-2013).pdf | 2018-08-10 |
| 16 | 116-MUM-2009-FORM 1 (2-7-2013).pdf | 2018-08-10 |
| 16 | 116-MUM-2009-FORM 13 (2-7-2013).pdf | 2018-08-10 |
| 17 | 116-MUM-2009-FORM 1(2-7-2013).pdf | 2018-08-10 |
| 17 | 116-mum-2009-form 1.pdf | 2018-08-10 |
| 18 | 116-mum-2009-form 1.pdf | 2018-08-10 |
| 18 | 116-MUM-2009-FORM 1(2-7-2013).pdf | 2018-08-10 |
| 19 | 116-MUM-2009-FORM 1 (2-7-2013).pdf | 2018-08-10 |
| 19 | 116-MUM-2009-FORM 13 (2-7-2013).pdf | 2018-08-10 |
| 20 | 116-MUM-2009-DESCRIPTION(GRANTED)-(6-8-2014).pdf | 2018-08-10 |
| 20 | 116-MUM-2009-FORM 13(2-7-2013).pdf | 2018-08-10 |
| 21 | 116-mum-2009-description(complete).pdf | 2018-08-10 |
| 21 | 116-MUM-2009-FORM 2(GRANTED)-(6-8-2014).pdf | 2018-08-10 |
| 22 | 116-MUM-2009-FORM 2(TITLE PAGE)-(GRANTED)-(6-8-2014).pdf | 2018-08-10 |
| 23 | 116-mum-2009-form 2(title page).pdf | 2018-08-10 |
| 23 | 116-mum-2009-correspondence.pdf | 2018-08-10 |
| 24 | 116-MUM-2009-CORRESPONDENCE(IPO)-(6-8-2014).pdf | 2018-08-10 |
| 25 | 116-MUM-2009-CORRESPONDENCE(2-7-2013).pdf | 2018-08-10 |
| 25 | 116-mum-2009-form 2.pdf | 2018-08-10 |
| 26 | 116-MUM-2009-CORRESPONDENCE (2-7-2013).pdf | 2018-08-10 |
| 26 | 116-mum-2009-form 26.pdf | 2018-08-10 |
| 27 | 116-mum-2009-claims.pdf | 2018-08-10 |
| 27 | 116-MUM-2009-MARKED COPY(2-7-2013).pdf | 2018-08-10 |
| 28 | 116-MUM-2009-POWER OF ATTORNEY (2-7-2013).pdf | 2018-08-10 |
| 29 | 116-MUM-2009-CLAIMS(GRANTED)-(6-8-2014).pdf | 2018-08-10 |
| 29 | 116-MUM-2009-POWER OF ATTORNEY(2-7-2013).pdf | 2018-08-10 |
| 30 | 116-MUM-2009-CLAIMS(AMENDED)-(2-7-2013).pdf | 2018-08-10 |
| 30 | 116-MUM-2009-REPLY TO EXAMINATION REPORT(2-7-2013).pdf | 2018-08-10 |
| 31 | 116-MUM-2009_EXAMREPORT.pdf | 2018-08-10 |
| 31 | 116-mum-2009-assignment.pdf | 2018-08-10 |
| 32 | 116-MUM-2009-CORRESPONDENCE(29-11-2010).pdf | 2010-11-29 |
| 32 | 116-mum-2009-abstract.pdf | 2018-08-10 |
| 33 | 116-MUM-2009-FORM 18(29-11-2010).pdf | 2010-11-29 |
| 34 | 116-MUM-2009-RELEVANT DOCUMENTS [30-09-2021(online)].pdf | 2021-09-30 |
| 34 | 116-MUM-2009-FORM 3(29-11-2010).pdf | 2010-11-29 |